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1. 发明申请

WO2010083303A1 PROCESSES FOR PRODUCTION OF MACROMOLECULAR AMINE-PHENOLIC ANTIOXIDANT COMPOSITIONS CONTAINING LOW AMOUNTS OF NON-MACROMOLECULAR BYPRODUCTS 审中-公开
标题翻译：生产含有非分子式副产物的低分子量胺类酚类抗氧化剂组合物的方法
公开(公告)号：WO2010083303A1
公开(公告)日：2010-07-22
申请号：PCT/US2010/021035
申请日：2010-01-14
申请人： ALBEMARLE CORPORATION , SABAHI, Mahmood , COLONIUS, Neal, J. , ELNAGAR, Hassan, Y. , GATTO, Vincent, J. , JONES, Sarah, C. , KARSEBOOM, Steven, G.
发明人： SABAHI, Mahmood , COLONIUS, Neal, J. , ELNAGAR, Hassan, Y. , GATTO, Vincent, J. , JONES, Sarah, C. , KARSEBOOM, Steven, G.
IPC分类号： C07C213/08 , C07C213/10 , C07C215/74 , C08K5/13 , C10M165/00
CPC分类号： C07C215/74 , C07C213/08 , C07C213/10 , C08K5/18 , C10M149/14 , C10M159/12 , C10M2217/041 , C10N2230/10 , C10N2230/40 , C10N2240/10 , C10N2270/00
摘要： Processes are provided for producing macromolecular oxidation inhibitors that are almost free of low molecular weight components. Such processes comprise heating a combination comprising an aromatic amine, an acid catalyst, an alkylating agent, and a solvent to about 35°C to about 25O°C, thereby forming a reaction solution comprising one or more macromolecular amine-phenolic antioxidant solids and one or more non-macromolecular byproducts; combining at least the reaction solution and an antisolvent such that a precipitant comprising a substantial portion of the macromolecular amine-phenolic antioxidant solids precipitates out of the reaction solution, while a substantial portion of the non-macromolecular byproducts remain in the reaction solution; separating the precipitant from the reaction solution; and drying the precipitant to produce a MAPAC comprising less than about 1 wt.% non-macromolecular byproducts.
摘要翻译：提供了生产几乎不含低分子量组分的大分子氧化抑制剂的方法。这样的方法包括将包含芳族胺，酸催化剂，烷基化剂和溶剂的组合物加热至约35℃至约250℃，从而形成包含一种或多种高分子胺 - 酚类抗氧化剂固体和一种或更多的非大分子副产物; 将至少反应溶液和抗溶剂结合，使得包含大部分大分子胺 - 酚类抗氧化剂固体的沉淀剂从反应溶液中沉淀出来，而大部分非大分子副产物残留在反应溶液中; 将沉淀剂与反应溶液分离; 并干燥沉淀剂以产生包含小于约1重量％的非大分子副产物的MAPAC。

2. 发明申请

WO2010017030A1 OCTYLATED PHENYL-ALPHA-NAPHTHYLAMINE PRODUCT MIXTURES AND PRODUCTION OF SUCH MIXTURES HAVING A HIGH CONTENT OF OCTYLATED PHENYL-ALPHA-NAPHTHYLAMINE 审中-公开
标题翻译：月桂基邻苯二甲酰苯胺产品的混合物和这种具有高含量的苯乙烯 - 邻苯二甲酸甲酯的混合物的生产
公开(公告)号：WO2010017030A1
公开(公告)日：2010-02-11
申请号：PCT/US2009/051302
申请日：2009-07-21
申请人： ALBEMARLE CORPORATION , KARSEBOOM, Steven, G. , ELNAGAR, Hassan, Y. , GATTO, Vincent, J. , MOEHLE, William, E.
发明人： KARSEBOOM, Steven, G. , ELNAGAR, Hassan, Y. , GATTO, Vincent, J. , MOEHLE, William, E.
IPC分类号： C07C209/68 , C07C211/58 , C10M133/12
CPC分类号： C07C209/68 , C10L1/14 , C10L1/1832 , C10L1/19 , C10L1/223 , C10M133/12 , C10M169/04 , C10M2203/1045 , C10M2207/026 , C10M2207/289 , C10M2215/065 , C10N2220/021 , C10N2220/031 , C10N2220/032 , C10N2230/10 , C10N2230/66 , C07C211/58
摘要： Process technology is described for producing a reaction-derived product mixture containing a high yield of octylated phenyl-alpha-naphthylamine by catalytic alkylation of phenyl-alpha-naphthylamine with diisobutylene. New reaction-derived product mixtures are produced. Also provided are novel reaction-derived octylated phenyl-alpha-naphthylamine reaction product mixtures from which catalyst residues and excess olefin components have been removed. These reaction product mixtures are effective as antioxidants for various oxygen- sensitive substrate materials such as oils and lubricants. Also described are new octylated phenyl-alpha-naphthylamine product mixtures and their use in forming clear, stable, liquid antioxidant compositions for addition to a wide variety of substrates.
摘要翻译：描述了用于通过苯基-α-萘胺与二异丁烯的催化烷基化生产含有高产率的辛基化苯基-α-萘胺的反应衍生产物混合物的工艺技术。产生新的反应衍生的产物混合物。还提供了新的反应衍生的辛基化苯基-α-萘胺反应产物混合物，从中除去催化剂残余物和过量的烯烃组分。这些反应产物混合物作为各种氧敏感基材如油和润滑剂的抗氧化剂是有效的。还描述了新的辛基化苯基-α-萘胺产物混合物及其在形成透明，稳定的液体抗氧化剂组合物中用于添加到各种基材中的用途。

3. 发明申请

WO2010017029A2 LOW-DUST OCTYLATED PHENYL-ALPHA-NAPHTHYLAMINES AND FORMATION THEREOF 审中-公开
标题翻译：低UST ATED ATED L L HA HA OF OF OF OF OF OF OF OF OF OF OF
公开(公告)号：WO2010017029A2
公开(公告)日：2010-02-11
申请号：PCT/US2009/051297
申请日：2009-07-21
申请人： ALBERMARLE CORPORATION , ELNAGAR, Hassan, Y. , GATTO, Vincent, J. , KARSEBOOM, Steven, G.
发明人： ELNAGAR, Hassan, Y. , GATTO, Vincent, J. , KARSEBOOM, Steven, G.
IPC分类号： C07C211/58
CPC分类号： C07C211/58 , C09K15/22 , C10M133/12 , C10M2215/065 , C10N2220/082 , C10N2230/10 , C10N2270/00
摘要： Essentially dust-free particulate octylated phenyl-alpha-naphthylamine antioxidant and particle size enhancement methods for its formation are described. Such products avoid potential adverse health concerns and explosive hazards during handling and usage of the product. Also, methods for recovering high yields of particulate octylated phenyl-alpha- naphthylamine from crude octylated phenyl-alpha-naphthylamine product mixtures formed by catalytic alkylation of phenyl-alpha-naphthylamine with diisobutylene are described.
摘要翻译：描述了基本上无尘的颗粒状辛基化苯基-α-萘胺抗氧化剂和其形成的粒径增强方法。此类产品可避免在产品处理和使用过程中潜在的不利健康问题和爆炸危险。此外，描述了通过苯基-α-萘胺与二异丁烯的催化烷基化形成的粗制辛基化苯基-α-萘胺产物混合物来回收高产率的颗粒状辛基化苯基-α-萘胺的方法。

4. 发明申请

WO2009002761A1 A METHOD FOR MAKING N-2,3-DIBROMOPROPYL-4,5-DIBROMOHEXAHYDROPHTHALIMIDE 审中-公开
标题翻译：制备N-2,3-二溴丙基-4,5-二溴甲醛的方法
公开(公告)号：WO2009002761A1
公开(公告)日：2008-12-31
申请号：PCT/US2008/067188
申请日：2008-06-17
申请人： ALBEMARLE CORPORATION , ANDERSON, Steven, Alan , LIN, Ronny, W. , MUTTERER, Vincent, Luc , JAMESON, Christopher, Chad , KARSEBOOM, Steven, G. , HUSSAIN, Saadat , COLONIUS, Neal, James , MORICE, Jorge , MACK, Arthur, G. , MAXWELL, Kimberly, Ann
发明人： ANDERSON, Steven, Alan , LIN, Ronny, W. , MUTTERER, Vincent, Luc , JAMESON, Christopher, Chad , KARSEBOOM, Steven, G. , HUSSAIN, Saadat , COLONIUS, Neal, James , MORICE, Jorge , MACK, Arthur, G. , MAXWELL, Kimberly, Ann
IPC分类号： C07D209/48
CPC分类号： C07D209/48
摘要： The present invention relates to process technology suitable for producing, on a commercial scale, N-2,3-dibromopropyl-4,5-dibromohexahydrophthalimide formula (1).
摘要翻译：本发明涉及适合于商业规模生产N-2,3-二溴丙基-4,5-二溴六氢邻苯二甲酰亚胺化合物（1）的工艺技术。

5. 发明申请

WO2009035836A1 A METHOD FOR MAKING N-2,3-DIBROMOPROPYL-4-5-DIBROMOHEXAHYDROPHTHALIMIDE 审中-公开
标题翻译：制备N-2,3-DIBROMOPROLY-4-5-DIBROMOHEXAHYDROPHTHALIMIDE的方法
公开(公告)号：WO2009035836A1
公开(公告)日：2009-03-19
申请号：PCT/US2008/073793
申请日：2008-08-21
申请人： ALBEMARLE CORPORATION , MAXWELL, Kimberly, Ann , KARSEBOOM, Steven, G. , APLIN, Jeffrey, Todd , LIN, Ronny, W. , MACK, Arthur, G. , MORICE, Jorge , HUSSAIN, Saadat , ANDERSON, Steven, Alan , JAMESON, Christopher, Chad , COLONIUS, Neal, James
发明人： MAXWELL, Kimberly, Ann , KARSEBOOM, Steven, G. , APLIN, Jeffrey, Todd , LIN, Ronny, W. , MACK, Arthur, G. , MORICE, Jorge , HUSSAIN, Saadat , ANDERSON, Steven, Alan , JAMESON, Christopher, Chad , COLONIUS, Neal, James
IPC分类号： C07D209/48
CPC分类号： C07D209/48
摘要： The present invention relates to process technology suitable for producing, on a commercial scale, N-2,3-dibromopropyl-4,5-dibromohexahydrophthalimide.
摘要翻译：本发明涉及适用于工业规模生产N-2,3-二溴丙基-4,5-二溴六氢邻苯二甲酰亚胺的工艺技术。

6. 发明申请

WO2017023487A1 PROCESSES FOR SYNTHESIZING METHOXY ALKYLETHER QUATERNARY AMMONIUM BROMIDES 审中-公开
标题翻译：合成甲氧基甲基四氢氨基甲酸铵的方法
公开(公告)号：WO2017023487A1
公开(公告)日：2017-02-09
申请号：PCT/US2016/041480
申请日：2016-07-08
申请人： ALBEMARLE CORPORATION
发明人： GE, Zhongxin , KARSEBOOM, Steven, G.
IPC分类号： C07D233/56 , C07C213/00 , C07C213/08 , C07D295/088
CPC分类号： C07D295/088 , C07C213/00 , C07C213/08 , C07D233/56 , C07C217/08
摘要： Processes for synthesizing methoxy alkylether quaternary ammonium halides from methoxy alkyl tertiary amines and alkyl halides are provided.
摘要翻译：提供从甲氧基烷基叔胺和烷基卤化物合成甲氧基烷基醚季铵卤化物的方法。

7. 发明申请

WO2013184415A1 REMOVAL OF BROMINE FROM GASEOUS HYDROGEN BROMIDE 审中-公开
标题翻译：从气体溴化物中去除溴
公开(公告)号：WO2013184415A1
公开(公告)日：2013-12-12
申请号：PCT/US2013/042677
申请日：2013-05-24
申请人： ALBEMARLE CORPORATION
发明人： HARROD, William, B. , HARDEN, John, M. , HEEB, Rhett, P. , KARSEBOOM, Steven, G. , SHARP, Gary, L. , WILLIAMS, Robert, E.
IPC分类号： C01B7/09 , C07C17/093
CPC分类号： C01B7/093 , B01D53/68 , C07C9/14 , C07C17/12 , C07C17/14 , C07C22/04 , Y02P20/582
摘要： Processes of and systems for removing free bromine from gaseous anhydrous HBr contaminated with free bromine are described. In one type of process the gaseous contaminated HBr is fed into countercurrent contact with at least one liquid alkylaromatic hydrocarbon within a packed section of a column while maintaining the packed section under free radical bromination conditions so that one or more than one liquid a- bromoalkylaromatic compound is produced along with one mole of gaseous HBr per mole of a- bromoalkylaromatic compound produced. In another type of process the gaseous anhydrous HBr is fed into countercurrent contact through at least two scrubbers so that the gaseous anhydrous HBr is scrubbed substantially free of bromine by passage through these at least two scrubbers, each of which contains a different specified type of scrubbing liquid. In one embodiment the liquid alkylaromatic hydrocarbon comprises 1,2-diphenylethane.
摘要翻译：描述了用游离溴污染的无水无水HBr除去游离溴的方法和系统。在一种类型的方法中，将气体污染的HBr与塔的填充部分内的至少一种液体烷基芳族烃进行逆流接触，同时将填充部分保持在自由基溴化条件下，使得一种或多于一种液体α-溴烷基芳族化合物与每摩尔产生的α-溴烷基芳族化合物一摩尔气态HBr一起产生。在另一种类型的方法中，气态无水HBr通过至少两个洗涤器进料到逆流接触中，使得气态无水HBr通过这些至少两个洗涤器被洗涤，基本上不含溴，每个洗涤器含有不同的指定类型的洗涤液体。在一个实施方案中，液体烷基芳族烃包括1,2-二苯基乙烷。

8. 发明申请

WO2016061342A1 METHODS FOR QUANTIFYING ZINC CONTENT OF FLUIDS 审中-公开
标题翻译：定量流体中锌含量的方法
公开(公告)号：WO2016061342A1
公开(公告)日：2016-04-21
申请号：PCT/US2015/055724
申请日：2015-10-15
申请人： ALBEMARLE CORPORATION
发明人： NALEPA, Christopher, J. , KARSEBOOM, Steven, G. , VIATOR, Ross, M.
IPC分类号： C09K8/524 , G01N21/49
CPC分类号： C09K8/03 , G01N31/22
摘要： Methods are provided for assessing whether a particular salt-based fluid that contains zinc is suitable for an intended use, in that it contains less than a specified quantity of zinc.
摘要翻译：提供了用于评估含锌特定盐基流体是否适用于预期用途的方法，因为其含有少于特定量的锌。

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