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    • 10. 发明申请
    • COMPOUND, ADHESIVE ARTICLE, AND METHODS OF MAKING THE SAME
    • 复合物,粘合剂制品及其制备方法
    • WO2018005285A1
    • 2018-01-04
    • PCT/US2017/039032
    • 2017-06-23
    • 3M INNOVATIVE PROPERTIES COMPANY
    • APPEANING, Maria A.BOULOS, Marie A.KINNING, David J.TEVEROVSKIY, GeorgiyJARIWALA, Chetan P.STEINER, Michael L.VANG, Sai
    • C09J7/02C09D183/04
    • A method of making an adhesive article comprises three steps. First, a backing is provided having first and second opposed major surfaces with respective first and second silicone release layers disposed thereon. The second silicone release layer further comprises a compound represented by the formula: R 1 represents a divalent hydrocarbon radical having from 2 to 40 carbon atoms or covalent bond. R 2 represents a monovalent or divalent poly(dimethylsiloxane) moiety. X represents -NH- or a covalent bond. R f represents a perfluorinated group having from 3 to 5 carbon atoms. y is 1 or 2. Second, an adhesive layer is disposed onto the first silicone release layer. Third, the adhesive layer is exposed to E-beam radiation within a process chamber containing oxygen to provide a crosslinked adhesive layer. An adhesive article made by the method and the compound are also disclosed.
    • 制造粘合制品的方法包括三个步骤。 首先,提供具有第一和第二相对主表面的背衬,其上设置有相应的第一和第二有机硅释放层。 第二有机硅剥离层还包含由下式表示的化合物:R 1表示具有2至40个碳原子或共价键的二价烃基。 R 2表示一价或二价聚(二甲基硅氧烷)部分。 X代表-NH-或共价键。 R f表示具有3至5个碳原子的全氟化基团。 y是1或2.第二,将粘合剂层设置在第一有机硅剥离层上。 第三,将粘合剂层暴露于含氧的处理室内的电子束辐射,以提供交联的粘合剂层。 还公开了由该方法和化合物制成的粘合剂制品。