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    • 1. 发明申请
    • METHOD AND A DEVICE FOR PREPARATION OF EXPANDED MICROSPHERES
    • 用于制备膨胀微球的方法和装置
    • WO2014198532A1
    • 2014-12-18
    • PCT/EP2014/060972
    • 2014-05-27
    • AKZO NOBEL CHEMICALS INTERNATIONAL B.V.
    • SVEDBERG, Lars-OlofAJDÉN, Per
    • C04B20/06
    • C08J9/16B01J8/087B01J2208/065C04B16/08C04B20/06C08J2203/22
    • The invention relates to a method and a device for the preparation of expanded thermoplastic microspheres from unexpanded thermally expandable thermoplastic microspheres comprising a thermoplastic polymer shell encapsulating a blowing agent. The method comprises: (a) feeding a slurry of such expandable thermoplastic microspheres in a liquid medium into a heating zone; (b) heating the slurry in the heating zone, without direct contact with any fluid heat transfer medium, so the expandable microspheres reach at least a temperature at which they would have started to expand at atmospheric pressure, and maintaining a pressure in the heating zone sufficiently high so the microspheres in the slurry do notfullyexpand; and, (c) withdrawing the slurry of expandable microspheres from the heating zone into a zone with a pressure sufficiently low for the microspheres to expand.
    • 本发明涉及一种从未膨胀的热可膨胀热塑性微球制备膨胀的热塑性微球的方法和装置,其包括封装发泡剂的热塑性聚合物壳。 该方法包括:(a)将这种可发性热塑性微球的浆液在液体介质中进料到加热区中; (b)加热加热区中的浆料,而不与任何流体传热介质直接接触,因此可膨胀微球体至少达到它们将在大气压下开始膨胀的温度,并保持加热区中的压力 足够高,使得浆料中的微球发生明显膨胀; 和(c)将可膨胀微球的浆料从加热区抽出到压力足够低以使微球膨胀的区域中。