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1. 发明申请

WO2009132293A1 NOVEL CRYSTAL FORMS OF QUINACRIDONES MADE FROM 2,9-DIMETHOXYQUINACRIDONE AND 2,9-DICHLOROQUINACRIDONE 审中-公开
标题翻译：来自2,9-二甲氧基吡啶酮和2,9-二氯喹啉酮的喹诺酮的新型晶体形式
公开(公告)号：WO2009132293A1
公开(公告)日：2009-10-29
申请号：PCT/US2009/041698
申请日：2009-04-24
申请人： SUN CHEMICAL CORPORATION , THOMPSON, Brian , RICE, Daphne , TIBBS, Tracie , MIMS, Bobby , FLATT, Thomas , FAUBION, Richard , WU, Wengan
发明人： THOMPSON, Brian , RICE, Daphne , TIBBS, Tracie , MIMS, Bobby , FLATT, Thomas , FAUBION, Richard , WU, Wengan
IPC分类号： C09B48/00
CPC分类号： C09B67/0036 , C09B67/0027 , C09D7/41
摘要： Novel crystal forms of solid solutions of 2,9-dimethyoxyquinacridone and 2,9- dichloroquinacridone. The crystal forms may be formed by a process comprising the steps of: a) heating a mixture of 2,5-di(4-methoxyanilino)terephthalic acid, and 2,5-di(4- chloroanilino)terephthalic acid in polyphorsphoric acid at a temperature less than 1050C to form a mixture of 2,9-dimethoxyquinacridone and 2,9-dichloroquinacridone; b) combining the mixture of 2,9-dimethoxyquinacridone and 2,9-dichloroquinacridone with water; and c) heating the mixture of 2,9-dimethoxyquinacridone and 2,9- dichloroquinacridone at a temperature not more than 110°C. Another crystal form may be formed by the process of heating a mixture of 2,9- dimethoxyquinacridone and 2,9-dichloroquinacridone in a polar aprotic solvent. These products are may be used for coloring fibers, plastics, paints, coatings, printing inks, color filters, cosmetics, automotive coatings, textiles, fibers, powder coatings, in-mold coatings, laminate films, and the like.
摘要翻译： 2,9-二甲氧基喹吖啶酮和2,9-二氯喹吖啶酮的新溶液的形式。晶体形式可以通过包括以下步骤的方法形成：a）在多晶磷酸中加热2,5-二（4-甲氧基苯胺基）对苯二甲酸和2,5-二（4-氯苯胺基）对苯二甲酸的混合物温度低于1050℃以形成2,9-二甲氧基喹吖啶酮和2,9-二氯喹吖啶酮的混合物; b）将2,9-二甲氧基喹吖啶酮和2,9-二氯喹吖啶酮的混合物与水混合; 和c）在不高于110℃的温度下加热2,9-二甲氧基喹吖啶酮和2,9-二氯喹吖啶酮的混合物。可以通过在极性非质子溶剂中加热2,9-二甲氧基喹吖啶酮和2,9-二氯喹吖啶酮的混合物的方法形成另一种晶体形式。这些产品可用于着色纤维，塑料，油漆，涂料，印刷油墨，滤色器，化妆品，汽车涂料，纺织品，纤维，粉末涂料，模内涂料，层压膜等。

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