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1. 发明申请

WO2019213110A1 HETEROGENEOUS WET SYNTHESIS PROCESS FOR PREPARATION OF HIGH PURITY TUNGSTEN PENTAHALIDE 审中-公开
公开(公告)号：WO2019213110A1
公开(公告)日：2019-11-07
申请号：PCT/US2019/029958
申请日：2019-04-30
申请人： L'AIR LIQUIDE, SOCIETE ANONYME POUR L'ETUDE ET L'EXPLOITATION DES PROCEDES GEORGES CLAUDE , AMERICAN AIR LIQUIDE, INC. , LIU, Yumin , LI, Feng , WAN, Zhiwen , FAFARD, Claudia , WIESE, Stefan , HUSSON, Guillaume , NIKIFOROV, Grigory , SUI, Bin , GIRARD, Jean-Marc
发明人： LIU, Yumin , LI, Feng , WAN, Zhiwen , FAFARD, Claudia , WIESE, Stefan , HUSSON, Guillaume , NIKIFOROV, Grigory , SUI, Bin , GIRARD, Jean-Marc
IPC分类号： C01G41/04
摘要： Synthesis of tungsten pentahalide compositions having low impurity profiles are disclosed. The specific impurity profile permits deposition of high purity tungsten-containing films using vapor deposition processes or other semiconductor manufacturing processes without introduction of performance-impacting contaminants.

2. 发明申请

WO2019213116A1 TUNGSTEN PENTACHLORIDE CONDITIONING AND CRYSTALLINE PHASE MANIPULATION 审中-公开
公开(公告)号：WO2019213116A1
公开(公告)日：2019-11-07
申请号：PCT/US2019/029970
申请日：2019-04-30
申请人： L'AIR LIQUIDE, SOCIETE ANONYME POUR L'ETUDE ET L'EXPLOITATION DES PROCEDES GEORGES CLAUDE , LI, Feng , PLAZA, Sonia , GIRARD, Jean-Marc , BLASCO, Nicolas , LIU, Yumin
发明人： LI, Feng , PLAZA, Sonia , GIRARD, Jean-Marc , BLASCO, Nicolas , LIU, Yumin
IPC分类号： C01G41/04
摘要： A process of conditioning tungsten pentachloride to form specific crystalline phases are disclosed. The specific crystalline phases permit stable vapor pressures over extended periods of time during vapor deposition and etching processes.

3. 发明申请

WO2005065820A1 RHODIUM CONTAINING CATALYSTS 审中-公开
标题翻译：含铑催化剂
公开(公告)号：WO2005065820A1
公开(公告)日：2005-07-21
申请号：PCT/US2004/038825
申请日：2004-11-19
申请人： CELANESE INTERNATIONAL CORPORATION , WANG, Tao , WADE, Leslie, E. , NICOLAU, Ioan , KIMMICH, Barbara , LIU, Yumin , HAN, Jun
发明人： WANG, Tao , WADE, Leslie, E. , NICOLAU, Ioan , KIMMICH, Barbara , LIU, Yumin , HAN, Jun
IPC分类号： B01J23/52
CPC分类号： C07C67/055 , B01J23/464 , B01J23/52 , B01J23/58 , B01J37/0205 , B01J37/03 , B01J37/16 , C07C69/01 , C07C69/15
摘要： The present invention addresses at least four different aspects relating to catalyst structure, methods of making those catalysts and methods of using those catalysts for making alkenyl alkanoates. Separately or together in combination, the various aspects of the invention are directed at improving the production of alkenyl alkanoates and VA in particular, including reduction of by-products and improved production efficiency. A first aspect of the present invention pertains to a unique palladium/gold catalyst or pre-catalyst (optionally calcined) that includes rhodium or another metal. A second aspect pertains to a palladium/gold catalyst or pre-catalyst that is based on a layered support material where on layer of the support material is substantially free of catalytic components. A third aspect pertains to a palladium/gold catalyst or pre-catalyst on a zirconia containing support material. A fourth aspect pertains to a palladium/gold catalyst or pre-catalyst that is produced from substantially chloride free catalytic components.
摘要翻译：本发明涉及与催化剂结构有关的至少四个不同方面，制备这些催化剂的方法和使用这些催化剂制备烯基链烷酸酯的方法。本发明的单独或一起组合地涉及改进烯基链烷酸酯和VA的生产，特别是包括副产物的还原和提高的生产效率。本发明的第一方面涉及包含铑或其它金属的独特的钯/金催化剂或预催化剂（任选煅烧的）。第二方面涉及基于层状载体材料的钯/金催化剂或预催化剂，其中载体材料层基本上不含催化组分。第三方面涉及在含氧化锆载体材料上的钯/金催化剂或预催化剂。第四方面涉及由基本上不含氯的催化组分制备的钯/金催化剂或预催化剂。

4. 发明申请

WO1993021117A1 PROCESS FOR DECREASING CHLORINE CONTENT OF CHLORINATED HYDROCARBONS 审中-公开
标题翻译：降低氯化氢氯化物含量的方法
公开(公告)号：WO1993021117A1
公开(公告)日：1993-10-28
申请号：PCT/US1993003529
申请日：1993-04-14
申请人： THE TRUSTEES OF PRINCETON UNIVERSITY , SCHWARTZ, Jefffrey , LIU, Yumin
发明人： THE TRUSTEES OF PRINCETON UNIVERSITY
IPC分类号： C02F01/70
CPC分类号： A62D3/37 , A62D3/34 , A62D2101/22 , A62D2203/04 , B01D53/8662 , B01D53/8668 , C02F1/70 , C07C17/23 , C07C209/36 , C07C209/42
摘要： The chlorine content in chlorinated hydrocarbons in an environment which admits the presence of air and moisture can be reduced by bringing the chlorinated hydrocarbon into contact wih a dechlorination reagent which comprises (i) a complex of a substantially nontoxic metal having at least two oxidation states and (ii) a reducing agent which reductively returns the complex from its second oxidation step to its first oxidation stage. A representative embodiment involves bis-( eta -cyclopentadienyl)titanium dichloride and sodium tetrahydridoborate.
摘要翻译：通过使氯化烃与脱氯试剂接触，可以减少允许存在空气和水分的环境中氯化烃中的氯含量，该脱氯试剂包括（i）具有至少两种氧化态的基本上无毒的金属的络合物和（ii）将络合物从其第二氧化步骤还原至其第一氧化阶段的还原剂。代表性的实施方案涉及二 - （η5 - 环戊二烯基）二氯化钛和四氢化硼酸钠。

5. 发明申请

WO2019213115A1 TUNGSTEN PENTACHLORIDE CONDITIONING AND CRYSTALLINE PHASE MANIPULATION 审中-公开
公开(公告)号：WO2019213115A1
公开(公告)日：2019-11-07
申请号：PCT/US2019/029969
申请日：2019-04-30
申请人： L'AIR LIQUIDE, SOCIETE ANONYME POUR L'ETUDE ET L'EXPLOITATION DES PROCEDES GEORGES CLAUDE , LI, Feng , PLAZA, Sonia , GIRARD, Jean-Marc , BLASCO, Nicolas , LIU, Yumin
发明人： LI, Feng , PLAZA, Sonia , GIRARD, Jean-Marc , BLASCO, Nicolas , LIU, Yumin
IPC分类号： H01L21/02 , H01L21/285 , H01L21/324
摘要： Conditioning of tungsten pentachloride to form specific crystalline phases is disclosed. The specific crystalline phases permit stable vapor pressures over extended periods of time during vapor deposition and etching processes.

6. 发明申请

WO1995010484A1 PROCESS FOR DECREASING CHLORINE CONTENT IN CHLORINATED HYDROCARBONS 审中-公开
标题翻译：降低氯化氢中氯离子含量的方法
公开(公告)号：WO1995010484A1
公开(公告)日：1995-04-20
申请号：PCT/US1994011697
申请日：1994-10-14
申请人： THE TRUSTEES OF PRINCETON UNIVERSITY , SCHWARTZ, Jeffrey , LIU, Yumin
发明人： THE TRUSTEES OF PRINCETON UNIVERSITY
IPC分类号： C02F01/70
CPC分类号： A62D3/37 , A62D2101/22 , A62D2203/04
摘要： The chlorine or halide content in a chlorinated hydrocarbon or halogenated aromatic hydrocarbon in an environment which admits to the presence of air and moisture can be reduced by bringing the chlorinated hydrocarbon or halogenated aromatic hydrocarbon into contact with a reagent which comprises (i) a complex of a substantially nontoxic metal having at least two oxidation states and (ii) a reducing agent which reductively returns the complex from its second oxidation step to its first oxidation stage. A representative embodiment involves bis-( eta -cyclopentadienyl)titanium dichloride and sodium tetrahydridoborate. Optionally, the reaction is conducted in the presence of an aliphatic or aromatic amine, optionally in the presence of an inert organic solvent.
摘要翻译：通过使氯代烃或卤代芳烃与试剂接触，可以减少允许存在空气和水分的环境中氯化烃或卤代芳烃中的氯或卤化物含量，该试剂包括（i）具有至少两种氧化态的基本上无毒的金属和（ii）将络合物从其第二氧化步骤还原至其第一氧化阶段的还原剂。代表性的实施方案涉及二 - （η5 - 环戊二烯基）二氯化钛和四氢化硼酸钠。任选地，反应在脂族或芳族胺的存在下进行，任选在惰性有机溶剂的存在下进行。

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