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1. 发明申请

WO2011050131A3 METHODS OF PREPARING FLUORINATED CARBOXYLIC ACIDS AND THEIR SALTS 审中-公开
标题翻译：制备氟化羧酸及其盐的方法
公开(公告)号：WO2011050131A3
公开(公告)日：2011-08-25
申请号：PCT/US2010053480
申请日：2010-10-21
申请人： 3M INNOVATIVE PROPERTIES CO , HINTZER KLAUS , VOGEL DENNIS E , GUERRA MIGUEL A , IGNATOWSKA JOLANTA , ROESCHENTHALER GERD-VOLKER , SHYSHKOV OLEG , VOGEL KIM M , ZIPPLIES TILMAN C
发明人： HINTZER KLAUS , VOGEL DENNIS E , GUERRA MIGUEL A , IGNATOWSKA JOLANTA , ROESCHENTHALER GERD-VOLKER , SHYSHKOV OLEG , VOGEL KIM M , ZIPPLIES TILMAN C
IPC分类号： C07C51/27 , C07C53/18 , C07C53/21 , C07C59/125 , C07C59/135
CPC分类号： C07C51/27 , C07C53/21 , C07C59/135
摘要： A method for preparing fluorinated carboxylic acids and theirs salts is described comprising subjecting a fluorinated alcohol of the general formula (A): A-CH2-OH to at least one first and at least one second oxidizing agent to produce a highly fluorinated carboxylic acid or their salts of the general formula (B): A-COO M+, wherein M+ represents a cation and wherein A in formulas (A) and (B) is the same and A represents the residue: Rf-[0]p-CX"Y"-[0]m-CX'Y'-[0]n-CXY- wherein Rf represents a fluorinated alkyl residue which may or may not contain one or more catenary oxygen atoms, p, m and n are independently from each other either 1 or O, X, X', X", Y, Y' and Y" are independently from each other H, F, CF3, or C2F5 with the proviso that not all of X, X', X", Y, Y' and Y' ' are H; or A represents the residue: R-CFX- wherein X and R are independently selected from a hydrogen, a halogen, or an alkyl, alkenyl, cycloalkyl, or aryl residue, which may or may not contain one or more fluorine atoms and which may or may not contain one or more catenary oxygen atoms; wherein said at least one first oxidizing agent is a compound that can be converted, by action of the second oxidizing agent, into a reactive species capable of oxidizing the fluorinated alcohol.
摘要翻译：描述了制备氟化羧酸及其盐的方法，包括使通式（A）的氟化醇：A-CH 2 -OH经历至少一种第一和至少一种第二氧化剂以产生高度氟化的羧酸或它们的通式（B）的盐：A-COO M +，其中M +表示阳离子，并且其中式（A）和（B）中的A相同且A表示残基：Rf- [O] p-CX“ 其中Rf表示可以含有或不含有一个或多个悬链氧原子的氟化烷基，p，m和n彼此独立地为 X'，X'，Y'，Y'和Y“各自独立地为H，F，CF 3或C 2 F 5，条件是不是所有的X，X'，X” Y'和Y“是H;或者A代表残基：R-CFX-，其中X和R独立地选自氢，卤素或烷基，烯基，环烷基或芳基残基，其可以或不可以含有一个或多个氟原子 ms并且可能包含或不包含一个或多个悬链氧原子; 其中所述至少一种第一氧化剂是能够通过所述第二氧化剂的作用转化为能够氧化所述氟化醇的反应性物质的化合物。

2. 发明申请

WO2010009191A3 FLUORINATED ETHER COMPOUNDS AND METHODS OF USING THE SAME 审中-公开
标题翻译：氟化醚化合物及其使用方法
公开(公告)号：WO2010009191A3
公开(公告)日：2010-07-22
申请号：PCT/US2009050627
申请日：2009-07-15
申请人： 3M INNOVATIVE PROPERTIES CO , DAMS RUDOLF J , TERRAZAS MICHAEL S , HINTZER KLAUS , QIU ZAI-MING , GUERRA MIGUEL A , MAURER ANDREAS R , KASPAR HARALD , LOCHHAAS KAI H , JUERGENS MICHAEL , ZIPPLIES TILMAN C , SCHWERTFEGER WERNER
发明人： DAMS RUDOLF J , TERRAZAS MICHAEL S , HINTZER KLAUS , QIU ZAI-MING , GUERRA MIGUEL A , MAURER ANDREAS R , KASPAR HARALD , LOCHHAAS KAI H , JUERGENS MICHAEL , ZIPPLIES TILMAN C , SCHWERTFEGER WERNER
IPC分类号： C07C235/10 , C07C217/28 , C07C219/06
CPC分类号： C07C235/10 , C07C69/708 , C07C211/11 , C07C211/14 , C07C291/04 , C07C309/14 , C07F9/091 , C07F9/3808 , C08G65/007
摘要： Compounds represented by formula (Rf-Q-X)s-Z. Each Rf is independently a partially fluorinated or fully fluorinated group selected from Rfa-(O)r-CHF-(CF2)n-; [Rfb-(O)t-C(L)H-CF2-O]m-W-; CF3CFH-O-(CF2)p-; CF3-(O-CF2)z-; and CF3-O-(CF2)3-O-CF2-. Methods of reducing surface tension of a liquid, making foams, and treating a surface using the compounds are also disclosed.
摘要翻译：由式（Rf-Q-X）s-Z表示的化合物。每个Rf独立地为选自Rfa-（O）r-CHF-（CF 2）n - 的部分氟化或完全氟化的基团; [Rfb-（O）T-C（L）H-CF 2 -O] M-W-; CF 3 CFH-O-（CF 2）p - ; CF 3 - （O-CF 2）z - ; 和CF 3 -O-（CF 2）3 -O-CF 2 - 。还公开了降低液体表面张力，制造泡沫和使用该化合物处理表面的方法。

3. 发明申请

WO2010021962A2 AZIDE-CONTAINING FLUOROPOLYMERS AND THEIR PREPARATION 审中-公开
标题翻译：含AZIO的氟聚合物及其制备
公开(公告)号：WO2010021962A2
公开(公告)日：2010-02-25
申请号：PCT/US2009053982
申请日：2009-08-17
申请人： 3M INNOVATIVE PROPERTIES CO , HINTZER KLAUS , JUERGENS MICHAEL , KASPAR HARALD , LOCHHAAS KAI HELMUT , SHYSHKOV OLEG , STREITER ANDRE , ZIPPLIES TILMAN C , BEUERMANN SABINE , IMRAN-ULHAQ MUHAMMAD
发明人： HINTZER KLAUS , JUERGENS MICHAEL , KASPAR HARALD , LOCHHAAS KAI HELMUT , SHYSHKOV OLEG , STREITER ANDRE , ZIPPLIES TILMAN C , BEUERMANN SABINE , IMRAN-ULHAQ MUHAMMAD
IPC分类号： C08F8/30 , C08F2/18 , C08F2/22 , C08F14/18 , C08F14/20 , C08F14/22 , C08F214/18 , C08F214/20 , C08F214/22
CPC分类号： C08F8/30 , C08F4/00 , C08F4/02 , C08F114/20 , C08F114/22 , C08G73/00 , Y10T428/139 , Y10T428/1397 , C08F14/18
摘要： Fluoropolymers containing one or more azide group wherein the azide group is not a sulfonyl-azide group and processes of preparing them.
摘要翻译：含有一个或多个叠氮基的含氟聚合物及其制备方法，其中叠氮基不是磺酰基叠氮基。

4. 发明申请

WO2010009296A2 FLUORINATED ETHER SILANES AND METHODS OF USING THE SAME 审中-公开
标题翻译：氟化硅醚及其使用方法
公开(公告)号：WO2010009296A2
公开(公告)日：2010-01-21
申请号：PCT/US2009050810
申请日：2009-07-16
申请人： 3M INNOVATIVE PROPERTIES CO , MAURER ANDREAS R , KASPAR HARALD , LOCHHAAS KAI HELMUT , JUERGENS MICHAEL , TERRAZAS MICHAEL S , GUERRA MIGUEL A , DAMS RUDOLF J , ZIPPLIES TILMAN C , QIU ZAI-MING , HINTZER KLAUS , SCHWERTFEGER WERNER
发明人： MAURER ANDREAS R , KASPAR HARALD , LOCHHAAS KAI HELMUT , JUERGENS MICHAEL , TERRAZAS MICHAEL S , GUERRA MIGUEL A , DAMS RUDOLF J , ZIPPLIES TILMAN C , QIU ZAI-MING , HINTZER KLAUS , SCHWERTFEGER WERNER
IPC分类号： C07F7/18 , B05D3/02
CPC分类号： C07F7/1836
摘要： Fluorinated compounds represented by formula Rf-Q-X-[Si(R)f(R1)3-f]g. Each Rf is independently a partially fluorinated or fully fluorinated group selected from Rfa-(O)r-CHF-(CF2)n-; [Rfb-(O)t-C(L)H-CF2-O]m-W-; CF3CFH-O-(CF2)p-; CF3-(O-CF2)z-; and CF3-O-(CF2)3-O-CF2-. Methods of treating a surface or a hydrocarbon-bearing formation using the fluorinated compounds and treated articles and treated hydrocarbon-bearing formations are also disclosed.
摘要翻译：由式Rf-Q-X- [Si（R）f（R1）3-f] g表示的氟化化合物。每个Rf独立地为选自Rfa-（O）r-CHF-（CF 2）n - 的部分氟化或完全氟化的基团; [Rfb-（O）T-C（L）H-CF 2 -O] M-W-; CF 3 CFH-O-（CF 2）p - ; CF 3 - （O-CF 2）z - ; 和CF 3 -O-（CF 2）3 -O-CF 2 - 。还公开了使用氟化化合物和经处理的制品和经处理的含烃地层处理表面或含烃地层的方法。

5. 发明申请

WO2011162971A3 POLYMERIZABLE COMPOSITIONS FREE OF ORGANIC EMULSIFIER AND POLYMERS AND METHODS OF MAKING THEREOF 审中-公开
标题翻译：无机有机聚合物和聚合物的可聚合组合物及其制备方法
公开(公告)号：WO2011162971A3
公开(公告)日：2012-04-12
申请号：PCT/US2011039772
申请日：2011-06-09
申请人： 3M INNOVATIVE PROPERTIES CO , BARAN JIMMIE R JR , FANSLER DUANE D , HINTZER KLAUS , HUNT WILLIAM J , KASPAR HARALD , ZIPPLIES TILMAN C
发明人： BARAN JIMMIE R JR , FANSLER DUANE D , HINTZER KLAUS , HUNT WILLIAM J , KASPAR HARALD , ZIPPLIES TILMAN C
IPC分类号： C08K3/36 , C08F2/22 , C08J5/18 , C08L25/04 , C08L27/12
CPC分类号： C08F2/10 , C08F2/20 , C08F2/22 , C08K3/36 , C08K2201/011
摘要： Described herein is a polymerizable composition substantially free of an organic emulsifier, methods of making, and articles thereof. The polymerizable composition comprises: a continuous phase; a polymerizable monomer; an initiator; and inorganic nanoparticles, wherein the inorganic nanoparticles are substantially free of groups that will copolymerize with the polymerizable monomer.
摘要翻译：本文描述的是基本上不含有机乳化剂，制备方法及其制品的可聚合组合物。可聚合组合物包括：连续相; 可聚合单体; 发起者和无机纳米颗粒，其中无机纳米颗粒基本上不含将与可聚合单体共聚的基团。

6. 发明申请

WO2010039820A2 PROCESS OF MAKING FLUOROOLEFINS BY THERMAL DECOMPOSITION OF FLUORINATED MATERIALS 审中-公开
标题翻译：氟化物热分解制备氟烯烃的方法
公开(公告)号：WO2010039820A2
公开(公告)日：2010-04-08
申请号：PCT/US2009059011
申请日：2009-09-30
申请人： 3M INNOVATIVE PROPERTIES CO , HINTZER KLAUS , KAEMPF GUNTHER J , KOLBECK THOMAS , ZIPPLIES TILMAN C , WILLERT-PORADA MONIKA A , GERDES THORSTEN , SCHMIDT-RODENKIRCHEN ACHIM
发明人： HINTZER KLAUS , KAEMPF GUNTHER J , KOLBECK THOMAS , ZIPPLIES TILMAN C , WILLERT-PORADA MONIKA A , GERDES THORSTEN , SCHMIDT-RODENKIRCHEN ACHIM
IPC分类号： C07C17/367 , C07C21/18 , C07C21/185
CPC分类号： C07C17/367 , C07C21/18 , C07C21/185
摘要： Process for producing fluorinated olefins from fluorinated materials, the process comprising thermally decomposing the fluoropolymers into fluoroolefins in a reactor having a feeding zone where the fluorinated materials are fed into the reactor and a decomposition zone where the fluorinated materials are thermally decomposed and wherein the thermal decomposition is carried out in the presence of microwave irradiation.
摘要翻译：由氟化材料生产氟化烯烃的方法，该方法包括在具有将氟化材料加入反应器的进料区和热分解氟化材料的分解区的反应器中将含氟聚合物热分解为氟代烯烃，并且其中热分解在微波照射下进行。

7. 发明申请

WO2011014715A3 FLUOROPOLYMER COMPOSITIONS CONTAINING A POLYOL COMPOUND AND METHODS OF MAKING THEM 审中-公开
标题翻译：含多元醇化合物的含氟聚合物组合物及其制备方法
公开(公告)号：WO2011014715A3
公开(公告)日：2011-05-05
申请号：PCT/US2010043805
申请日：2010-07-30
申请人： 3M INNOVATIVE PROPERTIES CO , ZIPPLIES TILMAN C , HINTZER KLAUS , DADALAS MICHAEL C , FREY OLIVER , LOCHHAAS KAI HELMUT
发明人： ZIPPLIES TILMAN C , HINTZER KLAUS , DADALAS MICHAEL C , FREY OLIVER , LOCHHAAS KAI HELMUT
IPC分类号： C08L5/00 , C08F14/18 , C08G18/28 , C08G18/62 , C08L27/12
CPC分类号： C08F14/18 , C08F2/16 , C08K5/053 , C08K5/103 , C08K5/151 , C08L5/00 , C08L27/16 , C08L27/18 , C08L27/20 , C09D127/18 , C08L2666/26
摘要： There are provided compositions comprising (i) at least one non-aromatic polyol compound containing at least one polyol unit having at least two hydroxyl groups and at least one long chain unit containing at least 6 carbon atoms; and (ii) at least one fluoropolymer comprising repeating units derived from a fluorinated olefin. There are also provided methods of improving the shear stability of fluoropolymer dispersions, methods of coating substrates, and substrates coated with the above described composition.
摘要翻译：提供了组合物，其包含（i）至少一种非芳族多元醇化合物，其含有至少一个具有至少两个羟基的多元醇单元和至少一个含有至少6个碳原子的长链单元; 和（ii）至少一种含有衍生自氟化烯烃的重复单元的含氟聚合物。还提供了改善含氟聚合物分散体的剪切稳定性的方法，涂布基材的方法和涂布有上述组合物的基材。

8. 发明申请

WO2008127461A2 THERMALLY STABLE FLUOROPOLYMERS 审中-公开
标题翻译：热稳定的氟聚合物
公开(公告)号：WO2008127461A2
公开(公告)日：2008-10-23
申请号：PCT/US2007086900
申请日：2007-12-10
申请人： 3M INNOVATIVE PROPERTIES CO , CHEN LISA P , KASPAR HARALD , ZIPPLIES TILMAN C , YODER BARBARA A , LINERT JEFFREY G
发明人： CHEN LISA P , KASPAR HARALD , ZIPPLIES TILMAN C , YODER BARBARA A , LINERT JEFFREY G
IPC分类号： C08F8/44
CPC分类号： C08F8/44 , C08F2800/10 , C08F214/26
摘要： A fluorinated polymer composition, an article made with the fluorinated polymer composition and a method of making the fluorinated polymer are provided. The method comprises a partially fluorinated polymer which has carboxylic or carboxylate end groups and forming a potassium salt with the end groups of the fluorinated polymer through ion exchange. The resulting partially fluorinated polymers demonstrate high thermal stability without the addition of thermal stabilizers.
摘要翻译：提供含氟聚合物组合物，由氟化聚合物组合物制成的制品和制备氟化聚合物的方法。该方法包括具有羧酸或羧酸酯端基并通过离子交换与氟化聚合物的端基形成钾盐的部分氟化聚合物。得到的部分氟化聚合物在不添加热稳定剂的情况下表现出高的热稳定性。

9. 发明申请

WO2015088784A3 HIGHLY FLUORINATED ELASTOMERS 审中-公开
标题翻译：高荧光弹性体
公开(公告)号：WO2015088784A3
公开(公告)日：2015-08-27
申请号：PCT/US2014067564
申请日：2014-11-26
申请人： 3M INNOVATIVE PROPERTIES CO
发明人： HINTZER KLAUS , JOCHUM FLORIAN D , KASPAR HARALD , LOCHHAAS KAI H , ZIPPLIES TILMAN C
IPC分类号： C08F214/26 , C08F216/12 , C08F216/14 , C08K5/14 , C08L27/18
CPC分类号： C08F214/262 , C08F214/26 , C08K5/06 , C08K5/095 , C08K5/14
摘要： Described herein is a peroxide curable, highly fluorinated elastomer derived from tetrafluoroethylene, a perfluoro ether monomer, and a compound selected from at least one of a highly fluorinated bisolefin ether and an iodine-containing perfluorinated ether.
摘要翻译：本文描述了由四氟乙烯衍生的过氧化物可固化的高度氟化的弹性体，全氟醚单体和选自高度氟化的双烯烃醚和含碘全氟化醚中的至少一种的化合物。

10. 发明申请

WO2016130914A8 TETRAFLUOROETHYLENE/HEXAFLUOROPROPYLENE COPOLYMERS INCLUDING PERFLUOROALKOXYALKYL PENDANT GROUPS 审中-公开
标题翻译：包含全氟烷氧基烷基的四氟乙烯/六氟丙烯共聚物
公开(公告)号：WO2016130914A8
公开(公告)日：2016-12-22
申请号：PCT/US2016017744
申请日：2016-02-12
申请人： 3M INNOVATIVE PROPERTIES CO
发明人： DUCHESNE DENIS , HINTZER KLAUS , KASPAR HARALD , LOCHHAAS KAI HELMUT , NELSON PER M , SCHROOTEN JENS , WEILANDT KARL D , ZIPPLIES TILMAN C
IPC分类号： H01B3/44 , C08F214/26 , C08J5/12
CPC分类号： C08F214/282 , C08F8/22 , C08F214/26 , C08F214/262 , H01B3/445
摘要： A copolymer having tetrafluoroethylene units, hexafluoropropylene units, and units independently represented by formula in a range from 0.02 to 2 mole percent, based on the total amount of the copolymer. Rf is a linear or branched perfluoroalkyl group having from 1 to 8 carbon atoms and optionally interrupted by one or more -O- groups, z is 1 or 2, each n is independently from 1 to 6, and m is 0 or 1. The copolymer has a melt flow index in a range from 25 grams per 10 minutes to 35 grams per 10 minutes and has a combined number of unstable end groups and -CF2H end groups in a range from 25 per 106 carbon atoms up to 120 per 106 carbon atoms. The copolymer can be extruded to make articles, such as insulated cables. A method of making the copolymer is also disclosed.
摘要翻译：基于共聚物的总量，具有四氟乙烯单元，六氟丙烯单元和由式独立地表示的单元的共聚物为0.02-2摩尔％。 Rf是具有1至8个碳原子并且任选被一个或多个-O-基团间隔的直链或支链全氟烷基，z为1或2，每个n独立地为1至6，并且m为0或1。共聚物具有25克每10分钟至35克每10分钟的熔体流动指数并且具有组合数量的不稳定端基和-CF 2 H端基，其范围为每10 6个碳原子25个至每10 6个碳原子120个原子。共聚物可以被挤压成制品，例如绝缘电缆。还公开了制造共聚物的方法。

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