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1. 发明申请

WO0212175A3 METHOD FOR PRODUCING HYDROLYSIS-STABLE AMMONIUM NITRILES 审中-公开
标题翻译：用于生产水解铵的亚硝酸盐
公开(公告)号：WO0212175A3
公开(公告)日：2002-04-11
申请号：PCT/EP0108883
申请日：2001-08-01
申请人： CLARIANT GMBH , SCHREIBER MANFRED , BORCHERS GEORG , MOGCK OLIVER , WEINELT FRANK
发明人： SCHREIBER MANFRED , BORCHERS GEORG , MOGCK OLIVER , WEINELT FRANK
IPC分类号： C11D3/395 , C07C253/30 , C07C253/32 , C07C255/24 , C07C255/25 , C07C303/32 , C07C303/42 , C07C309/31 , C11D3/39 , C11D7/54
CPC分类号： C11D3/3925 , C07C253/32 , C07C255/25
摘要： The invention relates to a method for producing hydrolysis-stable ammonium nitriles by reacting a compound of formula (1), wherein R , R , and R are identical or different and represent linear or branched C1-C24-alkyl groups, C2-C24-alkenyl groups, substituted or non-substituted benzyl or C1-C4-alkoxy-C1-C4-alkyl groups, or wherein R and R , together with the nitrogen atom to which they are bonded, form a ring with 4 to 6 C-atoms which can be substituted with C1-C5 alkyl, C1-C5 alkoxy, C1-C5 alkanoyl, phenyl, amino, ammonium, cyano, cyanamino, chlorine or bromine and which can contain in addition to the nitrogen atom, instead of the carbon atoms, one or two oxygen or nitrogen atoms, a group N-R or a group R -N-R , wherein R6 is hydrogen, C1-C5-alkyl, C2-C5-alkenyl, C2-C5-alkinyl, phenyl, C7-C9-aralkyl, C5-C7-cycloalkyl, C1-C6-alkanoyl, cyanomethyl or cyan, R and R are hydrogen, C1-C4-alkyl, C1-C4-alkenyl, C1-C4-alkoxy-C1-C4-alkyl, phenyl or C1-C3-alkylphenyl, preferably hydrogen, methyl or phenyl, R especially meaning hydrogen when R does not mean hydrogen, and X represents an anion; with an alkaline or ammonium salt of an alkane sulfonate, paraffin sulfonate, aryl sulfonate, alcohol sulfate or fatty acid alkyl carboxylate in the presence of water, at a high temperature.
摘要翻译：本发明涉及一种方法，用于由式（1）其中R <1>，R <2>，R <3>是相同的或不同的并且是直链或支链的C1-C24-的化合物反应而制造水解稳定的铵腈烷基，C2-C24链烯基，取代或未取代的苄基，或C1-C4烷氧基C1-C4烷基基团是或其中，R <1>和R <2>与氮原子一起连接形成一个其形式环具有4至6个C原子，其可与C1-C5烷基，C1-C5烷氧基，C1-C5链烷酰基，苯基，氨基，铵基，氰基，cyanamino，氯或溴取代，并且除了该氮原子 NR <6>或一个基团R可含有<3> -NR <6>，而不是碳原子，一个或两个氧原子或氮原子，一个基团，其中R6是氢，C1-C5烷基，C2-C5链烯基，C2- C5炔基，苯基，C7-C9芳烷基，C5-C7环烷基，C1-C6链烷酰基，氰基甲基或氰基，R <4>和R <5>是氢，C1-C4烷基，C1-C4 一 lkenyl，C1-C4烷氧基C1-C4烷基，有苯基或C1-C3烷基苯基，优选氢，甲基或苯基，其中特别是R <4>是氢，当R <5>不为氢，和X 是阴离子，用烷烃磺酸在水在升高的温度下存在的碱金属或铵盐，石蜡磺酸盐，芳基磺酸盐，醇硫酸酯或Fettsäurealkylcarboxylats。

2. 发明申请

WO2006032512A3 LIQUID FLUORINE-CONTAINING COMPOSITIONS FOR TREATING THE SURFACES OF MINERAL AND NON-MINERAL SUBSTRATES 审中-公开
标题翻译： LIQUID FLUOR CONTAINING COMPOSITIONS FOR矿物的表面处理和非矿物表面
公开(公告)号：WO2006032512A3
公开(公告)日：2007-06-07
申请号：PCT/EP2005010287
申请日：2005-09-22
申请人： DEGUSSA , MAIER ALOIS , STEIDL NORBERT , SCHROERS MICHAEL , WEINELT FRANK , STAUDHAMMER MARITA
发明人： MAIER ALOIS , STEIDL NORBERT , SCHROERS MICHAEL , WEINELT FRANK , STAUDHAMMER MARITA
IPC分类号： C08G77/24 , C04B41/49 , C08G77/26 , C09D7/47 , C09D183/08 , C09D183/10
CPC分类号： C03C17/28 , C03C17/326 , C03C17/328 , C04B41/4961 , C08G77/24 , C08G77/26 , C09D183/08 , C09D183/10
摘要： The invention relates to liquid fluorine-containing compositions which have a fluorine content, based on the solid resin, of approximately 5 to 75 % by weight, for the permanent treatment of porous and non-porous substrates. The inventive compositions are obtainable by a) producing a perfluoroalkyl component (A), b) dissolving approximately 5 to 100 parts by weight of the perfluoroalkyl component (A) obtained in step a) prior, during or after reaction in approximately 0 to 100 parts by weight of a solvent component (K), c 1 ) optionally (partially) hydrolyzing or silanolizing the perfluoroalkyl component (A) obtained in steps a) or b) in the presence of approximately 0 to 50 parts by weight of an aminoalkylalkoxysilane component (E)(i) and/or aminosilane component (E)(ii) with approximately 1 to 50 parts by weight of water, c 2 ) quaternizing the aminofunctional adduct with approximately 5 to 50 parts by weight of an acid component (L) (direct neutralization), c 3 ) optionally removing the released alcohol and/or the solvent component (K), d 1 ) dissolving the reaction product obtained in step c) subsequently or simultaneously in approximately 50 to 1000 parts by weight of water and oligomerizing it, d 2 ) optionally removing the released alcohol and/or the solvent component (K), e) whereby optionally during or after steps a) and/or b) and/or c) and/or d) approximately 0 to 50 parts by weight of a formulation component (M) can be added in any manner and/or approximately 0 to 50 parts by weight of a functionalization component (N) are added and/or co-reacted. The invention makes available vapor-permeable coating systems for permanently treating the surfaces of mineral and non-mineral substrates with oil, water and dirt-repellent surface agents or for modifying them. The inventive liquid fluorine-containing compositions have substantially improved properties of application at the same or lower fluorine content as conventional products.
摘要翻译：它将与相关的大约5个氟的固体树脂含量为75重量％为多孔和无孔基材液体含氟组合物，其是可获得的连续表面处理时间由第一一制备）描述为全氟烷（A）成分 b）约5至100份（重量）从步骤a）之前，期间或按重量计的溶剂组分（K）的在约0至100份在反应后解决了，C _{升）如果合适的话，全氟烷组分（a）从步骤a）或（b）以按重量计的氨基的烷氧基硅烷组分（e的存在的大约0〜50份）i）和/或氨基硅烷组分（e）（ii）用约1至50重量份的水（部分地）水解或silanolisiert，C _{2 ），按重量的酸成分（L）的氨基官能加合物与约5至50份季铵化的（直接中和）中，c _{3 ）如果需要的话，释放的醇及/ O 的溶剂组分（K）被去除，D _{1 ）c）中随后或同时将反应产物从步骤溶解在水中约50至1000份（重量）和低聚ð_{2 ）被去除，e）任选地，期间或步骤a）和/或b）和/或c）和/或d）以任何所需方式，如果需要的释放的醇及/或溶剂成分后（K）约0至50重量份添加的制剂成分（M）和/或约0至50重量份的官能组分（N）中的每一个添加和/或实现。以这种方式，对于永久油，水和防污表面处理或矿物和非矿物表面改性水蒸汽可渗透的涂层系统是可访问的。此外，本发明的液体含氟组合物的产品相比，根据现有技术的具有用于相同和下部氟含量显著更好的性能特性。}}}}}

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