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1. 发明申请

WO2014179647A1 ANALYTICAL METHOD FOR DETECTING FUEL MARKERS USING TWO GAS CHROMATOGRAPHIC CHANNELS WITH TWO SERIALLY-ARRANGED COLUMNS EACH 审中-公开
标题翻译：使用两个气相色谱通道检测燃料标记的分析方法与两个串联排列的色谱柱
公开(公告)号：WO2014179647A1
公开(公告)日：2014-11-06
申请号：PCT/US2014/036493
申请日：2014-05-02
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： GRAS, Ronda L. , LUONG, Jim C. , SMITH, Warren E.
IPC分类号： G01N30/60 , G01N30/72 , G01N33/28 , C10L1/00
CPC分类号： G01N33/2882 , C10L1/003 , G01N30/468 , G01N2030/047 , G01N2030/8854
摘要： A gas chromatographic method for detecting a first marker and a second marker in a fuel in two channels: (i) a first capillary column coated with polysiloxane and a second capillary column coated with polyethylene glycol; and (ii) a third capillary column coated with polymethylphenylsiloxane and a fourth deactivated capillary column. The steps are: (a) introducing a first sample into the first column to produce a first effluent; (b) introducing only a portion of the first effluent into the second column to produce a second effluent; (c) allowing the second effluent to pass through a mass spectrometer; (d) introducing a second sample into the third column to produce a third effluent; (e) introducing only a portion of the third effluent into the fourth column to produce a fourth effluent; (f) allowing the fourth effluent to pass through a mass spectrometer.
摘要翻译：一种用于在两个通道中检测燃料中的第一标记和第二标记的气相色谱法：（i）涂覆有聚硅氧烷的第一毛细管柱和涂有聚乙二醇的第二毛细管柱; 和（ii）涂覆有聚甲基苯基硅氧烷的第三毛细管柱和第四失活毛细管柱。步骤是：（a）将第一样品引入第一塔以产生第一流出物; （b）仅将一部分第一流出物引入第二塔以产生第二流出物; （c）允许第二流出物通过质谱仪; （d）将第二样品引入第三塔以产生第三流出物; （e）仅将一部分第三流出物引入第四塔以产生第四流出物; （f）允许第四流出物通过质谱仪。

2. 发明申请

WO2014179646A1 ANALYTICAL METHOD FOR DETECTING FUEL MARKERS 审中-公开
标题翻译：用于检测燃油标记的分析方法
公开(公告)号：WO2014179646A1
公开(公告)日：2014-11-06
申请号：PCT/US2014/036492
申请日：2014-05-02
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： GRAS, Ronda L. , LUONG, Jim C. , SMITH, Warren E.
IPC分类号： G01N33/28 , G01N30/60 , C10L1/00
CPC分类号： G01N30/7206 , C10L1/003 , G01N30/463 , G01N30/465 , G01N30/6078 , G01N30/7233 , G01N30/88 , G01N33/28 , G01N33/2882 , G01N2030/042 , G01N2030/8854
摘要： A gas chromatographic method for detecting a marker compound in a fuel by (a) introducing a sample of fuel into a first capillary column coated with a stationary phase based on polydimethylsiloxane and allowing the sample to flow through the first column to produce a first effluent; (b) allowing the first effluent to pass through a detector and identifying a retention time range in it which includes a retention time of the marker compound; (c) introducing only a portion of the first effluent stream which is within the retention time range into a second capillary column coated with either (i) an ionic sorbent or (ii) a polyethylene glycol, and allowing said portion to flow through the second capillary column to produce a second effluent stream; and (d) allowing the second effluent to pass through a detector; wherein the marker compound has formula Ar(R 2 ) m (OR 1 ) n and is present in the fuel at a level from 0.01 ppm to 100 ppm.
摘要翻译：一种用于通过以下步骤来检测燃料中的标记化合物的气相色谱法：（a）基于聚二甲基硅氧烷将样品引入到具有固定相的第一毛细管柱中并使样品流过第一塔以产生第一流出物; （b）允许第一流出物通过检测器并鉴定其中包含标记化合物的保留时间的保留时间范围; （c）将仅在保留时间范围内的第一流出物流的一部分引入涂覆有（i）离子吸附剂或（ii）聚乙二醇的第二毛细管柱中，并允许所述部分流过第二流出物流毛细管柱以产生第二流出物流; 和（d）允许第二流出物通过检测器; 其中标记化合物具有式Ar（R 2）m（OR 1）n，并且以0.01ppm至100ppm的水平存在于燃料中。

3. 发明申请

WO2015094544A1 METHOD FOR ANALYSIS OF TRACE LEVELS OF CHEMICAL ADDITIVES IN OIL RECOVERY PRODUCTION FLUIDS 审中-公开
标题翻译：油回收生产液中化学添加剂的痕量分析方法
公开(公告)号：WO2015094544A1
公开(公告)日：2015-06-25
申请号：PCT/US2014/066267
申请日：2014-11-19
申请人： DOW GLOBAL TECHNOLOGIES LLC
发明人： LUONG, Jim C. , GRAS, Ronda L. , WINNIFORD, William L. , AKIYA, Naoko
IPC分类号： E21B21/06 , G01N30/46 , G01N33/28 , G01N30/88
CPC分类号： G01N33/2823 , C09K8/594 , E21B43/2406 , E21B43/34 , E21B49/08 , E21B49/086 , G01N30/463 , G01N30/68 , G01N30/7206 , G01N33/2835 , G01N2030/8854
摘要： Disclosed is a method for analyzing and/or monitoring trace levels of chemical additives in production fluids for oil recovery processes, specifically from heavy oil and/or oil sands. The method comprises and extraction step coupled with a multi-dimensional gas chromatography analysis.
摘要翻译：公开了一种用于分析和/或监测油回收过程的生产流体中痕量水平的化学添加剂的方法，特别是从重油和/或油砂。该方法包括与萃取步骤相结合的多维气相色谱分析。

4. 发明申请

WO2014081556A1 DISTILLABLE FUEL MARKERS 审中-公开
标题翻译：可燃燃料标志
公开(公告)号：WO2014081556A1
公开(公告)日：2014-05-30
申请号：PCT/US2013/068476
申请日：2013-11-05
申请人： ANGUS CHEMICAL COMPANY , DOW GLOBAL TECHNOLOGIES LLC
发明人： GREEN, George David , SWEDO, Raymond , GRAS, Ronda L. , LUONG, Jim C.
IPC分类号： C10L1/00 , C10L1/185
CPC分类号： C10L1/18 , C10L1/003 , C10L1/1852 , C10L10/00 , C10L2200/0446 , C10L2230/02 , C10L2230/16 , C10L2270/026
摘要： A method for marking a petroleum hydrocarbon or a liquid biologically derived fuel by adding to the petroleum hydrocarbon or liquid biologically derived fuel at least one compound having formula Ar(R 2 ) m (OR 1 ) n , wherein Ar is an aromatic ring system having from six to twenty carbon atoms, R 1 is C 1 -C 12 alkyl or C 2 -C 12 alkenyl, R 2 is C 1 -C 12 alkyl or C 3 -C 12 alkenyl, m is an integer from zero to five and n is an integer from one to three; wherein each compound of formula Ar(R 2 ) m (OR 1 ) n is present at a level from 0.01 ppm to 100 ppm.
摘要翻译：一种通过向石油烃或液体生物衍生的燃料中加入至少一种具有式Ar（R 2）m（OR 1）n的化合物来标记石油烃或液体生物衍生的燃料的方法，其中Ar是具有6个至20个碳原子，R 1为C 1 -C 12烷基或C 2 -C 12烯基，R 2为C 1 -C 12烷基或C 3 -C 12烯基，m为0至5的整数，n为1至3的整数; 其中每个式Ar（R 2）m（OR 1）n的化合物以0.01ppm至100ppm的水平存在。

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