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1. 发明申请

WO1997002890A1 CLOTH OR CLOTH-LIKE PACKING WHICH IS SUBJECT TO LOW PRESSURE LOSSES AND HAS AN ORDERED STRUCTURE FOR USE IN MATERIAL-EXCHANGE COLUMNS AND RECTIFICATION METHOD USING SUCH PACKING 审中-公开
标题翻译：压降ARMS FABRIC保密，否则相似织物填料及使用传质柱和方法进行整改的有序结构中使用此包装
公开(公告)号：WO1997002890A1
公开(公告)日：1997-01-30
申请号：PCT/EP1996002851
申请日：1996-06-29
申请人： BASF AKTIENGESELLSCHAFT , BURST, Wolfram , HARTMANN, Horst , KAISER, Wulf , LAAS, Harald , GRAFEN, Paul , BOCKSTIEGEL, Bernhard , BALDENIUS, Kai-Uwe
发明人： BASF AKTIENGESELLSCHAFT
IPC分类号： B01J19/32
CPC分类号： B01J23/8913 , B01D3/008 , B01D3/141 , B01D3/146 , B01D3/16 , B01D53/864 , B01D53/8659 , B01D53/8662 , B01D53/8668 , B01D2255/102 , B01D2255/20715 , B01D2257/2062 , B01J19/32 , B01J23/63 , B01J23/6562 , B01J2219/3221 , B01J2219/3222 , B01J2219/32227 , B01J2219/32272 , B01J2219/32408 , B01J2219/32416 , B01J2219/326 , C07C17/38 , C07D311/72 , Y02P20/154 , Y10S62/906
摘要： The invention concerns packing elements which are subject to low pressure losses for use in material-exchange column assemblies, with the internal diameter of the column and a height of between 40 and 300 mm. These packing elements consist of dimensionally stable layers (2, 3) which have an ordered structure, contact one another and are made of cloth or cloth-like material. The packing elements are characterized in that: a) the contacting, deformed layers of cloth or cloth-like material, preferably metal cloth, are arranged such that they form a plurality of narrow flow ducts, preferably almost triangular, almost rectangular, square or almost equilateral hexagonal flow ducts, the angle of inclination (1) of the teeth of the individual cloth layers (2, 3) of the packing towards the column axis being only 0 to 25 DEG , preferably 3 to 14 DEG ; and b) in order to ensure the mechanical stability of the packing elements, wires or thin rods (4) are optionally mounted in a suitable arrangement between the cloth layers (2, 3), or the cloth layers (2, 3) are rigidly connected at some points of contact. The invention further concerns a process for obtaining pure substances from substance mixtures by rectification using the novel packing elements.
摘要翻译：对于所述柱的内径和40至300mm制成尺寸稳定的高度的传质塔的内部低压降填料元件有序结构和接触层（2，3）由布质材料或布状材料，其特征在于织物材料的一个）接触变形层或布状材料，优选地设置由金属网，从而形成多个窄流动通道，优选实质上三角形，几乎矩形的方形，或实际上正六边形流动通道，其中所述倾斜角（1）单独的布层的齿状物（2， 3）包装于柱轴线只有0至25℃，按重量计优选为3〜14°，并且b）连接，以保证填料元件的机械稳定性，如果需要，所述织物层（2之间，3）金属丝或细棒（4）在一个合适的布置的罪 d或织物层（2，3）在使用新的填料元件由整流获得来自物质混合物纯物质接触的一些点，以及方法牢固地连接。

2. 发明申请

WO1997002880A1 PROCESS FOR EXTRACTING PURE SUBSTANCES FROM MIXTURES OF HIGH-BOILING AIR AND/OR TEMPERATURE-SENSITIVE SUBSTANCES REQUIRING HIGH SEPARATIVE POWER BY RECTIFICATION IN A FINE VACUUM AND COLUMNS SUITABLE FOR THIS PROCESS 审中-公开
标题翻译：程序对获得纯物质混合物的高沸点空气和/或温度敏感性要求高切削性能BY整改罚款和真空此过程中适当的列物质
公开(公告)号：WO1997002880A1
公开(公告)日：1997-01-30
申请号：PCT/EP1996002852
申请日：1996-06-29
申请人： BASF AKTIENGESELLSCHAFT , HARTMANN, Horst , BURST, Wolfram , KAISER, Wulf , LAAS, Harald , GRAFEN, Paul , BOCKSTIEGEL, Bernhard , BALDENIUS, Kai-Uwe
发明人： BASF AKTIENGESELLSCHAFT
IPC分类号： B01D03/10
CPC分类号： B01D3/141 , B01D3/008 , B01D3/146 , B01D3/16 , B01J19/32 , B01J2219/3221 , B01J2219/3222 , B01J2219/32227 , B01J2219/32272 , B01J2219/32408 , B01J2219/32416 , B01J2219/326 , C07C17/38 , C07D311/72 , Y10S159/42 , Y10S261/72
摘要： The invention concerns a process for extracting pure substances from mixtures of high-boiling air and/or temperature-sensitive substances which require a high separative power by rectification in a fine vacuum in columns containing metal cloth packing with an ordered structure and using channel liquid separators with 500 or more draining points/m . The draining points are arranged at an angle of 90 DEG to the cloth layers of the packing elements (7, 8) located immediately below the distributors. Two or a plurality of the packing elements (7, 8) below the liquid separator (6) have only a slight height which practically ensures the exclusion of air. These packing elements are shaped such that, during rectification, no heat can be exchanged through the column wall. The invention also concerns the packing columns used for this process and the use of this process and this column for the distillative fine-purification of vitamin E acetate.
摘要翻译：一种用于在列使用信道的液体分配器具有500个或更多滴点/米<2>含金属布填料具有有序结构介质在真空下从高沸点空气和/或温度敏感的物质，其需要高分离效率的混合物获得纯的物质，通过精馏过程的90°到位于直接下方的歧管中的填料元件的布层的角度（7,8）被布置在其中2个或更多的填料元件（7,8）的液体分配器下面（6）只有具有小的高度几乎确保没有空气和被设计为使得在整流过程中没有热交换可以通过塔壁发生。该专利的主题也用于此过程填充柱和使用该方法的和列的维生素E乙酸酯蒸馏精细纯化。

3. 发明申请

WO1997028151A1 METHOD OF PRODUCING DL-'alpha'-TOCOPHEROL OR DL-'alpha'-TOCOPHERYL ACETATE 审中-公开
标题翻译：用于生产DL的α-生育酚或DL-α生育酚乙酸酯
公开(公告)号：WO1997028151A1
公开(公告)日：1997-08-07
申请号：PCT/EP1997000324
申请日：1997-01-24
申请人： BASF AKTIENGESELLSCHAFT , JAEDICKE, Hagen , GRAFEN, Paul , LAAS, Harald
发明人： BASF AKTIENGESELLSCHAFT
IPC分类号： C07D311/72
CPC分类号： C07D311/72
摘要： A method is disclosed of producing d1- alpha -tocopherol or d1- alpha -tocopheryl acetate by acid catalysed reaction of 2,3,5-trimethyl hydroquinone (TMH) with phytol or isophytol (IP) in a solvent at raised temperature and, where appropriate, subsequent esterification of the tocopherol thus obtained with acetic anhydride. The method is characterised in that the reaction is carried out in an optionally substituted cyclic five-ring carbonate such as 1,2-propylene carbonate, or in an optionally substituted five-ring lactone such as gamma -butyrolactone, as the solvent at temperatures of between 50 and 200 DEG C. The reaction works particularly well if, following the reaction of TMH and phytol or IP, the tocopherol which separates out as an upper phase as the reaction mixture cools and/or the reaction mixture is extracted using a suitable aliphatic hydrocarbon, the tocopherol is isolated by distillation from the extract, and the separated cyclic carbonate or gamma -lactone which can contain excess TMH and acidic catalyst is reused as solvent. In many cases, it has been shown to be advantageous to carry out the reaction of TMH with phytol or IP with removal of the water as azeotrope, using a suitable hydrocarbon and/or in the presence of a mixture of ortho-boric acid with oxalic acid, tartaric acid or citric acid, or alternatively in the presence of BF3 etherate as the acidic catalyst. Surprisingly, the five-ring carbonates and five-ring lactones prove to have sufficient stability under the reaction conditions and suitable solvent characteristics to permit the process to be carried out continuously.
摘要翻译：一种用于在升高的温度下在溶剂中通过2,3,5-三甲基对苯二酚（TMH）与叶绿醇或异植醇（IP）的酸催化反应制备DL-α-生育酚或DL-α-生育酚乙酸酯和，如果必要的话，随后的酯化过程用乙酸酐将所得的生育酚，其特征在于，所述反应在任选取代的环5-环碳酸酯进行，如1,2-丙二醇碳酸酯，或任选取代的5元环内酯，如γ-丁内酯的执行如在50的温度下，以200℃的溶剂该反应发生时，它被TMH和叶绿醇的反应之后，从提取物中分离或IP沉淀作为上层相的反应混合物生育酚的冷却和/或用合适的脂族烃中提取反应混合物，将生育酚分离通过蒸馏和分离的特别有利，也可有过量TMH和酸催化剂含有环状碳酸酯或重新用作溶剂的γ-内酯。在许多情况下，已被证明是有利的，如果TMH的反应用下除去反应与合适的烃的共沸物过程中形成的水的植醇或IP，和/或在原硼酸的一方面和草酸的混合物的存在下，酒石酸在另一方面或柠檬酸，或者如BF3醚合物的存在下，酸性催化剂进行。出人意料的是，5元环状碳酸酯，和5-元环内酯合适，即使是连续执行的方法的发现可能与反应条件下以及在对它们的溶液行为方面相对于它们的稳定性。

4. 发明申请

WO1993000326A1 OMEGA-3 POLYUNSATURATED FATTY-ACID DERIVATIVES, THEIR PREPARATION AND THEIR USE 审中-公开
标题翻译： OMEGA-3聚氧乙烯脂肪酸衍生物及其制备及其使用
公开(公告)号：WO1993000326A1
公开(公告)日：1993-01-07
申请号：PCT/EP1992001337
申请日：1992-06-13
申请人： BASF AKTIENGESELLSCHAFT , BOCKSTIEGEL, Bernhard , EMLING, Franz , JESSEL, Barbara , LECHTKEN, Peter , HOERCHER, Ulrich
发明人： BASF AKTIENGESELLSCHAFT
IPC分类号： C07C219/08
CPC分类号： C07C219/08 , C07C233/38
摘要： Described are compounds of the formula: R?1-X-Y-NR2R3¿, plus their salts with physiologically tolerable acids and their C¿1-2?-trialkylammonium salts. These compounds are suitable for use in the treatment of illnesses.

5. 发明申请

WO1993000325A1 ESTERS OF FATTY ACIDS WITH AMINO ALCOHOLS FOR USE IN THE TREATMENT OF ILLNESSES 审中-公开
标题翻译：含有氨基酸的脂肪酸用于治疗不良事件
公开(公告)号：WO1993000325A1
公开(公告)日：1993-01-07
申请号：PCT/EP1992001340
申请日：1992-06-13
申请人： BASF AKTIENGESELLSCHAFT , BOCKSTIEGEL, Bernhard , EMLING, Franz , KLING, Andreas , JESSEL, Barbara , JANSSEN, Bernd
发明人： BASF AKTIENGESELLSCHAFT
IPC分类号： C07C219/06
CPC分类号： C07C219/06
摘要： Described is the use, for the treatment of illnesses, of esters of fatty acids with amino alcohols of the formula I, in which R1 to R7 are as defined in the description.

6. 发明申请

WO1993019057A1 PROCESS FOR PRODUCING VITAMIN E 审中-公开
标题翻译：生产维生素E的方法
公开(公告)号：WO1993019057A1
公开(公告)日：1993-09-30
申请号：PCT/EP1993000498
申请日：1993-03-05
申请人： BASF AKTIENGESELLSCHAFT , GRAFEN, Paul , KIEFER, Hans , JAEDICKE, Hagen
发明人： BASF AKTIENGESELLSCHAFT
IPC分类号： C07D311/72
CPC分类号： C07D311/72
摘要： A process for producing dl-α-tocopherol or dl-α-tocophenyl acetate by acid-catalysed reaction of 2,3,5-trimethyl hydroquinone (TMH) with phytol or isophytol in a solvent at high temperature and, where appropriate, the subsequent esterification of the tocopherol obtained with acetanhydride. The process is characterized by the fact that the reaction takes place in the presence of a mixture of ortho-boric acid and certain aliphatic di- or tri-carboxylic acids, preferably in the presence of a mixture of ortho-boric and oxalic acids.

7. 发明申请

WO1996004238A1 PREPARATION OF O-(2-HYDROXYALKYL) OXIMES 审中-公开
标题翻译： O-（2-羟基烷基）氧化物的制备
公开(公告)号：WO1996004238A1
公开(公告)日：1996-02-15
申请号：PCT/EP1995003001
申请日：1995-07-28
申请人： BASF AKTIENGESELLSCHAFT , HARREUS, Albrecht , GÖTZ, Norbert , RANG, Harald , HARTMANN, Horst , MOHR, Jürgen , GEHRER, Eugen , LAUTH, Günter
发明人： BASF AKTIENGESELLSCHAFT
IPC分类号： C07C249/12
CPC分类号： C07C249/12
摘要： Preparation of O-(2-hydroxyalkyl) oximes of formula (I), (R and R are alkyl or R and R and the common C atom are 5-membered to 7-membered cycloalkyl; R is alkyl) by causing a ketoxime II to react with an olefin oxide III in the presence of a tertiary amine or with a carbonate IV in the presence of a catalyst. The end products (I) are suitable for use as intermediates for crop protection agents.
摘要翻译：式（I）的O-（2-羟基烷基）肟的制备，（R 1和R 2）是烷基或R 1和R 2，通式C原子是5-元至7- 通过在叔胺或碳酸酯IV的存在下，在催化剂存在下，使酮肟II与烯烃氧化物III反应，R 3为烷基。最终产品（I）适用于作物保护剂的中间体。

8. 发明申请

WO1995030648A1 PROCESS FOR PRODUCING ISOMER MIXTURES FROM O-PHENOXYALKYLHYDROXYL AMINES OR O-PHENOXYALKYLOXIMES 审中-公开
标题翻译：用于生产的异构体混合物ØPHENOXYALKYLHYDROXYLAMINEN或o phenoxyalkyloximes
公开(公告)号：WO1995030648A1
公开(公告)日：1995-11-16
申请号：PCT/EP1995001581
申请日：1995-04-26
申请人： BASF AKTIENGESELLSCHAFT , RANG, Harald , GÖTZ, Norbert , HARREUS, Albrecht , BORCHERS, Dirk , HARTMANN, Horst , MAYWALD, Volker , HEIMANN, Frank , BUSCHULTE, Thomas
发明人： BASF AKTIENGESELLSCHAFT
IPC分类号： C07C239/20
CPC分类号： C07C239/20 , C07C249/12 , C07C309/66
摘要： A process is disclosed for producing isomer mixtures from O-phenoxyalkylhydroxyl amines Ia: H2N-O-CH2-CH(R )-O-Ar and Ib: H2N-O-CH(R )-CH2-O-Ar (wherein R represents alkyl, Ar where appropriate a substituted phenyl) and the corresponding salt mixtures. This process involves the following steps: (a) an isomer mixture of O-(2-hydroxyethyl)-oximes (IIa) and (IIb) (in which R is an alkyl and R is an alkyl or alkoxy, or R and R together with the common C atom form a 5-7 member ring) is converted by reaction with a sulphonyl halogenide of formula (III): Hal-SO2-R (wherein R represents an organic group and Hal is a halogen) in the presence of a base to form the corresponding sulphonate mixture of (IVa) and (IVb); (b) this sulphonate mixture is reacted in the presence of a base with a phenol of formula (V): HO-Ar to produce a mixture of O-phenoxyalkyloximes of general formulae (VIa) and (VIb); (c) the mixture is hydrolysed in the presence of an acid and, if required, (d) the O-phenoxyalkylhydroxyl amines (Ia) and (Ib) are released from the resulting salts using a mineral base. The O-phenoxyalkylhydroxyl amines (Ia/Ib) and their precursors (VIa/VIb) are important intermediate products for plant protective agents and drugs.
摘要翻译：的异构体的混合物的制备O型Phenoxyalkylhydroxylaminen（Ia）中：H 2 N-O-CH2-CH（R <1>） - O-Ar和（Ib）中：H 2 N-O-CH（R <1>） - CH2-O-氩（R <1> =烷基; Ar为SUBST GEG苯基..）以及相应的盐的混合物，通过一）肟的异构体混合物O-（2-羟基乙基）（IIa）和（IIb）的（R <2> = 烷基，并且R <3> =烷基，烷氧基，或R <2>和R <3>使用通用C原子= 5-至7-元环）化合物与式（III）的磺酰卤一起：哈尔-SO 2 -R <4> <4>是且其中R是有机基团，Hal是卤素，在碱存在下的成的（IVa）的磺酸盐的相应的混合物和（IVb）中被转换，b）磺酸酯的混合物在碱的存在下与酚式（V）：HO-氩气，于通式（VIA）和（VIb）的O- phenoxyalkyloximes的混合物反应，c）中将该混合物水解在酸的存在下和，如果需要的话，d）从所述发生的盐，所述O- phenoxyalkylhydroxylamines（Ia）和（Ib）的装置矿工芭 Ë版本。 O型phenoxyalkylhydroxylamines（IA / IB）及其前体（VIA /ⅥB）是作物保护剂和药物的重要中间体。

9. 发明申请

WO1995015955A1 2,4-DIAMINOTHIAZOLES AND THEIR PRODUCTION 审中-公开
标题翻译： 2.4二氨基噻与生产
公开(公告)号：WO1995015955A1
公开(公告)日：1995-06-15
申请号：PCT/EP1994003981
申请日：1994-11-30
申请人： BASF AKTIENGESELLSCHAFT , HARTMANN, Horst , FLAIG, Ronald , BECKMANN, Stefan
发明人： BASF AKTIENGESELLSCHAFT
IPC分类号： C07D277/42
CPC分类号： C07D277/42
摘要： Diaminothiazoles of formula (I) in free form or in the form of their acid addition salts, in which the radicals R is C3-C10 dialkylamino, in which the alkyl groups may be interrupted by 1 to 3 oxygen atoms in the ether function, diphenyl amino or a 5 or 6-membered saturated heterocyclic radical, and process for producing 2,4 diaminothiazoles.
摘要翻译：式（I）的二氨基噻，以游离形式或它们的酸加成盐的形式，其中基团R <1> C3-C10二烷基氨基，其中所述烷基可以通过醚官能，二苯基氨基为1〜3个氧原子，或5元或6被中断意味着2,4- Diaminothiazolen的制备 - 元饱和杂环基团，以及方法。

10. 发明申请

WO2001051440A1 A PROCESS FOR THE PREPARATION OF SUBSTITUTED BENZOPHENONES 审中-公开
标题翻译：一种制备取代苯并噻吩的方法
公开(公告)号：WO2001051440A1
公开(公告)日：2001-07-19
申请号：PCT/EP2001000047
申请日：2001-01-04
申请人： BASF AKTIENGESELLSCHAFT
发明人： BASF AKTIENGESELLSCHAFT , KAMESWARAN, Venkataraman
IPC分类号： C07C45/46
CPC分类号： C07D295/185 , C07C45/008 , C07C45/46 , C07C201/12 , C07C49/84 , C07C205/45
摘要： There is provided a process for the preparation of a compound of formula (I) via the acylation of the appropriate substituted benzene substrate in the presence of graphite and FeC13. Compounds of formula (I) are useful as intermediates in the manufacture of agrichemical agents.
摘要翻译：提供了通过在石墨和FeC 13存在下酰化合适的取代苯底物制备式（I）化合物的方法。式（I）化合物可用作制造农药的中间体。

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