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1. 发明申请

WO2007137849A8 OLEFIN POLYMERISATION CATALYST 审中-公开
标题翻译： OLEFIN聚合催化剂
公开(公告)号：WO2007137849A8
公开(公告)日：2008-07-10
申请号：PCT/EP2007004828
申请日：2007-05-31
申请人： BOREALIS TECH OY , REKONEN PETRI , DENIFL PETER , LEINONEN TIMO
发明人： REKONEN PETRI , DENIFL PETER , LEINONEN TIMO
IPC分类号： C08F10/00 , C08F4/651 , C08F4/655
CPC分类号： C08F110/06 , C08F4/6557 , C08F4/651 , C08F2500/12 , C08F2500/18 , C08F2500/24
摘要： The present invention relates to particulate olefin polymerisation catalyst components comprising an alkaline earth metal, a compound of a transition metal and an electron donor, characterized in that the catalyst particle size distribution of the catalyst component is essentially monomodal and has a SPAN value below 1.2, where SPAN is defined as: (Particle diameter at 90 % cumulative size)-(Particle diameter at 10 % cumulative size) / (Particle diameter at 50 % cumulative size). The particulate olefin polymerisation catalyst components of the present invention are provided by a process which comprises preparing a solution of a complex of an alkaline earth metal and an electron donor by reacting a compound of said metal with said electron donor or a precursor thereof in an organic liquid reaction medium, reacting said complex in the solution form with a compound of a transition metal to produce a dispersion, wherein the dispersed phase predominantly contains the alkaline earth metal in said complex, and solidifying said dispersed phase to obtain said catalyst component, and is characterized in that a second organic liquid medium is added to the reactor after mixing the alkaline earth metal complex with the transition metal compound.
摘要翻译：本发明涉及包含碱土金属，过渡金属和电子给体的化合物的颗粒状烯烃聚合催化剂组分，其特征在于催化剂组分的催化剂粒度分布基本上是单峰的，SPAN值低于1.2， SPAN定义为：（颗粒直径为90％累积尺寸） - （10％累积尺寸下的粒径）/（50％累积尺寸下的粒径）。通过一种方法提供本发明的颗粒状烯烃聚合催化剂组分，该方法包括通过使所述金属的化合物与所述电子给体或其前体在有机物中反应制备碱土金属和电子给体的络合物的溶液液体反应介质，使所述溶液形式的复合物与过渡金属的化合物反应以产生分散体，其中分散相主要包含所述络合物中的碱土金属，并固化所述分散相以获得所述催化剂组分，并且是其特征在于，在将碱土金属络合物与过渡金属化合物混合后，将第二有机液体介质加入到反应器中。

2. 发明申请

WO2010127997A3 PREPARATION OF PRECIPITATED ZN PP CATALYSTS WITH INTERNAL PORE STRUCTURE USING NANOPARTICLES 审中-公开
标题翻译：使用纳米颗粒制备具有内部结构的ZN PP催化剂
公开(公告)号：WO2010127997A3
公开(公告)日：2010-12-29
申请号：PCT/EP2010055885
申请日：2010-04-30
申请人： BOREALIS AG , HAIKARAINEN ANSSI , DENIFL PETER , LEINONEN TIMO
发明人： HAIKARAINEN ANSSI , DENIFL PETER , LEINONEN TIMO
IPC分类号： C08F10/06 , C08F4/02 , C08F4/651 , C08F4/654
CPC分类号： C08F4/643 , C08F10/06 , C08F210/06 , C08L23/12 , Y10T428/2982 , C08F4/651 , C08F4/02 , C08F2/001 , C08F4/6548 , C08F4/6546 , C08F4/025 , C08L23/16 , C08F210/16 , C08F2500/05 , C08F2500/12 , C08F2500/18 , C08F2500/24
摘要： Process for the preparation of a catalyst being in the form of solid particles comprising the steps of °preparing a solution of a complex of a metal which is selected from one of the groups 1 to 3 of the periodic table (IUPAC) and an electron donor by reacting a compound of said metal with said electron donorin an organic liquid reaction medium; °adding to said solution solid material obtaining a suspension, said solid material -does not comprise catalytically active sites, -has a specific surface area below 500 m2/g, and -has a mean particle size below 200 nm; °combining said suspension at a temperature of at least 50°C with at least one transition metal compound resulting in a precipitation of said catalyst being in the form of a solid particle, wherein said transition metal compound is selected from one of the groups 4 to 10 of the periodic table (IUPAC) or a compound of actinide or lanthanide; and °optionally separating said catalyst; said catalyst being in the form of solid particles, which -have a specific surface area of less than 20 m2/g, and -contain said solid material.
摘要翻译：制备固体颗粒形式的催化剂的方法包括以下步骤：制备选自元素周期表（IUPAC）中1组至3族之一的金属络合物和电子给体通过使所述金属的化合物与所述电子给体的反应有机液体反应介质; 加入到所述溶液固体材料中得到悬浮液，所述固体材料不包含催化活性位点 - 具有低于500m 2 / g的比表面积，并且具有低于200nm的平均粒度; °将所述悬浮液在至少50℃的温度下与至少一种过渡金属化合物结合，导致所述催化剂以固体颗粒的形式沉淀，其中所述过渡金属化合物选自组4至 10的周期表（IUPAC）或锕系元素或镧系元素的化合物; 和任选地分离所述催化剂; 所述催化剂为具有小于20m 2 / g的比表面积的固体颗粒的形式，并且包含所述固体材料。

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