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    • 2. 发明申请
    • METHOD OF OPERATING A DYNAMIC NUCLEAR POLARIZATION SYSTEM
    • 一种动态核极化系统的运行方法
    • WO2006106285A1
    • 2006-10-12
    • PCT/GB2006/000653
    • 2006-02-24
    • OXFORD INSTRUMENTS MOLECULAR BIOTOOLS LIMITEDSTRANGE, Daniel, RobertSLADE, Robert, Andrew
    • STRANGE, Daniel, RobertSLADE, Robert, Andrew
    • G01R33/28
    • G01R33/28G01R33/62
    • A method of operating a DNP system comprising: a cryostat (1) ; a magnetic field generator (2) located in the cryostat for generating a magnetic field in a working volume; a microwave cavity (8) within which the working volume is located; and a waveguide (18) for supplying microwave power to the microwave cavity; the method comprising: a) locating a sample in the working volume and subjecting the sample to a magnetic field generated by the magnetic field generator; b) supplying liquid coolant to the working volume to cool the sample; c) irradiating the sample with microwave power so as to hyperpolarize nuclear spins in the sample; and d) warming the sample following the irradiation step by expelling liquid coolant from the working volume while leaving the sample in the working volume.
    • 一种操作DNP系统的方法,包括:低温恒温器(1); 位于所述低温恒温器中的用于产生工作容积中的磁场的磁场发生器(2) 工作容积所在的微波腔(8); 以及用于向微波腔提供微波功率的波导(18); 所述方法包括:a)将样品定位在所述工作体积中并使所述样品经受由所述磁场发生器产生的磁场; b)向工作容积供应液体冷却剂以冷却样品; c)用微波功率照射样品,以使样品中的核自旋超极化; 以及d)在照射步骤之后,通过从工作容积中排出液体冷却剂,同时将样品留在工作容积中来加热样品。