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    • 2. 发明申请
    • METHOD FOR DETERMINING CONCENTRATIONS OF ADDITIVES IN ACID COPPER ELECTROCHEMICAL DEPOSITION BATHS
    • 用于确定酸性电化学沉积物中添加剂浓度的方法
    • WO2003106990A1
    • 2003-12-24
    • PCT/US2003/017568
    • 2003-06-04
    • ADVANCED TECHNOLOGY MATERIALS, INC.
    • HAN, JianwenETTERMAN, Ronni, M.ROBERTSON, Peter, M.BHELLA, RichardPRICE, David
    • G01N27/42
    • G01N27/4161G01N27/42
    • The present invention relates to a method for determining concentration of brightener and leveler contained in an aqueous acid metal electroplating solution, which minimizes the interference between the effects of the brightener and the effects of the leveler, by firstly determining the concentration of the brightener at a first set of measurement conditions, and secondly determining the concentration of the leveler at a second set of measurement conditions, provided that the first set of measurement conditions differ from the second set of measurement conditions on either (1) the rotation speed of a rotating disc electrode used for measuring plating potential of said aqueous acid metal electroplating solution, or (2) the electroplating duration at which the plating potential of said aqueous acid metal electroplating solution is measured, such that the rotation speed of the first set of measurement conditions is lower than the rotation speed of the second set of measurement conditions, and that the electroplating duration of the first set of measurement conditions is shorter than that of the second set of measurement conditions.
    • 本发明涉及一种用于测定含水酸性金属电镀溶液中的增白剂和矫正剂浓度的方法,其通过首先确定增白剂的浓度来最小化增白剂的作用和矫味剂的影响之间的干扰 第一组测量条件,其次在第二组测量条件下确定矫直机的浓度,条件是第一组测量条件与第二组测量条件不同,(1)旋转盘的旋转速度 用于测量所述含水酸性金属电镀溶液的电镀电位的电极,或(2)测量所述酸性金属电镀溶液的电镀电位的电镀持续时间,使得第一组测量条件的转速较低 比第二组测量条件的转速高, 并且第一组测量条件的电镀持续时间比第二组测量条件的电镀持续时间短。