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1. 发明申请

WO1998011854A1 HYDROPHILIC POLYETHER POLYURETHANES CONTAINING CARBOXYLIC ACID 审中-公开
标题翻译：含有羧基的羟基聚醚聚氨酯
公开(公告)号：WO1998011854A1
公开(公告)日：1998-03-26
申请号：PCT/US1997016967
申请日：1997-09-19
申请人： TYNDALE PLAINS-HUNTER, LTD.
发明人： TYNDALE PLAINS-HUNTER, LTD. , REICH, Murray, H. , NELSON, Ken
IPC分类号： A61F13/00
CPC分类号： C08G18/758 , A61K8/87 , A61L15/26 , A61L15/58 , A61L29/085 , A61Q9/00 , A61Q15/00 , A61Q19/00 , C08G18/0823 , C08G18/4833 , C08G18/6674 , Y10S528/904 , Y10S528/905 , C08L75/08
摘要： An improved polyurethane is prepared by reacting a diol, an organic diisocyanate and a carboxylic acid with a critical selection of the amount of water in the reaction mixture. The polyurethane has improved adhesion, hydrophilicity and strength. The polymer has improved feel, and washability. Solutions of the polymer have low viscosity in aqueous solutions.
摘要翻译：通过二醇，有机二异氰酸酯和羧酸与反应混合物中水的临界选择反应来制备改进的聚氨酯。聚氨酯具有改善的粘合性，亲水性和强度。聚合物具有改善的手感和可洗性。聚合物的溶液在水溶液中具有低粘度。

2. 发明申请

WO1989007619A1 HYDROPHILIC CARBOXY POLYURETHANES 审中-公开
标题翻译：亲水性聚氨酯
公开(公告)号：WO1989007619A1
公开(公告)日：1989-08-24
申请号：PCT/US1988000637
申请日：1988-02-19
申请人： TYNDALE PLAINS-HUNTER, LTD.
发明人： TYNDALE PLAINS-HUNTER, LTD. , JOHNSTON, Christian, W. , TEFFENHART, John, M.
IPC分类号： C08G18/30
CPC分类号： C08G18/832 , A61K8/87 , A61K47/34 , A61L15/26 , A61L27/18 , A61L29/06 , A61L29/085 , A61Q3/02 , C08G18/0823 , C08G18/34 , C08G18/6625 , Y10T428/31551 , Y10T428/31605 , C08L75/04
摘要： Hydrophilic polyurethane polymers having carboxy groups in the polymer backbone are prepared by reacting a polyol component, an ester of a carboxylic acid and a polyisocyanate to form a polyurethane intermediate. The intermediate is then saponified and the saponified product neutralized to form free carboxy groups. The water absorption of the intermediates and saponified polymers is above 10 % and the polyurethanes may range from rigid solids to gel-like, high water absorptive polymers. Neutralization of the carboxy group with ammonium hydroxide produces a water soluble polyurethane which becomes water insoluble when the ammonia is driven off. The carboxy groups introduced into the polymeric chain provide reactive sites for attachment of various side-groups and also allow for various curing procedures. The polymers exhibit excellent adhesion to various substrates, and are suitable for use as light sensitive photographic layers on films, paper or glass; as boat and pipe coatings for decreasing hydrodynamic drag; as drug delivery systems; as burn and wound dressings; in cosmetic applications; in body implants; as coatings on cannulae; and a host of other applications.

3. 发明申请

WO1989007117A1 THERMALLY REVERSIBLE POLYURETHANE HYDROGELS AND COSMETIC, BIOLOGICAL AND MEDICAL USES 审中-公开
标题翻译：热可逆聚氨酯水凝胶和化妆品，生物和医疗用途
公开(公告)号：WO1989007117A1
公开(公告)日：1989-08-10
申请号：PCT/US1988000280
申请日：1988-02-01
申请人： TYNDALE PLAINS-HUNTER, LTD.
发明人： TYNDALE PLAINS-HUNTER, LTD. , GOULD, Francis, E. , JOHNSTON, Christian, W. , SEEMS, George, E.
IPC分类号： C08G18/30
CPC分类号： A61K8/042 , A61K8/87 , A61K9/2031 , A61L26/0019 , A61L26/008 , A61Q13/00 , A61Q15/00 , A61Q17/00 , A61Q19/00 , C08G18/4833 , C08G18/6674 , C08G18/758 , C08G2210/00 , C08L75/04
摘要： Thermally reversible polyurethane hydrogels are formed by adding water to a gel forming hydrophilic polyurethane polymer produced by reacting under anhydrous conditions an organic diisocyanate with a glycol component in an NCO/OH mole ratio of from about 0.5/1 to about 1/1 wherein the percentage by weight of the diisocyanate in the reaction mixture is from about 2 % to about 25 %. The hydrogels are solids at room temperature but liquify at higher temperatures such as body temperature and therefore are useful as carriers for the protection, delivery and sustained release of a variety of active agents including pharmaceuticals, cosmetics, living cells and organisms.
摘要翻译：通过向形成亲水性聚氨酯聚合物的凝胶形成亲水性聚氨酯聚合物，在无水条件下使有机二异氰酸酯与NCO / OH摩尔比为约0.5 / 1〜约1/1的二醇成分反应生成热可逆性聚氨酯水凝胶，其中百分比的反应混合物中的二异氰酸酯为约2％至约25％。水凝胶在室温下为固体，但在较高温度例如体温下液化，因此可用作各种活性剂（包括药物，化妆品，活细胞和生物体）的保护，递送和持续释放的载体。

4. 发明申请

WO1989003860A1 MOISTURE SENSITIVE ELASTOMER COMPOSITIONS 审中-公开
标题翻译：水分敏感性弹性体组合物
公开(公告)号：WO1989003860A1
公开(公告)日：1989-05-05
申请号：PCT/US1988003577
申请日：1988-10-12
申请人： TYNDALE PLAINS-HUNTER, LTD.
发明人： TYNDALE PLAINS-HUNTER, LTD. , FAUST, Ellsworth, E. , KLIMENT, Charles, K. , GOULD, Francis, E.
IPC分类号： C08L75/08
CPC分类号： C08G18/12 , A61B42/00 , A61L9/042 , A61L15/225 , A61L29/049 , A61L31/041 , C08G18/0804 , C08G18/4833 , C08G18/6674 , C08K7/00 , C08K2201/00 , C08L7/02 , C08L9/08 , C08L9/10 , C08L21/00 , C08L21/02 , C08L75/08 , A61L15/46 , A61L15/44 , C08L75/04 , C08L11/00 , C08L25/10 , C08L9/00 , C08G18/302 , C08L2666/14 , C08L2666/08 , A61F6/04 , A61F6/08
摘要： Elastomer compositions, having water absorptive properties, are produced by subjecting a homogeneous blend of a curable rubber latex and a hydrophilic polyurethane polymer, to curing conditions. Moisture permeable membranes, water swellable sealants, extruded shapes and active agent media are produced from the composition.
摘要翻译：具有吸水性质的弹性体组合物通过将可固化橡胶胶乳和亲水性聚氨酯聚合物的均匀共混物进行固化来制备。通过该组合物生产水分渗透膜，水可膨胀密封剂，挤出形状和活性剂介质。

5. 发明申请

WO9947127A8 HYDROPHILIC AND HYDROPHOBIC POLYETHER POLYURETHANES AND USES THEREFOR 审中-公开
标题翻译：水解和疏水性聚酯聚氨酯及其用途
公开(公告)号：WO9947127A8
公开(公告)日：1999-11-25
申请号：PCT/US9905657
申请日：1999-03-15
申请人： TYNDALE PLAINS HUNTER LTD , REICH MURRAY H , TEFFENHART JOHN , KUZMA JIRINA
发明人： REICH MURRAY H , TEFFENHART JOHN , KUZMA JIRINA
IPC分类号： A61K8/87 , A61K9/22 , A61K47/34 , A61L27/18 , A61L29/06 , A61L31/06 , A61Q5/00 , A61Q5/02 , A61Q5/12 , A61Q19/00 , B32B27/40 , C08G18/40 , C08G18/44 , C08G18/48 , C08G18/50 , C08G18/61 , C08G18/66 , C08G18/75 , B32B27/00 , C08F8/30 , C08L75/00 , D02G3/00
CPC分类号： C08G18/758 , A61K8/87 , A61K47/34 , A61L27/18 , A61L29/06 , A61L31/06 , A61Q5/02 , A61Q5/06 , A61Q5/12 , A61Q9/02 , A61Q17/04 , A61Q19/00 , B32B27/40 , C08G18/4018 , C08G18/44 , C08G18/4808 , C08G18/4858 , C08G18/5096 , C08G18/61 , C08G18/6607 , C08G18/667 , C08G18/6674 , C08G18/6681 , Y10T428/2933 , Y10T428/31551 , Y10T428/31565 , Y10T428/31587 , C08L75/08
摘要： An improved amphiphilic diol is prepared with a controlled type and amount of alkylene glycol, catalyst, hydrophobic and hydrophilic diol with diisocyanate and water. Critical selection of the type, molecular weight and ratios of hydrophilic to hydrophobic diol, isocyanate to hydroxyl groups, average molecular weight of the diol component, the amount of water in the reaction mixture produces a polyurethane having high slip, Shore A Hardness values, wet tensile strength and tear strength. This invention also includes uses of the polyurethane in catheters, shaving products, synthetic valves, veins and arteries, stents, ports, shunts and coatings. Preferably, the polyurethane is used in combination with a filler for application to rubber gloves. In addition, dispersions, lotions, gels and solutions can be formed of the polyurethane.
摘要翻译：用受控类型和量的亚烷基二醇，催化剂，疏水和亲水二醇与二异氰酸酯和水制备改进的两亲二醇。关键选择亲水至疏水二醇，异氰酸酯与羟基的相对分子量和比例，二醇组分的平均分子量，反应混合物中的水量产生具有高滑移，肖氏A硬度值，湿润的聚氨酯拉伸强度和撕裂强度。本发明还包括聚氨酯在导管，剃须产品，合成瓣膜，静脉和动脉，支架，口，分流器和涂层中的用途。优选地，聚氨酯与填料一起使用以用于橡胶手套。此外，分散体，洗剂，凝胶和溶液可以由聚氨酯形成。

6. 发明申请

WO1998008884A1 HYDROPHILIC AND HYDROPHOBIC POLYETHER POLYURETHANES AND USES THEREFOR 审中-公开
标题翻译：水解和疏水性聚酯聚氨酯及其用途
公开(公告)号：WO1998008884A1
公开(公告)日：1998-03-05
申请号：PCT/US1997015008
申请日：1997-08-26
申请人： TYNDALE PLAINS-HUNTER, LTD.
发明人： TYNDALE PLAINS-HUNTER, LTD. , REICH, Murray, H. , NELSON, Ken , KUZMA, Jirina
IPC分类号： C08G18/48
CPC分类号： C08G18/667 , A61K8/87 , A61K47/34 , A61L26/0019 , A61L27/18 , A61L27/34 , A61L29/06 , A61L29/085 , A61L31/06 , A61L31/10 , A61Q5/02 , A61Q5/12 , A61Q19/00 , B32B27/40 , C08G18/302 , C08G18/4018 , C08G18/44 , C08G18/4808 , C08G18/4858 , C08G18/5096 , C08G18/61 , C08G18/6511 , C08G18/6607 , C08G18/6674 , C08G18/6681 , C08G18/758 , C08L75/08
摘要： An improved amphiphilic diol is prepared with a controlled type and amount of alkylene glycol, hydrophobic and hydrophilic diol with diisocyanate and water. Critical selection of the type, molecular weight and ratios of hydrophilic to hydrophobic diol, isocyanate to hydroxyl groups, average molecular weight of the diol component, the amount of water in the reaction mixture produces a polyurethane having high slip, Shore A Hardness values, wet tensile strength and tear strength. This invention also includes uses of the polyurethane in catheters, shaving products, synthetic valves, veins and arteries, stents, ports, shunts and coatings. Preferably, the polyurethane is used in combination with a filler for application to rubber gloves. In addition, dispersions, lotions, gels and solutions can be formed of the polyurethane.
摘要翻译：用受控类型和量的亚烷基二醇，疏水和亲水的二醇与二异氰酸酯和水制备改进的两亲二醇。关键选择亲水至疏水二醇，异氰酸酯与羟基的类型，分子量和比例，二醇组分的平均分子量，反应混合物中的水量产生高滑爽聚氨酯，肖氏A硬度值，湿润拉伸强度和撕裂强度。本发明还包括聚氨酯在导管，剃须产品，合成瓣膜，静脉和动脉，支架，端口，分流器和涂层中的用途。优选地，聚氨酯与用于橡胶手套的填料结合使用。此外，分散体，洗剂，凝胶和溶液可以由聚氨酯形成。

7. 发明申请

WO1996015171A1 POLYETHER POLYURETHANE POLYMERS, GELS, SOLUTIONS AND USES THEREOF 审中-公开
标题翻译：聚酯聚氨酯聚合物，凝胶，溶液及其用途
公开(公告)号：WO1996015171A1
公开(公告)日：1996-05-23
申请号：PCT/US1995014542
申请日：1995-11-08
申请人： TYNDALE PLAINS-HUNTER, LTD.
发明人： TYNDALE PLAINS-HUNTER, LTD. , REICH, Murray, H. , NELSON, Ken , KUZMA, Jirina
IPC分类号： C08G18/30
CPC分类号： A61K8/042 , A61K8/87 , A61L26/0019 , A61L27/18 , A61Q15/00 , A61Q17/04 , A61Q19/00 , C08G18/0857 , C08G18/302 , C08G18/6674 , C08G18/75 , C08G18/758 , C08G2210/00 , C08G2220/00 , Y10S424/13 , Y10T428/31551 , C08L75/04
摘要： A new polyurethane is prepared by reacting a diol component and an organic diisocyanate with critical selection of the amount of water in the reaction mixture and the diol component. The diol component is a long chain polyoxyethylene glycol optionally mixed with a low molecular weight polyoxyethylene glycol. A tough gel can be formed by mixing the polyurethane in a diol or triol and water solution. The tough gel can be used in burn and wound dressings, electroconductive pads, high slip materials and surgical implants. An optically clear gel can also be formed. Solutions and emulsions can be formed of the polymer and combined with fillers to form face creams and antiperspirants. A film can cover one side of the gel for burn and wound applications. The gel can be used in squeeze tubes and in spray cans in burn wound care dressings and industrial applications and in bags and containers for use in plastic surgery implants.
摘要翻译：通过使二醇组分和有机二异氰酸酯与反应混合物和二醇组分中的水的临界选择反应来制备新的聚氨酯。二醇组分是任选与低分子量聚氧乙烯二醇混合的长链聚氧乙二醇。可以通过将聚氨酯混合在二醇或三醇和水溶液中来形成坚韧的凝胶。坚韧的凝胶可用于烧伤和伤口敷料，导电垫，高滑动材料和手术植入物。还可以形成光学透明的凝胶。溶液和乳液可以由聚合物形成并与填料组合以形成面霜和止汗剂。胶片可以覆盖凝胶的一面，用于烧伤和伤口应用。该凝胶可用于挤压管和喷涂罐中，用于烧伤伤口护理敷料和工业应用以及用于整形手术植入物的袋子和容器中。

8. 发明申请

WO1993012802A1 BIOMEDICAL WATER SOLUBLE HYDROPHILIC POLYURETHANE POLYMERS AND METHOD OF USE THEREOF 审中-公开
标题翻译：生物医药水溶性聚合物聚氨酯聚合物及其使用方法
公开(公告)号：WO1993012802A1
公开(公告)日：1993-07-08
申请号：PCT/US1992011162
申请日：1992-12-22
申请人： TYNDALE PLAINS-HUNTER LTD.
发明人： TYNDALE PLAINS-HUNTER LTD. , GOULD, Francis, E. , REICH, Murray, H.
IPC分类号： A61K31/785
CPC分类号： A61K31/785 , A61K9/0048 , A61K47/34 , Y10S514/825 , Y10S514/912 , Y10S514/913 , Y10S514/914 , Y10S514/915
摘要： A method for treating a body condition comprising introducing an aqueous solution of a water soluble polyether polyurethane into said body condition.

9. 发明申请

WO1989008672A1 HYDROPHILIC POLYURETHANES PREPARED FROM MIXED OXYALKYLENE GLYCOLS 审中-公开
标题翻译：由混合的氧亚氨基甘油制备的亲水聚氨酯
公开(公告)号：WO1989008672A1
公开(公告)日：1989-09-21
申请号：PCT/US1988003677
申请日：1988-10-19
申请人： TYNDALE PLAINS-HUNTER, LTD.
发明人： TYNDALE PLAINS-HUNTER, LTD. , TEFFENHART, John, M.
IPC分类号： C08G18/48
CPC分类号： A61Q19/08 , A61K8/0208 , A61K8/87 , A61K9/2853 , A61K9/4891 , A61K9/7015 , A61L27/34 , A61L29/085 , A61L31/10 , A61Q15/00 , A61Q19/00 , C08G18/302 , C08G18/6674 , Y10S528/904 , C08L75/04 , A61B42/00
摘要： A hydrophilic, thermoplastic polyurethane polymer of improved dimensional stability and mechanical strength having an average molecular weight of from about 10,000 to about 200,000 produced by reacting (A) an organic diisocyanate with (B) a blend of glycol components comprising (i) ethylene glycol and/or diethylene glycol, (ii) a polyoxyethylene glycol having an average molecular weight of from about 400 to about 20,000 and (iii) a polyoxypropylene glycol having an average molecular weight of from about 200 to about 2500, and (C) water in an amount up to about 0.5% by weight of the reaction mixture. The polymers are particularly useful in the form of a film product such as gloves and condoms. Other uses are as low friction coatings, body implants and active agent release media.

10. 发明申请

WO1989005319A1 HYDROPHILIC POLYURETHANES OF IMPROVED STRENGTH 审中-公开
标题翻译：改善强度的亲水聚氨酯
公开(公告)号：WO1989005319A1
公开(公告)日：1989-06-15
申请号：PCT/US1988004263
申请日：1988-11-30
申请人： TYNDALE PLAINS-HUNTER, LTD.
发明人： TYNDALE PLAINS-HUNTER, LTD. , GOULD, Francis, E. , JOHNSTON, Christian, W.
IPC分类号： C08G18/28
CPC分类号： G02B1/043 , A61L15/26 , A61L27/18 , A61L29/085 , A61L31/06 , C08G18/302 , C08G18/4833 , C08G18/65 , C08G18/6674 , C08G2210/00 , Y10S623/924 , C08L75/04
摘要： The strength and integrity of hydrophilic polyurethane resins prepared by reacting a diol component, an organic chain extender and an organic diisocyanate are improved by critical selection of the diol component, the amount of water in the reaction mixture and the mole ratios of the reactants. The diol component is at least one of (1) a long chain poly(oxyethylene) glycol of molecular weight above 2500 and (2) a medium chain poly(oxyalkylene) glycol or polyester glycol of 250-2500 molecular weight. The chain extender is a difunctional compound having a molecular weight of less than 250. The amount of water in the reaction mixture is 0.5 to 2.5 wt. % and the mole ratios of the diols and water to the chain extender may range as follows: (i) 0.4 to 0.5 of diol (1) and 0.5 to 8.0 of water; (ii) 0.1 to 0.75 of diol (2) and 0.05 to 3.3 of water; (iii) 0.06 to 0.04 of diol (1), 0.1 to 0.2 of diol (2) and 0.25 to 1.25 of water. The polyurethanes have improved utility as carriers for medicaments and a variety of other active agents, as shaped bodies including cannulae, body implants and films, as coating for anti-drag applications, and particularly as needleless catheters for avoidance of contamination from needles.
摘要翻译：通过二醇组分，有机扩链剂和有机二异氰酸酯反应制备的亲水性聚氨酯树脂的强度和完整性通过二醇组分的临界选择，反应混合物中的水量和反应物的摩尔比得到改善。二醇组分是（1）分子量高于2500的长链聚（氧乙烯）二醇和（2）分子量为250-2500的中链聚（氧亚烷基）二醇或聚酯二醇中的至少一种。扩链剂是分子量小于250的双官能化合物。反应混合物中的水的量为0.5-2.5wt。％，二醇和水与扩链剂的摩尔比可以如下：（i）0.4至0.5的二醇（1）和0.5至8.0的水; （ii）0.1至0.75的二醇（2）和0.05至3.3的水; （iii）0.06至0.04的二醇（1），0.1至0.2的二醇（2）和0.25至1.25的水。作为用于药物和各种其它活性剂的载体，聚氨酯具有改进的作用，作为包括套管，体植入物和膜的成形体，作为抗牵引应用的涂层，特别是作为避免针头污染的无针导管。

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