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61. 发明申请

WO2003018518A1 PROCESS TO BROMOMETHYLATE AROMATIC COMPOUNDS 审中-公开
标题翻译：溴甲酰化芳族化合物的方法
公开(公告)号：WO2003018518A1
公开(公告)日：2003-03-06
申请号：PCT/IL2001/000814
申请日：2001-08-29
申请人： MAKHTESHIM CHEMICAL WORKS LTD. , GRABARNICK, Michael , SASSON, Yoel
发明人： GRABARNICK, Michael , SASSON, Yoel
IPC分类号： C07C17/32
CPC分类号： C07F9/4028 , C07B37/04 , C07C17/32 , C07C41/22 , C07C43/123 , C07C2527/125 , C07C2527/135 , C07C2527/138 , C07C22/04
摘要： The present invention provides a process for bromomethylation of organic compounds, wherein said process is a two stage process comprising of the following stages: a) reacting paraformaldehyde with hydrogen bromide and separating bis-bromomethyl ether (BBME) from the reaction mixture, and, b) reacting BBME obtained in stage (a) with an organic compound in the presence of a Lewis acid, to obtain the bromomethylated organic compound. Further provided by the present invention is a process for the preparation of 4,4'-bis-(diethylphosphonomethyl)-biphenyl (BPMB).
摘要翻译：本发明提供一种有机化合物的溴甲基化方法，其中所述方法是包括以下步骤的两步方法：a）使多聚甲醛与溴化氢反应并从反应混合物中分离双溴甲基醚（BBME），和b ）使在步骤（a）中获得的BBME与路易斯酸存在下的有机化合物反应，得到溴甲基化的有机化合物。本发明还提供了制备4,4'-双（二乙基膦酰基甲基） - 联苯（BPMB）的方法。

62. 发明申请

WO02022525A1 FLUORINATION METHOD 审中-公开
标题翻译：荧光法
公开(公告)号：WO02022525A1
公开(公告)日：2002-03-21
申请号：PCT/GB2001/004028
申请日：2001-09-10
IPC分类号： C07B39/00 , C07C17/12 , C07C41/22 , C07C43/192 , C07C43/225 , C07C45/30 , C07C49/697
CPC分类号： C07C17/12 , C07B39/00 , C07C41/22 , C07C43/225
摘要： A process is provided for the fluorination of an aromatic fused ring compound which comprises treating the compound with fluorine. A preferred process involves treating a solution of a naphthalene compound in an inert solvent with elemental fluorine, preferably comprised in a gas stream and diluted with an inert gas. The process provides a convenient and simple method by which fluorinated derivatives may be prepared with a high degree of specificity and shows improved yields over methods known from the prior art.
摘要翻译：提供用于氟化芳族稠合环化合物的方法，其包括用氟处理该化合物。优选的方法包括用惰性溶剂中的萘化合物在元素氟中处理溶液，优选包含在气流中并用惰性气体稀释。该方法提供了一种方便和简单的方法，通过该方法可以以高度的特异性制备氟化衍生物，并且与现有技术中已知的方法相比显示出提高的产率。

63. 发明申请

WO0117931A2 REGENERATION OF ONIUM FLUORIDE-HF ADDUCTS 审中-公开
标题翻译：再生鎓氟化物HF加合物
公开(公告)号：WO0117931A2
公开(公告)日：2001-03-15
申请号：PCT/EP0008396
申请日：2000-08-29
申请人： SOLVAY FLUOR & DERIVATE , BRAUN MAX , PALSHERM STEFAN
发明人： BRAUN MAX , PALSHERM STEFAN
IPC分类号： B01J31/02 , B01J31/40 , B01J38/42 , C01B7/19 , C01B17/45 , C07B39/00 , C07B61/00 , C07C17/20 , C07C41/22 , C07C51/58 , C07C209/68 , C07C211/07 , C07C211/63 , C07C17/00
CPC分类号： C01B17/4576 , C01B7/191 , C07B39/00 , C07C17/206 , C07C41/22 , C07C51/58 , C07C211/07
摘要： The invention relates to the use of hydrogen fluoride adducts and ammonium fluorides for fluorinating acid chlorides and halogen carbon compounds, such as chlorine alkanes or chlorethers. The used adducts can be regenerated and then re-used in fluorination reactions.
摘要翻译：氟化氢和氟化铵加成物可用于酸氯化物和卤化碳化合物，如氯代或氯醚的氟化。用过的加合物可以再生和氟化反应重用。

64. 发明申请

WO00075093A1 METHOD OF MAKING alpha , alpha , alpha -TRIFLUOROMETHOXYBENZENES 审中-公开
标题翻译：制备α，α，α-三氟甲氧基苯甲酸的方法
公开(公告)号：WO00075093A1
公开(公告)日：2000-12-14
申请号：PCT/GB1999/001784
申请日：1999-06-07
IPC分类号： C07C41/22 , C07C43/225
CPC分类号： C07C41/22 , C07C43/225
摘要： Disclosed is a process for making an alpha , alpha , alpha -trifluoromethoxybenzene by reacting an alpha , alpha , alpha -trichloromethoxybenzene or an alpha , alpha , alpha -tribromomethoxybenzene with gaseous hydrogen fluoride in the presence of a catalyst of antimony pentachloride, molybdenum pentachloride, molybdenum dichloride dioxide, molybdenum oxide, or a mixture thereof. The hydrogen fluoride is used in an amount of about 1 to about 1.4 times stoichiometric and is at about atmospheric pressure. The reaction is performed at about 30 to about 100 DEG C.
摘要翻译：公开了通过使α，α，α-三氯甲氧基苯或α，α，α-三溴甲氧基苯与气态氟化氢在五氯化锑，五氯化钼，二氯化钼，氧化钼或其混合物。氟化氢的使用量为化学计量的约1至约1.4倍，并且处于约大气压。反应在约30至约100℃下进行

65. 发明申请

WO99020588A1 PREPARATION OF ISOFLURANE BY REACTION OF 2,2,2-TRIFLUOROETHYL DIFLUOROMETHYL ETHER AND CHLORINE IN ADDED WATER, AT LOW TEMPERATURES AND/OR AT HIGHER CONVERSIONS 审中-公开
标题翻译：通过在低温和/或高转化率下，在添加水中加入2,2,2-三氟乙基二氟甲基醚和氯化物反应制备异氟醚
公开(公告)号：WO99020588A1
公开(公告)日：1999-04-29
申请号：PCT/US1998/021997
申请日：1998-10-15
IPC分类号： C07C41/22 , C07C43/12 , C07C41/00
CPC分类号： C07C41/22 , C07C43/123
摘要： A process for preparing isoflurane (1-chloro-2,2,2-trifluoroethyl difluoromethyl ether) by reacting PFE (2,2,2-trifluoroethyl difluoromethyl ether) with chlorine in the presence of ultraviolet light and added water, at a low temperature and/or at a high conversion.
摘要翻译：一种在紫外光和加水存在下，使PFE（2,2,2-三氟乙基二氟甲基醚）与氯反应制备异氟烷（1-氯-2,2,2-三氟乙基二氟甲基醚）的方法，和/或高转化率。

66. 发明申请

WO98034930A1 PROCESS FOR THE MANUFACTURE OF EPOXY COMPOUNDS 审中-公开
标题翻译：环氧化合物的制备方法
公开(公告)号：WO98034930A1
公开(公告)日：1998-08-13
申请号：PCT/EP1998/000721
申请日：1998-02-06
IPC分类号： C07D301/26 , C07C17/16 , C07C41/22 , C07C43/23 , C07D301/24 , C07D303/23 , C07D303/30 , C08G59/04 , C08G59/06
CPC分类号： C07D301/26 , C07C41/03 , C07C41/22 , C08G59/063 , C07C43/23
摘要： Process for the preparation of compounds of the formula (A) wherein Hal represents chlorine, bromine or iodine and preferably chlorine, wherein Ra represents a residue comprising one or more additional groups of the formula (A') from compounds (III) wherein R2 represents a residue comprising one or more additional groups of the formula (VI) by reaction with gaseous hydrogen halide in the presence of a catalytic amount of an organic acid; process for the preparation of epoxy compounds starting from the reaction (I), and epoxy resins obtained via this process showing a significantly lower content of intermingled halogen.
摘要翻译：制备式（A）化合物的方法，其中Hal表示氯，溴或碘，优选氯，其中R a表示包含一个或多个另外的式（A'）基团的残基，其中R 2表示在催化量的有机酸存在下，通过与气态卤化氢反应，形成一个或多个式（Ⅵ）另外的基团的残基; 从反应（I）开始制备环氧化合物的方法和通过该方法获得的环氧树脂显示出显着较低的混合卤素含量。

67. 发明申请

WO1998031652A1 PROCESS FOR THE SYNTHESIS OF HEXAFLUOROISOPROPYL ETHERS 审中-公开
标题翻译：合成十六烷基醚的方法
公开(公告)号：WO1998031652A1
公开(公告)日：1998-07-23
申请号：PCT/US1997024054
申请日：1997-12-30
申请人： UNIVERSITY OF IOWA RESEARCH FOUNDATION
发明人： UNIVERSITY OF IOWA RESEARCH FOUNDATION , BAKER, Max., T. , TINKER, John, H. , RUZICKA, Jan, A.
IPC分类号： C07C41/00
CPC分类号： C07C41/22 , C07C43/12 , C07C43/123
摘要： A method of synthesizing 1,1,1,3,3,3-hexafluoroisopropyl ether compounds, including, or such as sevoflurane, from methoxymalononitrile, a compound also known as alpha , alpha -dicyanomethyl methyl ether, and having the formula (CN)2CHOCH3, and having the chemical structure (I).
摘要翻译：一种合成1,1,1,3,3,3-六氟异丙基醚化合物的方法，其中包括七氟烷，或由七氟醚，甲氧基丙二腈，也称为α，α-二氰基甲基甲基醚，并具有式（CN） 2CHOCH 3，并且具有化学结构（I）。

68. 发明申请

WO1998027041A1 METHOD OF PREPARING NONAFLUOROISOBUTYL METHYL ETHER 审中-公开
标题翻译：制备非离子型甲基醚的方法
公开(公告)号：WO1998027041A1
公开(公告)日：1998-06-25
申请号：PCT/US1997020203
申请日：1997-11-04
申请人： MINNESOTA MINING AND MANUFACTURING COMPANY
发明人： MINNESOTA MINING AND MANUFACTURING COMPANY , COSTELLO, Michael, G.
IPC分类号： C07C43/12
CPC分类号： C07C43/12 , C07C41/06 , C07C41/22 , C07C41/24 , C07C43/17
摘要： A method of preparing nonafluoroisobutyl methyl ether comprising the step of fluorinating heptafluoroisobutenyl methyl ether.
摘要翻译：一种制备非氟异丁基甲基醚的方法，包括氟化七氟异丁烯基甲基醚的步骤。

69. 发明申请

WO1995004020A1 PROCESS FOR THE PREPARATION OF PERFLUOROALKYL IODIDE 审中-公开
标题翻译：制备全氟代碘化物的方法
公开(公告)号：WO1995004020A1
公开(公告)日：1995-02-09
申请号：PCT/US1994008072
申请日：1994-07-26
申请人： E.I. DU PONT DE NEMOURS AND COMPANY
发明人： E.I. DU PONT DE NEMOURS AND COMPANY , PETROV, Viacheslav, Alexandrovich , KRESPAN, Carl, George
IPC分类号： C07C17/04
CPC分类号： C07C303/22 , C07C17/04 , C07C41/22 , C07C19/16 , C07C309/82 , C07C43/123
摘要： A process for the preparation of perfluoroalkyl iodides, especially perfluoroethyl iodide, by reaction of perfluorinated compounds which contain a carbon carbon double bond with ICl in HF solvent in the presence of Lewis acid catalysts. The compounds are used as telogens for the telomerization of tetrafluoroethylene to long-chain perfluoroalkyl iodides.
摘要翻译：在路易斯酸催化剂存在下，通过在HF溶剂中将包含碳碳双键的全氟化合物与ICl反应制备全氟烷基碘化物，特别是全氟乙基碘的方法。这些化合物用作四聚体将四氟乙烯调聚成长链全氟烷基碘化物的方法。

70. 发明申请

WO1994019391A1 FLUORINATED POLYETHERS AND THEIR PREPARATION 审中-公开
标题翻译：氟化聚醚及其制备
公开(公告)号：WO1994019391A1
公开(公告)日：1994-09-01
申请号：PCT/GB1994000381
申请日：1994-02-25
申请人： BNFL FLUOROCHEMICALS LTD. , CHAMBERS, Richard, Dickinson , JOEL, Andrew, Keith
发明人： BNFL FLUOROCHEMICALS LTD.
IPC分类号： C08G65/00
CPC分类号： C08G65/3236 , C07C41/22 , C07C43/126
摘要： A process for the preparation of a perfluoropolyether having general formula (1) as defined hereinbefore, which process includes the direct fluorination with elemental fluorine of a polyether having general formula (2) as defined hereinbefore, wherein the fluorination is carried out in the presence of a solvent which is an ether having at least one substituent RF, wherein RF is a fluorinated hydrocarbon group. The said solvent ether is preferably a fluorinated volatile ether. The said solvent ether preferably has at least two groups RF which may be the same or different groups. Each group RF preferably has from two to four carbon atoms and at least two fluorine atoms. The said solvent ether may be an alicyclic ether having from 3 to 5 carbon atoms in its alicyclic ring. The intermediate polyether of formula (2) may be prepared by a process in which an appropriate straight-chained or cyclic polyether is reacted with an appropriate fluoroalkene in the presence of a sensitising medium and ultra-violet radiation is applied to energise the medium and promote multiple fluorination.
摘要翻译：一种制备具有上述通式（1）的全氟聚醚的方法，该方法包括用如上定义的通式（2）的聚醚的元素氟直接氟化，其中氟化在作为具有至少一个取代基RF的醚的溶剂，其中RF是氟化烃基。所述溶剂醚优选为氟化挥发性醚。所述溶剂醚优选具有至少两个可以相同或不同基团的基团。每组RF优选具有2至4个碳原子和至少2个氟原子。所述溶剂醚可以是其脂环中具有3至5个碳原子的脂环醚。式（2）的中间聚醚可以通过一种方法制备，其中适当的直链或环状聚醚在敏化介质存在下与合适的氟代烯烃反应，并且使用紫外线辐射来激发介质并促进多次氟化。

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