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1. 发明申请

WO1998029575A1 METHOD FOR VACUUM/REDUCED-PRESSURE REFINING AND FACILITY FOR VACUUM/REDUCED-PRESSURE REFINING 审中-公开
标题翻译：用于真空/降低压力精炼的真空/降低压力精炼方法
公开(公告)号：WO1998029575A1
公开(公告)日：1998-07-09
申请号：PCT/JP1997004823
申请日：1997-12-25
申请人： NIPPON STEEL CORPORATION , SHIMOMURA, Kensuke , SADACHIKA, Masaru , TAKANO, Hironori , OGAWA, Gaku , ABE, Kenji , OKIMORI, Mayumi , MAKINO, Nobuyuki , IWASAKI, Hiroshi , TANAKA, Tomoaki , MORISHIGE, Hiroaki
发明人： NIPPON STEEL CORPORATION
IPC分类号： C21C07/10
CPC分类号： C21C7/10 , C21C5/28
摘要： Problem: dust collection in a vacuum/reduced-pressure refining process is conducted using an inexpensive filter without causing damage on and burn of the filter. Solving means: a vacuum/reduced-pressure refining vessel (1), a dry type dust collector (3) using a filter (2) and a reduced-pressure exhaust device (4) are connected sequentially by an upstream-side duct (5) and a downstream-side duct (6), and a gate valve (7) is provided to the upstream-side duct (5). At the time of starting the vaccum/reduced-pressure refining process, non-oxidizing gas is fed into the upstream side of the gate valve (7) and oxygen on the upstream side is replaced thereby substantially. Thereafter, the upstream side is closed gastightly, the gate valve (7) is opened after the closed state on the upstream side is accomplished, and the dust collector (3) is operated. It is preferable that after the vacuum/reduced-pressure refining process the gate valve (7) is closed, only the non-oxidizing gas is fed into the upstream side of the valve to recover the pressure, and then the vessel is opened to the atmosphere, and it is also preferable that after the vacuum/reduced-pressure refining process, an opening part on the duct collector (3) side is closed during the standby till the subsequent vacuum/reduced-pressure refining process is started.
摘要翻译：问题：使用便宜的过滤器进行真空/减压精炼过程中的灰尘收集，而不会损坏和燃烧过滤器。解决方法：使用过滤器（2）和减压排气装置（4）的真空/减压精炼容器（1），干式集尘器（3），依次由上游侧管道（5））和下游侧管道（6），并且闸门（7）设置在上游侧管道（5）上。在开始真空/减压精炼过程时，非氧化性气体被进料到闸阀（7）的上游侧，并且上游侧的氧气基本上被替换。此后，上游侧气密地关闭，在上游侧的关闭状态完成之后，闸阀（7）打开，并且集尘器（3）被操作。优选的是，在真空/减压精炼处理之后，闸阀（7）关闭，只有非氧化气体被供给到阀的上游侧以回收压力，然后将容器打开至气氛中，优选在真空/减压精制处理之后，在待机状态下，在收集器（3）侧的开口部分被关闭，直到开始后续的真空/减压精制处理。

2. 发明申请

WO1994010115A1 PROCESS FOR PRODUCING AROMATIC HYDROXYLIC COMPOUND 审中-公开
标题翻译：生产芳香羟基化合物的方法
公开(公告)号：WO1994010115A1
公开(公告)日：1994-05-11
申请号：PCT/JP1993001586
申请日：1993-11-01
申请人： MITSUI PETROCHEMICAL INDUSTRIES, LTD. , ARAKI, Shintaro , IWASAKI, Hiroshi , OHNO, Hiroyasu , HASHIMOTO, Isao , MUKAIYAMA, Teruaki
发明人： MITSUI PETROCHEMICAL INDUSTRIES, LTD.
IPC分类号： C07C39/04
CPC分类号： C07C37/08 , Y02P20/52 , C07C39/04 , C07C39/07 , C07C39/08
摘要： A process for producing an aromatic hydroxylic compound represented by the general formula Ar-(OH)n (wherein Ar represents an n-valent aromatic hydrocarbon group; and n represents an integer of 1 or 2), by the acidic decomposition of a hydroperoxide represented by general formula (I); (wherein Ar and n are each as defined above) in the presence of an acid catalyst selected from among tetrafluoroboric, hexafluorosilicic and hexafluorophosphoric acids. The process enables an aromatic hydroxyclic compound to be produced in a high yield while suppressing the formation of hydroxy-acetone as a by-product. An effective suppression of the by-product formation and a higher yield of the target compound can be achieved by conducting the acidic decomposition in two stages, i.e. the first stage wherein the reaction is conducted in the first reactor at a temperature of 50-95 DEG C and the resulting reaction mixture is sent to the second reactor, and the second stage wherein the reaction is conducted at a temperature of 80-120 DEG C.
摘要翻译：由通式Ar-（OH）n（其中Ar表示n价的芳香族烃基，n表示1或2的整数）表示的芳香族羟基化合物的制造方法，通过表示的氢过氧化物的酸性分解通式（I）; （其中Ar和n各自如上所定义）在选自四氟硼酸，六氟硅酸和六氟磷酸的酸催化剂存在下反应。该方法能够以高产率制备芳族羟基化合物，同时抑制作为副产物的羟基 - 丙酮的形成。可以通过两步进行酸性分解来实现副产物形成的有效抑制和目标化合物的较高产率，即其中反应在第一反应器中在50-95℃的温度下进行的第一阶段并将所得反应混合物送至第二反应器，其中反应在80-120℃的温度下进行。

3. 发明申请

WO1991017007A1 HORIZONTAL CONTINUOUS CASTING METHOD AND APPARATUS THEREFOR 审中-公开
标题翻译：水平连续铸造方法及其设备
公开(公告)号：WO1991017007A1
公开(公告)日：1991-11-14
申请号：PCT/JP1991000613
申请日：1991-05-09
申请人： NIPPON STEEL CORPORATION , MATSUSHIMA, Tatsuhito , SAITA, Seishiro , INOUE, Masayuki , NAKASHIMA, Hiroyuki , MATSUMURA, Shogo , IWASAKI, Hiroshi , HANZAWA, Ryuzo , KAWAMOTO, Katsuhiko , OHGURO, Haruo , MORIMOTO, Yukio , KOSUGE, Toshihiro
发明人： NIPPON STEEL CORPORATION
IPC分类号： B22D11/04
CPC分类号： B22D11/047
摘要： A horizontal continuous casting method for preventing defects in casting such as blow-holes of an ingot piece in horizontal continuous casting, and an apparatus therefor. An object of the present invention is to prevent the intrusion of gas at about the inlet of a mold (1) and the connecting portion of the mold (1) into the mold (1) and prevent the occurrence of defects in casting such as blow-holes of the ingot piece, and seal the inlet of the mold (1) simultaneously with the connection of a tundish (10) to the mold (1) in the horizontal continuous casting apparatus wherein one of the tundish (10) and the mold (1) is made movable. The horizontal continuous casting method according to the present invention is characterized in that, in the horizontal continuous casting apparatus wherein a feed nozzle (3) is connected to the mold (1) through a break ring (2) in a direction of drawing the ingot piece, a shielding means (7) is provided between the feed nozzle (3) and the mold (1) and the casting is carried out in a state where a spatial portion (6) inside the shielding means is reduced in pressure.

4. 发明申请

WO2004027408A1 LICHTQUELLE FÜR EIN MESSSYSTEM MIT PHOTOEMPFINDLICHER ELEKTRODE ZUM NACHWEIS EINES ODER MEHRERER ANALYTEN 审中-公开
标题翻译：光源，用于测量与感光电极系统用于一种或多种分析物检测
公开(公告)号：WO2004027408A1
公开(公告)日：2004-04-01
申请号：PCT/DE2003/002952
申请日：2003-09-05
申请人： FORSCHUNGSZENTRUM JÜLICH GMBH , SCHÖNING, Michael, Josef , OTTO, Ralph , YOSHINOBU, Tatsuo , IWASAKI, Hiroshi
发明人： SCHÖNING, Michael, Josef , OTTO, Ralph , YOSHINOBU, Tatsuo , IWASAKI, Hiroshi
IPC分类号： G01N27/30
CPC分类号： G01N27/305
摘要： Die Erfindung betrifft eine Lichtquelle (2) für ein Meßsystem mit photoempfindlicher Elektrode (3) zum Nachweis eines oder mehrerer Analyten. Die Lichtquelle (2) weist Mittel zur lokalen Beleuchtung der photoempfindlichen Elektrode (3) auf. Als Mittel sind insbesondere gekrümmte optische Fasern (42) oder drehbare Lochscheiben (32) vorgesehen, die zur lokalen Beleuchtung der photoempfindlichen Elektrode (3) dienen. Dadurch kann vorteilhaft auf die Verwendung komplex gesteuerter Beleuchtungsarrays zur lokalen Beleuchtung der photoempfindlichen Elektrode (3) verzichtet werden. Dadurch wird das Meßsystem tragbar und miniaturiesierbar. Es ist vorstellbar, solche Lichtquellen (2) generell in Sensoren oder Mikroskopen, insbesondere in Mikroskopen, z. B. in Rastersondenmikroskopen einzusetzen.
摘要翻译：本发明涉及一种光源（2），用于与感光电极（3）的测量系统用于检测一种或多种分析物。所述光源（2）具有用于将感光电极（3）的局部照明装置。为平均值弯曲光纤（42）或旋转穿孔盘（32），特别是被提供，其用于对感光电极（3）的局部照明。这消除了需要使用复杂有利地控制照明阵列的光敏电极（3）的局部照明。因此，测量系统是便携式的并且miniaturiesierbar。可以设想，这样的光源（2）通常在传感器或显微镜，特别是显微镜，Z。 B.在扫描探针显微镜使用。

5. 发明申请

WO1998011047A1 METHOD FOR PURIFYING CRUDE NAPHTHALENEDICARBOXYLIC ACID AND PROCESS FOR PREPARING POLYETHYLENE NAPHTHALATE 审中-公开
标题翻译：净化萘二甲酸的方法和制备聚萘二甲酸乙二醇酯的方法
公开(公告)号：WO1998011047A1
公开(公告)日：1998-03-19
申请号：PCT/JP1997003129
申请日：1997-09-05
申请人： MITSUI CHEMICALS, INC. , IWASAKI, Hiroshi , INOKI, Satoshi , UEKI, Hiromi
发明人： MITSUI CHEMICALS, INC.
IPC分类号： C07C51/493
CPC分类号： C08G63/78 , C07C51/493 , C07C67/60 , C08G63/189 , C07C63/38 , C07C69/76
摘要： A method for preparing polyethylene naphthalate having a low impurity content from a naphthalenedicarboxylic acid containing impurities, which comprises mixing a crude naphthalenedicarboxylic acid with an aqueous ethylene glycol solution, heating the mixture to esterify a part of the naphthalenedicarboxylic acid to prepare a naphthalenedicarboxylic ester, dissolving the naphthalenedicarboxylic ester in the aqueous ethylene glycol solution, bringing hydrogenatable impurities contained in the crude naphthalenedicarboxylic acid into contact with hydrogen in the presence of a hydrogenation catalyst to hydrogenate the impurities to thereby dissolve the same in the aqueous ethylene glycol solution, crystallizing the naphthalenedicarboxylic ester, separating the crystallized naphthalenedicarboxylic ester from the aqueous ethylene glycol solution, and polycondensating the resultant naphtalenedicarboxylic ester. A method for purifying a crude naphtalenedicarboxylic acid to obtain a naphthalenedicarboxylic acid and a naphthalenedicarboxylic ester each having a low aldehyde content from a naphthalenedicarboxylic acid containing aldehydes, which comprises mixing a crude naphthalenedicarboxylic acid with an aqueous alcohol solution, heating the mixture to esterify a part of the naphthalenedicarboxylic acid to prepare a naphthalenedicarboxylic ester, dissolving the naphthalenedicarboxylic ester in the aqueous alcohol solution, bringing the aldehydes contained in the crude naphthalenedicarboxylic acid into contact with a salt of sulfurous acid to prepare an aldehyde adduct, dissolving the aldehyde adduct in an aqueous alcohol solution, and crystallizing and separating the naphthalenedicarboxylic acid and the naphthalenedicarboxylic ester.
摘要翻译：一种从含有杂质的萘二甲酸制备杂质含量低的聚萘二甲酸乙二醇酯的方法，其包括将粗萘二甲酸与乙二醇水溶液混合，加热该混合物以酯化一部分萘二甲酸以制备萘二甲酸酯，溶解乙二醇水溶液中的萘二甲酸酯，使粗萘二羧酸中含有的可氢化杂质在氢化催化剂存在下与氢接触，氢化杂质，从而将其溶解在乙二醇水溶液中，使萘二羧酸酯结晶从乙二醇水溶液中分离结晶的萘二甲酸酯，并使所得的萘二甲酸酯缩聚。一种纯化粗萘二甲酸以从萘醛二羧酸含醛中分离醛含量低的萘二甲酸和萘二羧酸的方法，该方法包括将粗萘二甲酸与醇水溶液混合，加热混合物以酯化部分的萘二甲酸以制备萘二羧酸酯，将萘二甲酸酯溶解在醇水溶液中，使粗萘二羧酸中所含的醛与亚硫酸盐接触以制备醛加合物，将醛加合物溶解在水醇溶液，并结晶并分离萘二甲酸和萘二甲酸酯。

6. 发明申请

WO2004027407A1 MESSSYSTEM MIT PHOTOEMPFINDLICHER ELEKTRODE 审中-公开
标题翻译：有照片感应电极测量系统
公开(公告)号：WO2004027407A1
公开(公告)日：2004-04-01
申请号：PCT/DE2003/002951
申请日：2003-09-05
申请人： FORSCHUNGSZENTRUM JÜLICH GMBH , SCHÖNING, Michael, Josef , OTTO, Ralph , YOSHINOBU, Tatsuo , IWASAKI, Hiroshi
发明人： SCHÖNING, Michael, Josef , OTTO, Ralph , YOSHINOBU, Tatsuo , IWASAKI, Hiroshi
IPC分类号： G01N27/30
CPC分类号： G01N27/305
摘要： Die Erfindung betrifft ein tragbares Messsystem zum Nachweis eines oder mehrerer .Analyten, umfassend einen Behälter (1) und eine photempfindliche Elektrode (3) sowie eine oder mehrere Lichtquellen (2). Das Messsystem ist dadurch gekennzeichnet, daß die Lichtquelle (2) oder die Lichtquellen (2) innerhalb des Behälters (1) angeordnet sind. Dies führt zu einem kompakten, kleinen und modular aufgebauten Messsystem. Vorteilhaft ist die photoempfindliche Elektrode (3) als Teil der Wand des Behälters (1) in dieser angeordnet.
摘要翻译：本发明涉及一种便携式测量系统，用于检测一个或多个.Analyten包括容器（1）和一个photempfindliche电极（3）和一个或多个光源（2）。该测量系统的特征在于，所述光源（2）或容器（1）内的光源（2）被布置。这导致在一个紧凑，小型模块化测量系统。光敏电极（3）是有利的，因为设置在其中的容器（1）的壁的一部分。

7. 发明申请

WO0235219A3 MEASURING DEVICE FOR DETECTING ONE-DIMENSIONAL OR MULTIDIMENSIONAL DISTRIBUTION OF A CHEMICAL OR BIOCHEMICAL COMPONENT 审中-公开
标题翻译：测量器具，用于检测单或多维分布化学或生化成分
公开(公告)号：WO0235219A3
公开(公告)日：2002-12-19
申请号：PCT/DE0103980
申请日：2001-10-23
申请人： FORSCHUNGSZENTRUM JUELICH GMBH , SCHOENING MICHAEL JOSEF , POGHOSSIAN ARSHAK , LUETH HANS , YOSHINOBU TATSUO , IWASAKI HIROSHI
发明人： SCHOENING MICHAEL JOSEF , POGHOSSIAN ARSHAK , LUETH HANS , YOSHINOBU TATSUO , IWASAKI HIROSHI
IPC分类号： G01N27/00 , G01N27/30
CPC分类号： G01N27/002
摘要： The invention relates to a measuring device for one-dimensional or multidimensional detection of chemical or biological components (analytes). A photosensitive contact is applied to a semiconductor structure and the modification of the potential barrier of the contact upon illumination is used as a functional principle, thereby avoiding all stated disadvantages of prior art, while at the same time guaranteeing two-dimensional local resolution of the analyte substance to be detected by means of a sensor.
摘要翻译：当施加用于化学或生物组分（分析物）上的半导体层结构的感光性接触的一个维或二维检测根据本发明的测量装置和所利用的接触的势垒的照明作为原则功能期间的变化。因此，所有上述缺点都可避免与现有技术定期，同时仍然要被检测的分析物的二维空间分辨率由传感器来保证。

8. 发明申请

WO1997044307A1 NAPHTHALENEDICARBOXYLIC ACID PARTICLES AND PROCESS FOR THE PRODUCTION THEREOF 审中-公开
标题翻译：萘二甲酸钠颗粒及其生产方法
公开(公告)号：WO1997044307A1
公开(公告)日：1997-11-27
申请号：PCT/JP1997001619
申请日：1997-05-14
申请人： MITSUI CHEMICALS, INC. , IWASAKI, Hiroshi , INOKI, Satoshi
发明人： MITSUI CHEMICALS, INC.
IPC分类号： C07C63/38
CPC分类号： C08G63/189 , C07C51/09 , C07C63/38
摘要： Naphthalenedicarboxylic acid (NDA) particles excellent in fluidity in slurry state, which can be produced by heating a mixture comprising naphthalenedicarboxylic acid and/or ester, an alcohol and water to prepare a solution in water/alcohol, lowering the alcohol concentration of the solution to hydrolyze the ester, precipitating naphthalenedicarboxylic acid particles, and recovering the particles.
摘要翻译：可以通过加热包含萘二甲酸和/或酯，醇和水的混合物来制备在水/醇中的溶液，从而将溶液的醇浓度降低到溶液状态的流动性优异的萘二甲酸（NDA）水解酯，沉淀萘二甲酸颗粒，并回收颗粒。

9. 发明申请

WO1997017391A1 PROCESS FOR PRODUCING POLYETHYLENE NAPHTHALATE 审中-公开
标题翻译：生产聚乙烯亚麻酸的方法
公开(公告)号：WO1997017391A1
公开(公告)日：1997-05-15
申请号：PCT/JP1996003116
申请日：1996-10-25
申请人： MITSUI PETROCHEMICAL INDUSTRIES, LTD. , IWASAKI, Hiroshi , ISHIBASHI, Masayasu , UEKI, Hiromi , HIRAOKA, Shoji , MATSUYOSHI, Toru , INOKI, Satoshi
发明人： MITSUI PETROCHEMICAL INDUSTRIES, LTD.
IPC分类号： C08G63/189
CPC分类号： C08G63/189 , C08G63/78 , C08G63/82
摘要： In the production of polyethylene naphthalate of the present invention, the esterification reaction between naphthalenedicarboxylic acid and ethylene glycol is conducted while causing water to be present in a reaction system from a start of reaction, in the presence of at least one catalyst selected from the group consisting of nitric, carboxylic, phosphoric and hydrogenphosphoric salts and amines according to necessity, to thereby attain an esterification ratio of 45 to 80 %, so that a liquid mixture of naphthalenedicarboxylic acid esterification reaction products containing naphthalenedicarboxylic acid, carboxyl-hydroxyethoxycarbonylnaphthalene and bis(hydroxyethoxycarbonyl)naphthalene is obtained. Subsequently, a crystal is separated from this liquid mixture to thereby obtain a mixture of esterification reaction products. Thereafter, this mixture having ethylene glycol added thereto according to necessity is subjected to polycondensation. The polyethylene naphthalate obtained by the process of the present invention ensures a low content of naphthalenedicarboxylic acid esters each having diethylene glycol skeleton therein, thereby having excellent quality, for example, in appearance.
摘要翻译：在本发明的聚萘二甲酸乙二醇酯的制造中，萘二甲酸与乙二醇之间的酯化反应是在反应开始时在反应体系中存在的条件下，在至少一种选自根据需要由硝酸，羧酸，磷酸和氢磷酸盐和胺组成，由此达到45-80％的酯化比例，使得含萘二羧酸，羧基 - 羟基乙氧基羰基萘和双（羟基乙氧基羰基）的萘二羧酸酯化反应产物的液体混合物）萘。随后，从该液体混合物中分离出晶体，从而得到酯化反应产物的混合物。此后，根据需要将具有乙二醇的混合物进行缩聚。通过本发明的方法获得的聚萘二甲酸乙二醇酯确保了各自具有二甘醇骨架的萘二羧酸酯含量低，因此具有优异的外观质量。

10. 发明申请

WO1997017318A1 METHOD FOR PURIFYING CRUDE NAPHTHALENEDICARBOXYLIC ACID 审中-公开
标题翻译：净化萘二甲酸的方法
公开(公告)号：WO1997017318A1
公开(公告)日：1997-05-15
申请号：PCT/JP1996003180
申请日：1996-10-30
申请人： MITSUI PETROCHEMICAL INDUSTRIES, LTD. , IWASAKI, Hiroshi , HIROKANE, Nobuya , ISHIBASHI, Masayasu , INOKI, Satoshi
发明人： MITSUI PETROCHEMICAL INDUSTRIES, LTD.
IPC分类号： C07C63/38
CPC分类号： C07C51/487 , C07C63/38
摘要： The invention provides a method for purifying a crude naphthalenedicarboxylic acid comprising the steps of mixing a crude naphthalenedicarboxylic acid and a water/alcohol solvent to esterify a part of the naphthalenedicarboxylic acid, thereby dissolving a naphthalenedicarboxylic ester into the solvent, and then contacting the resulting reaction mixture with hydrogen in the presence of a hydrogenation catalyst to hydrogenate impurities which are contained in the crude naphthalenedicarboxylic acid and which are capable of being hydrogenated, thereby dissolving and removing hydrogenation products into the water/methanol solvent. A mixture of a naphthalenedicarboxylic acid and a naphthalendicarboxylic ester with reduced impurity contents, or a high-purity naphthalenedicarboxylic acid can be obtained.
摘要翻译：本发明提供纯化粗萘二甲酸的方法，包括将粗萘二甲酸和水/醇溶剂混合以酯化一部分萘二甲酸，从而将萘二甲酸酯溶解到溶剂中，然后使所得反应与氢气在氢化催化剂存在下与氢气混合，氢化粗萘二甲酸中含有的杂质，能够被氢化，从而将氢化产物溶解并除去到水/甲醇溶剂中。可以获得具有降低的杂质含量的萘二甲酸和萘二甲酸酯的混合物或高纯度萘二甲酸。

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