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1. 发明申请

WO2013003061A1 IMPROVED PROCESS FOR MAKING LOW VISCOSITY, FAST CURING SILANE TERMINATED POLYMERS 审中-公开
标题翻译：用于制造低粘度的改进方法，快速固化硅烷终止聚合物
公开(公告)号：WO2013003061A1
公开(公告)日：2013-01-03
申请号：PCT/US2012/042444
申请日：2012-06-14
申请人： DOW GLOBAL TECHNOLOGIES LLC , VYAKARANAM, Kamesh R. , ZHANG, Ling , MINNIKANTI, Venkat S. , DUGGAL, Rajat , KOONCE, William A. , SINGH, Amarnath , ATHEY, Phillip S.
发明人： VYAKARANAM, Kamesh R. , ZHANG, Ling , MINNIKANTI, Venkat S. , DUGGAL, Rajat , KOONCE, William A. , SINGH, Amarnath , ATHEY, Phillip S.
IPC分类号： C08G18/10 , C08G18/28 , C08G18/71 , C08G18/76
CPC分类号： C08G18/10 , C08G18/289 , C08G18/718 , C08G18/7621 , C08G2190/00 , C08G18/4825 , C08G18/4829
摘要： Methods of producing a composition comprising a crosslinkable silane-terminated polymer having at least one crosslinkable silyl group in each molecule are provided. The method may comprise providing a polymer having at least one unsaturated group and at least one alcohol hydroxyl group in each molecule and having a number average molecular weight between about 100 and about 5,000, adding to the polymer a compound having a hydrogen-silicon bond and a crosslinkable silyl group in each molecule and a hydrosilylation catalyst to thereby carry out a hydrosilylation reaction to form a composition comprising hydrosilylated polymers, wherein the hydrosilylation reaction has a hydrosilylation efficiency greater than 50% as determined by 1 H-NMR, capping the hydrosilylated polymers by adding the hydrosilylated polymer to at least one isocyanate at an index of between about 100 and about 250, and reacting the isocyanate capped hydrosilylated polymer with a polyol having a nominal functionality of at least 2 to form the composition comprising a crosslinkable silane-terminated polymer.
摘要翻译：提供了包含在每个分子中具有至少一个交联性甲硅烷基的可交联硅烷封端的聚合物的组合物的方法。该方法可以包括提供在每个分子中具有至少一个不饱和基团和至少一个醇羟基并且数均分子量在约100至约5,000之间的聚合物，向聚合物中加入具有氢 - 硅键的化合物和每个分子中的可交联甲硅烷基和氢化硅烷化催化剂，由此进行氢化硅烷化反应以形成包含氢化硅烷化聚合物的组合物，其中氢化硅烷化反应的氢化硅烷化效率大于50％，如通过1 H-NMR确定的，氢化硅烷化聚合物由将氢化硅烷化聚合物以约100至约250的指数加入到至少一种异氰酸酯中，并使异氰酸酯封端的硅烷化聚合物与标称官能度至少为2的多元醇反应，以形成包含可交联硅烷封端的聚合物的组合物。

2. 发明申请

WO2011078922A1 POLYURETHANE-BASED SEALANT FOR INSULATED GLASS UNITS 审中-公开
标题翻译：基于聚氨酯的绝缘玻璃密封件
公开(公告)号：WO2011078922A1
公开(公告)日：2011-06-30
申请号：PCT/US2010/056677
申请日：2010-11-15
申请人： DOW GLOBAL TECHNOLOGIES LLC , RADHAKRISHNAN, Bindushree , LATHAM, Dwight, D. , GRIER, Laura, A. , KOONCE, William, A. , SCHAEFER, Matthias , RIES, Paul, D.
发明人： RADHAKRISHNAN, Bindushree , LATHAM, Dwight, D. , GRIER, Laura, A. , KOONCE, William, A. , SCHAEFER, Matthias , RIES, Paul, D.
IPC分类号： C09J175/04 , C03C27/10 , C08G18/10 , C08G18/36 , C08K5/00 , C09K3/10 , C08G18/79
CPC分类号： C09K3/1021 , C08G18/10 , C08G18/36 , C08G18/4288 , C08G18/4891 , C08G18/6674 , C08G2190/00 , C08K5/10 , C08G18/664 , C08L75/04
摘要： Insulated glass units are sealed with polyurethane made using a natural oil-based polyol (NOBP). In one embodiment the NOBP is made using a monol-rich monomer containing high levels of mono-hydroxy functional fatty acid methyl esters. Insulated glass sealants based on these compounds provide enhanced resistance to UV and oxidative degradation as compared to conventional products while still providing the required barrier and mechanical properties.
摘要翻译：绝缘玻璃单元使用天然油基多元醇（NOBP）制成的聚氨酯密封。在一个实施方案中，使用含有高含量单羟基官能脂肪酸甲酯的单醇富含单体制备NOBP。与常规产品相比，基于这些化合物的绝缘玻璃密封剂提供了对UV和氧化降解的增强的抗性，同时仍然提供所需的屏障和机械性能。

3. 发明申请

WO2005000934A1 HIGH PERFORMANCE POLYURETHANE CARPET BACKINGS CONTAINING MODIFIED VEGETABLE OIL POLYOLS 审中-公开
标题翻译：高性能聚氨酯地毯背包含改性蔬菜油多元醇
公开(公告)号：WO2005000934A1
公开(公告)日：2005-01-06
申请号：PCT/US2004/016981
申请日：2004-05-28
申请人： DOW GLOBAL TECHNOLOGIES INC , JENKINES, Randall, C. , MOBLEY, Larry, W. , KOONCE, William, A.
发明人： JENKINES, Randall, C. , MOBLEY, Larry, W. , KOONCE, William, A.
IPC分类号： C08G18/36
CPC分类号： C08G18/4288 , C08G18/4018 , C08G18/4841 , C08G18/7664 , C08G2150/60
摘要： Carpet backing for residential, commercial and recreational carpet which exhibits a tuftbind greater than 4.5 kg, ASTM D 1335, contains a polyurethane reaction product of a polyisocyanate; an active hydrogen containing compound; and a polyol reaction product. Typically, the polyol reaction product is a reaction product of a polyol and a vegetable oil and contains less than about 50 percent by weight of unreacted vegetable oil. The vegetable oil is preferably selected from palm oil, safflower oil, canola oil, soy oil, cottonseed oil and rapeseed oil. In a preferred embodiment, the vegetable oil is blown. Typically, the amount of unreacted vegetable oil in the polyol reaction product is less than about 34 weight percent. The hard segment of the resulting polyurethane reaction product constitutes at least 20 weight percent of the polyurethane reaction product. The carpet backing of the invention may be used as a precoat, a laminate or foam coating.
摘要翻译： ASTM D 1335的住宅，商业和娱乐地毯的地毯背衬大于4.5公斤，含有多异氰酸酯的聚氨酯反应产物; 含氢活性化合物; 和多元醇反应产物。通常，多元醇反应产物是多元醇和植物油的反应产物，并且含有小于约50重量％的未反应植物油。植物油优选选自棕榈油，红花油，卡诺拉油，大豆油，棉籽油和菜籽油。在优选的实施方案中，植物油被吹送。通常，多元醇反应产物中未反应的植物油的量小于约34重量％。所得聚氨酯反应产物的硬链段构成聚氨酯反应产物的至少20重量％。本发明的地毯背衬可以用作预涂层，层压板或泡沫涂层。

4. 发明申请

WO2013032718A1 METHOD FOR PREPARING FLEXIBLE POLYURETHANE FOAM WITH HYDROLYSABLE SILANE COMPOUNDS 审中-公开
标题翻译：用可水解硅烷化合物制备柔性聚氨酯泡沫体的方法
公开(公告)号：WO2013032718A1
公开(公告)日：2013-03-07
申请号：PCT/US2012/051031
申请日：2012-08-16
申请人： DOW GLOBAL TECHNOLOGIES LLC , WALIA, Parvinder, S. , OBI, Bernard, E , MINNIKANTI, Venkat, S. , KOONCE, William, A. , VYAKARANAM, Kamesh, R. , ZHANG, Ling , FREGNI, Sabrina
发明人： WALIA, Parvinder, S. , OBI, Bernard, E , MINNIKANTI, Venkat, S. , KOONCE, William, A. , VYAKARANAM, Kamesh, R. , ZHANG, Ling , FREGNI, Sabrina
IPC分类号： C08J9/00 , C08J9/12
CPC分类号： C08G18/289 , C08G18/10 , C08G18/165 , C08G18/1833 , C08G18/1841 , C08G18/2063 , C08G18/246 , C08G18/3275 , C08G18/4816 , C08G18/4841 , C08G18/6688 , C08G18/7664 , C08G18/778 , C08G2101/0008 , C08G2101/005 , C08G2101/0058 , C08G2101/0083
摘要： Flexible polyurethane foams are made using certain hydrolysable silane compounds in the foam formulation. The hydrolysable silane compounds contain at least one isocyanate-reactive group and at least one hydrolysable silane group. The presence of the hydrolysable silane compound in the foam formulation leads to improved tensile, tear and elongation properties without an adverse effect on other important foam properties such as resiliency and hysteresis loss.
摘要翻译：在泡沫配方中使用某些可水解的硅烷化合物来制造柔性聚氨酯泡沫。可水解硅烷化合物含有至少一个异氰酸酯反应性基团和至少一个可水解硅烷基团。可发泡的硅烷化合物在泡沫配方中的存在导致提高的拉伸，撕裂和伸长性能，而对其他重要的泡沫性能如弹性和滞后损失没有不利影响。

5. 发明申请

WO2013003053A1 SILANE TERMINATED POLYMER FOR COATING, ADHESIVES, SEALANT AND ELASTOMER APPLICATIONS 审中-公开
标题翻译：用于涂料，胶粘剂，密封剂和弹性体应用的硅烷封端聚合物
公开(公告)号：WO2013003053A1
公开(公告)日：2013-01-03
申请号：PCT/US2012/042385
申请日：2012-06-14
申请人： DOW GLOBAL TECHNOLOGIES LLC , VYAKARANAM, Kamesh R. , KOONCE, William A. , ZHANG, Ling , ROSER, Jean-Luc
发明人： VYAKARANAM, Kamesh R. , KOONCE, William A. , ZHANG, Ling , ROSER, Jean-Luc
IPC分类号： C08G18/10 , C08G18/28 , C08G18/63 , C08G18/71 , C08G18/76
CPC分类号： C08G81/025 , C08G18/10 , C08G18/289 , C08G18/632 , C08G18/718 , C08G18/7621 , C08G18/63
摘要： A copolymer-filled crosslinkable silane-terminated polymer having at least one crosslinkable silyl group in each molecule is provided. The copolymer-filled crosslinkable silane-terminated polymer is the reaction product of a copolymer-filled polyol and an isocyanate capped hydrosilylated polymer. The isocyanate capped hydrosilylated polymer is the reaction product of at least one isocyanate and a hydrosilylated polymer. The hydrosilylated polymer is the reaction product of a polymer having at least one unsaturated group and at least one alcoholic group in each molecule and a compound having a hydrogen-silicon bond and a crosslinkable silyl group in each molecule. The copolymer-filled crosslinkable silane-terminated polymers exhibit improved modulus and tensile strength properties while maintaining elongation properties.
摘要翻译：提供了在每个分子中具有至少一个可交联甲硅烷基的共聚物填充的可交联硅烷封端的聚合物。共聚物填充的可交联硅烷封端的聚合物是共聚物填充的多元醇和异氰酸酯封端的氢化硅烷化聚合物的反应产物。异氰酸酯封端的氢化硅烷化聚合物是至少一种异氰酸酯和氢化硅烷化聚合物的反应产物。氢化硅烷化聚合物是在每个分子中具有至少一个不饱和基团和至少一个醇基的聚合物的反应产物和在每个分子中具有氢 - 硅键和交联性甲硅烷基的化合物。共聚物填充的可交联硅烷封端的聚合物在保持伸长性能的同时表现出改善的模量和拉伸强度性能。

6. 发明申请

WO2009009654A1 ROOM TEMPERATURE CURABLE POLYMERS AND PRECURSORS THEREOF 审中-公开
标题翻译：室温可固化聚合物及其前身
公开(公告)号：WO2009009654A1
公开(公告)日：2009-01-15
申请号：PCT/US2008/069634
申请日：2008-07-10
申请人： DOW GLOBAL TECHNOLOGIES INC. , POPA, Paul , LYSENKO, Zenon , BABB, David , KOONCE, William , SPILMAN, Gary
发明人： POPA, Paul , LYSENKO, Zenon , BABB, David , KOONCE, William , SPILMAN, Gary
IPC分类号： C08G18/42 , C08G18/71 , C09J175/06
CPC分类号： C08G18/4288 , C08G18/4269 , C08G18/4277 , C08G18/718 , C08G2190/00 , C09J175/06
摘要： A polyester polyol, referred to hereinafter as a MHMS polyol comprises fatty acid based mer units wherein at least about 80 weight percent of the fatty acid based mer units are from methyl 9 (10) hydroxymethylstearate, or is prepared from an oil having fatty acids or fatty acid esters which are at least about 80 weight percent oleic acid or esters thereof and which has an average hydroxyl functionality of from 1.5 to 4. A reaction product, referred to herein after as MHMS alkoxysilane prepolymer, is produced from at least one such MHMS polyol and at least one isocyanate functional silane. The prepolymer is moisture cured to form a silylated MHMS polymer. The process of preparing a MHMS polyol comprises (A) reacting a fatty acid ester wherein at least about 80 weight percent of the fatty acid esters are methyl 9 (10) hydroxymethylstearate, or are prepared from an oil having fatty acids or fatty acid esters which are at least about 80 weight percent oleic acid or esters thereof with an initiator having at least 2 reactive groups selected from primary hydroxyl groups, amine groups, terminal isocyanate groups, terminal carbonyl groups or a combination thereof. The process of preparing at least one MHMS alkoxysilane prepolymer comprises steps of: (a) supplying at least one MHMS polyol; (b) supplying at least one isocyanate functional silane and (c) admixing the MHMS polyol and isocyanate functional silane or combination thereof, optionally in the presence of at least one catalyst to produce at least one MHMS alkoxysilane prepolymer. A process of preparing at least one silylated MHMS polymer comprises steps of: (a) supplying at least one MHMS alkoxysilane prepolymer; and (b) exposing it to moisture under conditions such that at least one silylated MHMS polymer is formed. Articles comprising the polyol, prepolymer, or polymer include elastomers, sealants, adhesives, coatings and the like.
摘要翻译：以下称为MHMS多元醇的聚酯多元醇包括脂肪酸基mer单元，其中至少约80重量％的脂肪酸基mer单元为9（10）羟甲基硬脂酸甲酯，或由具有脂肪酸或至少约80重量％的油酸或其酯的脂肪酸酯，其平均羟基官能度为1.5-4。本文以下称为MHMS烷氧基硅烷预聚物的反应产物由至少一种这样的MHMS 多元醇和至少一种异氰酸酯官能的硅烷。将预聚物水分固化以形成甲硅烷基化的MHMS聚合物。制备MHMS多元醇的方法包括（A）脂肪酸酯，其中至少约80重量％的脂肪酸酯是甲基9（10）羟甲基硬脂酸酯，或由具有脂肪酸或脂肪酸酯的油制备，至少约80重量％的油酸或其酯与具有至少2个选自伯羟基，胺基，末端异氰酸酯基，末端羰基或其组合的反应性基团的引发剂。制备至少一种MHMS烷氧基硅烷预聚物的方法包括以下步骤：（a）供应至少一种MHMS多元醇; （b）提供至少一种异氰酸酯官能的硅烷和（c）任选地在至少一种催化剂的存在下混合MHMS多元醇和异氰酸酯官能的硅烷或其组合以产生至少一种MHMS烷氧基硅烷预聚物。制备至少一种甲硅烷基化MHMS聚合物的方法包括以下步骤：（a）供应至少一种MHMS烷氧基硅烷预聚物; 和（b）在形成至少一种甲硅烷基化的MHMS聚合物的条件下将其暴露于水分。包含多元醇，预聚物或聚合物的制品包括弹性体，密封剂，粘合剂，涂料等。

7. 发明申请

WO2006002131A1 POLYURETHANE COMPOSITIONS WITH GLASS FILLER AND METHOD OF MAKING SAME 审中-公开
标题翻译：具有玻璃填料的聚氨酯组合物及其制备方法
公开(公告)号：WO2006002131A1
公开(公告)日：2006-01-05
申请号：PCT/US2005/021864
申请日：2005-06-17
申请人： DOW GLOBAL TECHNOLOGIES INC. , JENKINES, Randall, C. , KOONCE, William, A. , MOBLEY, Larry, W.
发明人： JENKINES, Randall, C. , KOONCE, William, A. , MOBLEY, Larry, W.
IPC分类号： C08J5/00
CPC分类号： C08K3/40 , C08J5/00 , C08J2375/04 , D06N7/0073 , D06N7/0086 , D06N2203/068 , D06N2205/08 , D06N2205/10 , Y10T428/249921 , Y10T428/25 , Y10T428/252 , C08L75/04
摘要： The method forms a polyurethane article and involves dispersing polyurethane particles in a substantially aqueous liquid, mixing in a fine glass filler such as a post-consumer ground soda-lime glass, casting the filled dispersion and coalescing the particles by removing the liquid such that a polyurethane article having fused particles are formed. The polyurethane articles are useful as carpet backings.
摘要翻译：该方法形成聚氨酯制品，并且涉及将聚氨酯颗粒分散在基本上含水的液体中，在细玻璃填料如消费后研磨的钠钙玻璃中混合，浇注填充的分散体并通过除去液体使颗粒聚结，使得形成具有熔融颗粒的聚氨酯制品。聚氨酯制品可用作地毯背衬。

8. 发明申请

WO2005085311A1 IMPROVED POLYURETHANE DISPERSIONS AND COATINGS MADE THEREFROM 审中-公开
标题翻译：改进的聚氨酯分散体和涂层
公开(公告)号：WO2005085311A1
公开(公告)日：2005-09-15
申请号：PCT/US2005/006348
申请日：2005-02-28
申请人： DOW GLOBAL TECHNOLOGIES INC. , KOONCE, William, A. , BHATTACHARJEE, Debkumar , KAUL, Surendar, N.
发明人： KOONCE, William, A. , BHATTACHARJEE, Debkumar , KAUL, Surendar, N.
IPC分类号： C08G18/08
CPC分类号： C08G18/0866 , C08K5/04 , C08K5/21 , C08L75/04
摘要： A polyurethane having enhanced properties is made from an aqueous polyurethane dispersion having therein a nonvolatile, non-reactive, property enhancing water-soluble (NNPEW) compound such as urea. Even though the NNPEW is soluble in water, the NNPEW remains in the polyurethane after being exposed to water. In another embodiment, the NNPEW may react with a compound present in the dispersion other than the polyurethane particles of the dispersion when removing the water of the dispersion to form the polyurethane or upon subsequent heating.
摘要翻译：具有增强性能的聚氨酯由其中具有不挥发性，非反应性，性能增强水溶性（NNPEW）化合物如尿素的水性聚氨酯分散体制成。即使NNPEW溶于水，NNPEW在暴露于水中后仍保留在聚氨酯中。在另一个实施方案中，当除去分散体的水以形成聚氨酯或随后加热时，NNPEW可与分散体中除了分散体的聚氨酯颗粒之外的化合物反应。

9. 发明申请

WO2013003051A3 SILANE TERMINATED POLYCARBONATE-POLYESTER COPOLYMERS FOR COATING, ADHESIVES, SEALANT AND ELASTOMER APPLICATIONS 审中-公开
标题翻译：用于涂料，粘合剂，密封剂和弹性体应用的硅烷端基聚碳酸酯 - 聚酯共聚物
公开(公告)号：WO2013003051A3
公开(公告)日：2013-06-06
申请号：PCT/US2012042357
申请日：2012-06-14
申请人： DOW GLOBAL TECHNOLOGIES LLC , VYAKARANAM KAMESH R , SINGH HARPREET , ZHANG LING , HEATH WILLIAM H , SINGH AMARNATH , KOONCE WILLIAM A
发明人： VYAKARANAM KAMESH R , SINGH HARPREET , ZHANG LING , HEATH WILLIAM H , SINGH AMARNATH , KOONCE WILLIAM A
IPC分类号： C08G18/42 , C08G63/64 , C08G63/91 , C09J175/06
CPC分类号： C08G63/64 , C08G18/44 , C08G18/809 , C08G63/695 , C08G63/91 , C09D169/00 , C09D175/04 , C09J169/00 , C09J175/04
摘要： Crosslinkable silyl group-containing polymers that may be made using polycarbonate-polyester copolymer polyols and methods for making the same are provided. The crosslinkable silane-terminated polymer is the reaction product of a polycarbonate-polyester copolymer polyol and an isocyanate capped hydrosilylated polymer. The isocyanate capped hydrosilylated polymer is the reaction product of at least one isocyanate and a hydrosilylated polymer. The hydrosilylated polymer is the reaction product of a polymer having at least one unsaturated group and at least one alcohol hydroxyl group in each molecule and a compound having a hydrogen-silicon bond and a crosslinkable silyl group in each molecule. The crosslinkable silane-terminated polymer exhibits improved viscosity properties, UV stability and weatherability.
摘要翻译：提供了可使用聚碳酸酯 - 聚酯共聚物多元醇制备的含交联性甲硅烷基的聚合物及其制备方法。可交联硅烷封端的聚合物是聚碳酸酯 - 聚酯共聚物多元醇和异氰酸酯封端的氢化硅烷化聚合物的反应产物。异氰酸酯封端的氢化硅烷化聚合物是至少一种异氰酸酯和氢化硅烷化聚合物的反应产物。氢化硅烷化聚合物是每个分子中具有至少一个不饱和基团和至少一个醇羟基的聚合物与每个分子中具有氢 - 硅键和可交联甲硅烷基的化合物的反应产物。可交联的硅烷封端的聚合物表现出改进的粘度性质，UV稳定性和耐候性。

10. 发明申请

WO2011150161A3 METHODS FOR PRODUCING CROSSLINKABLE SILYL GROUP-CONTAINING POLYOXYALKYLENE POLYMERS. 审中-公开
标题翻译：用于生产可交联含硅烷基的聚氧乙烯聚合物的方法。
公开(公告)号：WO2011150161A3
公开(公告)日：2012-07-19
申请号：PCT/US2011038065
申请日：2011-05-26
申请人： DOW GLOBAL TECHNOLOGIES LLC , ZHANG LING , AGUILAR DANIEL , BHATTACHARJEE DEBKUMAR , KOONCE WILLIAM , SAHA BASUDEB
发明人： ZHANG LING , AGUILAR DANIEL , BHATTACHARJEE DEBKUMAR , KOONCE WILLIAM , SAHA BASUDEB
IPC分类号： C08G65/26 , C08G18/28 , C08G65/336
CPC分类号： C08G65/336 , C08G18/289 , C08G18/7664 , C08G65/2663
摘要： Embodiments of the invention provide for a method of producing a silylated polyoxyalkylene polymer having at least one crosslinkable silyl group and at least one hydroxyl group in each molecule. The method comprises providing a polyoxyalkylene polymer having at least one unsaturated group and at least one alcoholic hydroxyl group in each molecule, wherein the polyoxyalkylene polymer includes an impurity double metal cyanide complex mixed therein, and wherein the polyoxyalkylene polymer has not been treated with a metal-coordinating compound; and adding to the polyoxyalkylene polymer a compound having a hydrogen-silicon bond and a crosslinkable silyl group in each molecule and a hydrosilylation catalyst to thereby carry out a hydrosilylation reaction, wherein the hydrosilyation reaction is performed in an absence of a metal-coordinating compound.
摘要翻译：本发明的实施方案提供了在每个分子中具有至少一个交联性甲硅烷基和至少一个羟基的甲硅烷基化聚氧化烯聚合物的制备方法。该方法包括提供在每个分子中具有至少一个不饱和基团和至少一个醇羟基的聚氧化烯聚合物，其中所述聚氧化烯聚合物包含混合在其中的杂质双金属氰化物络合物，并且其中所述聚氧化烯聚合物未被金属处理配位化合物并且在每个分子中加入具有氢硅键和交联性甲硅烷基的化合物和氢化硅烷化催化剂，从而进行氢化硅烷化反应，其中在没有金属配位化合物的情况下进行氢化反应。

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