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1. 发明申请

WO2009049168A1 PROCESS FOR MANUFACTURING CLEAN FLUOROPOLYMERS 审中-公开
标题翻译：制造清洁荧光体的方法
公开(公告)号：WO2009049168A1
公开(公告)日：2009-04-16
申请号：PCT/US2008/079529
申请日：2008-10-10
申请人： 3M INNOVATIVE PROPERTIES COMPANY , HINTZER, Klaus , LOCHHAAS, Kai H. , JÜRGENS, Michael , KASPAR, Harald , ZIPPLIES, Tilman C. , STREITER, André
发明人： HINTZER, Klaus , LOCHHAAS, Kai H. , JÜRGENS, Michael , KASPAR, Harald , ZIPPLIES, Tilman C. , STREITER, André
IPC分类号： C08F14/18 , C08F2/24 , C08L27/12
CPC分类号： C08K5/19 , C08F2/24 , C08F14/18 , C08F214/18 , C08K5/095 , C08F2/16 , C08L27/12
摘要： There is provided a fluoroelastomer characterized by containing one type or more types of fluorinated emulsifiers represented by the formula: F-(CF 2 )t -[O(CF 2 )n]m-O-(CHF)o-(CF 2 )p-X where m = 0 to 3; n = 1 to 5; o = 0 to 1; p = 1 to 3; t = 1 to 10; and where when t = 2 than o ≠ 0; and further where X is selected from a group consisting of a carboxyl acid group and a salt of a carboxylic acid group. A method for preparing fluoroelastomers by using such fluorinated emulsifiers in emulsion polymerization of fluoromonomers and articles containing such fluoroelastomers are also provided. A fluorinated elastomer dispersion including an aqueous mixture of a crosslinkable fluorinated elastomer and such fluorinated emulsifiers are also provided. The fluoroelastomers created with such fluorinated emulsifiers are essentially free of cations other than NH 4 + and H + and have a low glass transition temperature.
摘要翻译：提供一种含氟弹性体，其特征在于含有由式F-（CF 2）t - [O（CF 2）n] m O - （CHF）o - （CF 2）p X表示的一种或多种类型的氟化乳化剂，其中m = 0 到3; n = 1〜5; o = 0至1; p = 1〜3; t = 1〜10; 而当t = 2时， 0; 并且进一步其中X选自羧酸基团和羧酸基团的盐。还提供了通过使用这种氟化乳化剂在含氟单体和含有这些含氟弹性体的制品的乳液聚合中制备含氟弹性体的方法。还提供了包含可交联氟化弹性体和这种氟化乳化剂的水性混合物的含氟弹性体分散体。用这种氟化乳化剂生产的含氟弹性体基本上不含NH 4+和H +以外的阳离子，并具有低的玻璃化转变温度。

2. 发明申请

WO2009002617A1 PROCESS FOR REMOVING FLUORINATED COMPOUNDS FROM AN AQUEOUS PHASE ORIGINATING FROM THE PREPARATION OF FLUOROPOLYMERS 审中-公开
标题翻译：从制备氟聚合物的水相中去除荧光化合物的方法
公开(公告)号：WO2009002617A1
公开(公告)日：2008-12-31
申请号：PCT/US2008/062976
申请日：2008-05-08
申请人： 3M INNOVATIVE PROPERTIES COMPANY , HINTZER, Klaus , JÜRGENS, Michael , MAURER, Andreas R. , SCHWERTFEGER, Werner , ZIPPLIES, Tilman C. , LOCHHAAS, Kai H. , KASPAR, Harald
发明人： HINTZER, Klaus , JÜRGENS, Michael , MAURER, Andreas R. , SCHWERTFEGER, Werner , ZIPPLIES, Tilman C. , LOCHHAAS, Kai H. , KASPAR, Harald
IPC分类号： C01B25/237 , C01B25/16 , C08F14/18 , C08F214/18 , C08F8/00
CPC分类号： C08F214/18 , C08F6/16 , C08F6/22 , C08F14/18 , C08F114/18 , C08L27/12 , C08F2/10
摘要： A process of removing fluorinated compounds from an aqueous phase originating from the preparation of fluoropolymers said process comprising the use of polycationic polymers.
摘要翻译：从含氟聚合物的制备的水相中除去氟化化合物的方法，所述方法包括使用聚阳离子聚合物。

3. 发明申请

WO2017106119A1 AMINE-CONTAINING POLYMERS, DISPERSIONS THEREOF AND METHODS OF MAKING AND USING THE SAME 审中-公开
标题翻译：含胺聚合物，其分散体及其制备和使用方法
公开(公告)号：WO2017106119A1
公开(公告)日：2017-06-22
申请号：PCT/US2016/066253
申请日：2016-12-13
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： BULINSKI, Michael J. , COSTELLO, Michael G. , DUCHESNE, Denis , HINTZER, Klaus , LAMANNA, William M. , LOCHHAAS, Kai H. , PARENT, Michael J. , SMITH, Sean M.
IPC分类号： C08F14/18 , C08F8/32 , C08L27/12 , C08K5/01
CPC分类号： C08F8/32 , C08F214/22 , C08F214/26 , C08F226/06 , C09D127/16 , C09D127/18
摘要： Described herein is a polymer comprising: interpolymerized units of (i) a fluorinated terminal alkene monomer and (ii) a tertiary amine-containing fluorinated monomer comprising at least one of a vinyl amine, a substituted vinyl amine, an allyl amine, a substituted allyl amine, and combinations thereof; wherein the polymer can be amorphous or semi-crystalline with a melting point no greater than 325C. Dispersions thereof and methods of making and using the same are also described.
摘要翻译：本文描述了一种聚合物，其包含：（i）氟化末端烯烃单体和（ii）含叔胺的氟化单体的共聚单元，所述含叔胺氟化单体包含乙烯基胺，取代的乙烯基胺，烯丙基胺，取代的烯丙基胺及其组合; 其中聚合物可以是无定形或半结晶的，熔点不超过325℃。也描述了其分散体及其制备和使用方法。

4. 发明申请

WO2015088784A2 HIGHLY FLUORINATED ELASTOMERS 审中-公开
标题翻译：高度氟化弹性体
公开(公告)号：WO2015088784A2
公开(公告)日：2015-06-18
申请号：PCT/US2014/067564
申请日：2014-11-26
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： HINTZER, Klaus , JOCHUM, Florian D. , KASPAR, Harald , LOCHHAAS, Kai H. , ZIPPLIES, Tilman C.
IPC分类号： C08F214/26
CPC分类号： C08F214/262 , C08F214/26 , C08K5/06 , C08K5/095 , C08K5/14
摘要： Described herein is a peroxide curable, highly fluorinated elastomer derived from tetrafluoroethylene, a perfluoro ether monomer, and a compound selected from at least one of a highly fluorinated bisolefin ether and an iodine-containing perfluorinated ether.
摘要翻译：本文描述了由四氟乙烯，全氟醚单体和选自高度氟化的双烯烃醚和含碘的全氟化醚中的至少一种的化合物衍生的可过氧化物固化的高度氟化的弹性体。 / p>

5. 发明申请

WO2014099311A1 METHOD OF MAKING FLUOROPOLYMERS WITH A POLYIODIDE, COMPOSITIONS AND ARTICLES THEREOF 审中-公开
标题翻译：制备具有聚酰亚胺，组合物及其制品的氟聚合物的方法
公开(公告)号：WO2014099311A1
公开(公告)日：2014-06-26
申请号：PCT/US2013/072143
申请日：2013-11-27
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： HINTZER, Klaus , JOCHUM, Florian D. , KASPAR, Harald , LOCHHAAS, Kai H. , ZIPPLIES, Tilman C.
IPC分类号： C08F14/16 , C08F14/18 , C08F14/26 , C08F2/16 , C08F214/26
CPC分类号： C08F214/222 , C08F2/16 , C08F14/16 , C08F14/18 , C08F14/26 , C08F214/262
摘要： Described herein is a method of making a fluoropolymer and fluoropolymers thereof, wherein the method comprises: (a) providing an aqueous solution comprising a water soluble polyiodide salt of Formula (I): M +y [I-I-(I)J y - wherein M is a cation group having a valence y, y is an integer of at least 1 and n is an integer of at least 1; and (b) initiating polymerization of a monomer in the aqueous solution, wherein the monomer is a fluorinated monomer.
摘要翻译：本文描述了制备氟聚合物及其含氟聚合物的方法，其中所述方法包括：（a）提供包含式（I）的水溶性多碘化物盐的水溶液：M + y [II-（I）Jy - 其中M 是具有y价的阳离子基团，y是至少为1的整数，n是至少为1的整数; 和（b）引发单体在水溶液中的聚合，其中单体是氟化单体。

6. 发明申请

WO2007140091A1 COATING COMPOSITION 审中-公开
标题翻译：涂料组合物
公开(公告)号：WO2007140091A1
公开(公告)日：2007-12-06
申请号：PCT/US2007/068528
申请日：2007-05-09
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： HINTZER, Klaus , JÜRGENS, Michael , KASPAR, Harald , KOENIGSMANN, Herbert , LOCHHAAS, Kai H. , MAURER, Andreas R. , SCHWERTFEGER, Werner , ZIPPLIES, Tilman C. , MAYER, Ludwig , DADALAS, Michael C. , MOORE, George G.I. , SCHULZ, Jay F. , FLYNN, Richard M.
IPC分类号： C09D127/12 , C09D7/12 , C08L27/12 , C08K3/00 , C07C59/135 , C08F2/00
CPC分类号： C09D127/18 , C08K5/06 , C08K5/09 , C08L27/12 , C08L71/02 , C08L2205/02 , C08L2205/03 , C08L2205/035 , C08L2666/02 , C08L2666/14
摘要： A coating composition having (i) an aqueous dispersion of fluoropolymer particles comprising a non-melt processible polymer of tetrafluoroethylene, (ii) a fluorinated surfactant, (iii) a non-ionic non-fluorinated surfactant and (iv) a non-fluorinated polymer, wherein the fluorinated surfactant is selected from fluorinated carboxylic acids or salts thereof of the general formula (I): wherein L represents a linear partially or fully fluorinated alkylene group or an aliphatic hydrocarbon group, R f represents a linear partially or fully fluorinated aliphatic group or a linear partially or fully fluorinated aliphatic group interrupted with one or more oxygen atoms, X i+ represents a cation having the valence i and i is 1, 2 or 3.
摘要翻译：一种涂料组合物，其具有（i）含氟聚合物颗粒的水性分散体，其包含四氟乙烯的不可熔融加工聚合物，（ii）氟化表面活性剂，（iii）非离子非氟化表面活性剂和（iv）非氟化聚合物其中氟化表面活性剂选自通式（I）的氟化羧酸或其盐：其中L表示直链部分或完全氟化的亚烷基或脂族烃基，R f表示线性部分或完全氟化的脂族基团或被一个或多个氧原子间隔的线性部分或完全氟化的脂族基团，X i表示具有i价和i为1,2或3的阳离子。

7. 发明申请

WO2005052041A1 BROMINE, CHLORINE OR IODINE FUNCTIONAL POLYMER ELECTROLYTES CROSSLINKED BY E-BEAM 审中-公开
标题翻译：电子束交联的溴，氯或碘功能聚合物电解质
公开(公告)号：WO2005052041A1
公开(公告)日：2005-06-09
申请号：PCT/US2004/034835
申请日：2004-10-20
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： YANDRASITS, Michael A., , HAMROCK, Steven J., , HINTZER, Klaus , THALER, Arne , FUKUSHI, Tatsuo , JING, Naiyong , LOCHHAAS, Kai H.
IPC分类号： C08J5/22
CPC分类号： C08J5/225 , B01D67/009 , B01D71/32 , B01D71/82 , C08F114/26 , C08J3/28 , C08J2327/18 , H01M8/1023 , H01M8/1039 , H01M8/1072 , H01M8/1088 , H01M2300/0082 , Y02P70/56
摘要： A method is provided for making a crosslinked polymer electrolyte, typically in the form of a membrane for use as a polymer electrolyte membrane in an electrolytic cell such as a fuel cell, as well as the polymer so made, the method comprising application of electron beam radiation to a highly fluorinated fluoropolymer comprising: a backbone derived in part from tetrafluoro-ethylene monomer, first pendent groups which include a group according to the formula -SO 2 X, where X is F, C1, Br, OH or -O - M + , where M + is a monovalent cation, and second pendent groups which include Br, C1 or I. Typically, the membrane has a thickness of 90 microns or less, more typically 60 or less, and most typically 30 microns or less.
摘要翻译：提供了一种用于制造交联聚合物电解质的方法，该电解质通常是在诸如燃料电池的电解槽中用作聚合物电解质膜的膜形式，以及如此制备的聚合物，该方法包括施加电子束辐射到高度氟化的含氟聚合物，其包含：部分由四氟乙烯单体衍生的主链，第一侧基，其包括根据式-SO 2 X的基团，其中X是F，Cl，Br，OH或-O M 其中M +是一价阳离子，第二侧基包括Br，Cl或I.通常，膜的厚度为90微米或更小，更通常为60或更小，最通常为30微米或更少。

8. 发明申请

WO2017053563A1 METHOD OF MAKING A COPOLYMER OF TETRAFLUOROETHYLENE HAVING SULFONYL PENDANT GROUPS 审中-公开
标题翻译：制备具有亚磺酸基团的四氟乙烯共聚物的方法
公开(公告)号：WO2017053563A1
公开(公告)日：2017-03-30
申请号：PCT/US2016/053104
申请日：2016-09-22
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： DAHLKE, Gregg D. , DUCHESNE, Denis , HINTZER, Klaus , HIRSCHBERG, Markus , LOCHHAAS, Kai H. , THALER, Arne , ZIPPLIES, Tilman C.
IPC分类号： C08F216/14 , C08F214/26 , H01M8/10 , H01M8/1032 , H01M8/1039
CPC分类号： C08F214/26 , C08F216/14 , H01M8/1039 , Y02P70/56
摘要： A method of making a copolymer is disclosed. The method includes copolymerizing components including tetrafluoroethylene and a compound represented by formula CF 2 =CF-O-(CF 2 ) a -SO 2 X, wherein "a" is a number from 1 to 4, and X is -NZH, -NZ-SO 2 -(CF 2 ) 1-6 -SO 2 X', or -OZ, wherein Z is independently a hydrogen, an alkali metal cation, or a quaternary ammonium cation, and wherein X' is independently -NZH or -OZ. The components include at least 60 mole % of tetrafluoroethylene based on the total amount of components. A copolymer prepared by the method is also provided. A method of making a membrane using the copolymer is also provided. The present disclosure also provides a polymer electrolyte membrane that includes a copolymer made by the method and a membrane electrode assembly that includes such a polymer electrolyte membrane.
摘要翻译：公开了制备共聚物的方法。该方法包括使包含四氟乙烯和式CF2 = CF-O-（CF2）a-SO2X表示的化合物的组分共聚合，其中“a”为1至4的数，X为-NZH，-NZ-SO2-（ CF 2）1-6-SO 2 X'或-OZ，其中Z独立地是氢，碱金属阳离子或季铵阳离子，并且其中X'独立地是-NZH或-OZ。基于组分的总量，组分包括至少60摩尔％的四氟乙烯。还提供了通过该方法制备的共聚物。还提供了使用共聚物制造膜的方法。本公开还提供了一种聚合物电解质膜，其包括通过该方法制备的共聚物和包括这种聚合物电解质膜的膜电极组件。

9. 发明申请

WO2016028582A1 FLUOROTHERMOPLASTIC POLYMER COMPOSITIONS 审中-公开
标题翻译：光热塑性聚合物组合物
公开(公告)号：WO2016028582A1
公开(公告)日：2016-02-25
申请号：PCT/US2015/044964
申请日：2015-08-13
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： CHEN, Lisa P. , HINTZER, Klaus , KASPAR, Harald , LOCHHAAS, Kai H. , MUGGLI, Mark W. , SCHROOTEN, Jens , SOHLO, Allen M. , TRAUNSPURGER, Helmut , WEILANDT, Karl D. , ZIPPLIES, Tilman C.
IPC分类号： C08L27/18 , C08L27/16 , C08L27/20
CPC分类号： C08L27/18 , B32B1/08 , B32B7/12 , B32B25/08 , B32B25/12 , B32B25/14 , B32B27/18 , B32B27/20 , B32B27/304 , B32B27/322 , B32B2264/0242 , B32B2264/0257 , B32B2264/102 , B32B2270/00 , B32B2307/50 , B32B2307/7265 , B32B2597/00 , B32B2605/08 , C08F259/08 , C08L2205/025
摘要： Described herein is a composition comprising (i) a hydrofluorothermoplastic polymer, wherein the hydrofluorothermoplastic polymer is derived from: (a) 50-85 mol% tetrafluoroethene; (b) 2-15 mol% hexafluoropropene; (c) 10-35 mol% vinylidene fluoride; and (d) 0.1 to 5 mol% of a bromine-containing monomer; and (ii) a perhalogenated thermoplastic polymer. Such compositions can be used in multilayer constructions in, for example, fuel hose applications.
摘要翻译：本文描述的是一种组合物，其包含（i）氢氟发热聚合物，其中所述氢氟热塑性聚合物衍生自：（a）50-85mol％四氟乙烯; （b）2-15摩尔％六氟丙烯; （c）10-35mol％偏二氟乙烯; 和（d）0.1〜5摩尔％的含溴单体; 和（ii）全卤代热塑性聚合物。这种组合物可用于例如燃料软管应用中的多层结构中。

10. 发明申请

WO2015134435A1 HIGHLY FLUORINATED ELASTOMERS 审中-公开
标题翻译：高荧光弹性体
公开(公告)号：WO2015134435A1
公开(公告)日：2015-09-11
申请号：PCT/US2015/018402
申请日：2015-03-03
申请人： 3M INNOVATIVE PROPERTIES COMPANY
发明人： HINTZER, Klaus , JOCHUM, Florian D. , KASPAR, Harald , LOCHHAAS, Kai H. , ZIPPLIES, Tilman C.
IPC分类号： C08L15/02 , C08L23/28
CPC分类号： C08G65/007 , C08F214/262 , C08K5/06 , C08L23/28
摘要： Described herein is a peroxide curable, highly fluorinated elastomer derived from (a) a fluorinated di-iodo ether compound of the following formula I: R f -CF(I)- (CX 2 ) n -(CX 2 CXR) m -O-R"f-O k -(CXR'CX 2 ) p -(CX 2 ) q -CF(I)-R' f wherein X is independently selected from F, H, and Cl; R f and R' f are independently selected from F and a monovalent perfluoroalkane having 1-3 carbons; R is F, or a partially fluorinated or perfluorinated alkane comprising 1-3 carbons; R" f is a divalent fluoroalkylene having 1-5 carbons or a divalent fluorinated alkylene ether having 1-8 carbons and at least one ether linkage; k is 0 or 1; and n, m, and p are independently selected from an integer from 0-5, with the proviso that when k is 0, n + m is at least 1 and p + q is at least 1; and (b) a fluorinated monomer.
摘要翻译：本文描述了一种过氧化物可固化的高度氟化的弹性体，其衍生自（a）下式I的氟化二碘醚化合物：Rf-CF（I） - （CX2）n-（CX2CXR）mOR“f-Ok-（ CXR'CX2）p-（CX2）q-CF（I）-R'f其中X独立地选自F，H和Cl; Rf和R'f独立地选自F和具有1-3的单价全氟烷烃碳; R为F，或含有1-3个碳的部分氟化或全氟化烷烃; R“f为具有1-5个碳原子的二价氟代亚烷基或具有1-8个碳原子和至少一个醚键的二价氟化亚烷基醚; k为0或1; 并且n，m和p独立地选自0-5的整数，条件是当k为0时，n + m为至少1，p + q为至少1; 和（b）氟化单体。

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