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61. 发明申请

WO2022155661A1 METHODS FOR PRODUCING ANHYDROUS HYDROGEN IODIDE (HI) 审中-公开
公开(公告)号：WO2022155661A1
公开(公告)日：2022-07-21
申请号：PCT/US2022/070178
申请日：2022-01-13
申请人： HONEYWELL INTERNATIONAL INC.
发明人： CHIU, Yuon , WANG, Haiyou , KOPKALLI, Haluk , JUNGONG, Christian , NAIR, Haridasan K. , SINGH, Rajiv Ratna , MERKEL, Daniel C. , WANG, Tao , YANG, Terris , WILCOX, Richard
IPC分类号： C01B7/13 , B01J20/02
摘要： A method of removing water from a mixture of hydrogen iodide (HI) and water includes providing a mixture comprising hydrogen iodide and water and contacting the mixture with an adsorbent to selectively adsorb water from the mixture, contacting the mixture with a weak acid to absorb water from the mixture and/or separating the water from hydrogen iodide (HI) by azeotropic distillation to produce anhydrous hydrogen iodide (HI).

62. 发明申请

WO2022155659A1 METHODS FOR REMOVING WATER FROM IODINE (I2) 审中-公开
公开(公告)号：WO2022155659A1
公开(公告)日：2022-07-21
申请号：PCT/US2022/070176
申请日：2022-01-13
申请人： HONEYWELL INTERNATIONAL INC.
发明人： CHIU, Yuon , WANG, Haiyou , KOPKALLI, Haluk , JUNGONG, Christian , NAIR, Haridasan K. , SINGH, Rajiv Ratna , MERKEL, Daniel C. , WANG, Tao , YANG, Terris , WILCOX, Richard
IPC分类号： B01D15/00 , C01B7/14
摘要： A method of removing water from a mixture of iodine (I2) and water includes providing a mixture comprising iodine and water and: contacting the mixture with an adsorbent to selectively adsorb water from the mixture, contacting the mixture with a concentrated acid to absorb water from the mixture, separating the water from mixture by distillation, contacting the mixture with a gas that is inert to iodine (I2), contacting the mixture with hydrogen iodide (HI), or combinations thereof.

63. 发明申请

WO2020081364A1 AZEOTROPE OR AZEOTROPE-LIKE COMPOSITIONS OF TRIFLUOROIODOMETHANE (CF3I) AND HEXAFLUOROACETONE (HFA) 审中-公开
公开(公告)号：WO2020081364A1
公开(公告)日：2020-04-23
申请号：PCT/US2019/055650
申请日：2019-10-10
申请人： HONEYWELL INTERNATIONAL INC.
发明人： JUNGONG, Christian , WANG, Haiyou , MERKEL, Daniel C. , PHAM, Hang T. , HULSE, Ryan J.
IPC分类号： C09K5/04
摘要： The present disclosure provides azeotrope or azeotrope-like compositions including trifluoroiodomethane (CFsl) and hexafluoroacetone (HFA), and a method of forming an azeotrope or azeotrope-like composition comprising the step of combining hexafluoroacetone (HFA) and trifluoroiodomethane (CF3I) to form an azeotrope or azeotrope-like comprising hexafluoroacetone (HFA) and trifluoroiodomethane (CF3l) having a boiling point of about -29.84°C ± 0.30°C at a pressure of about 14.40 psia ± 0.30 psia.

64. 发明申请

WO2019136410A1 SYSTEMS AND METHODS FOR REDUCING THE FORMATION OF IMPURITIES DURING 244bb DEHYDROCHLORINATION TO 1234yf 审中-公开
公开(公告)号：WO2019136410A1
公开(公告)日：2019-07-11
申请号：PCT/US2019/012619
申请日：2019-01-08
申请人： HONEYWELL INTERNATIONAL INC.
发明人： WANG, Haiyou , YANG, Terris , MERKEL, Daniel C. , KOPKALLI, Haluk , CERRI, Gustavo , CHIU, Yuon , HORWATH, Richard D.
IPC分类号： C07C17/25 , C07C21/18
摘要： The present disclosure provides various manufacturing processes for the production of 2,3,3,3-tetrafluoropropene (HFO-1234yf or 1234yf). Such methods may allow for the improved yields, more economical processes, and waste reduction in the production of 1234yf and subsequent processes.

65. 发明申请

WO2018044560A1 AZEOTROPIC OR AZEOTROPE-LIKE COMPOSITIONS OF 1,3,3-TRICHLORO-3-FLUORO-1-ENE (HCFO-1231zd) AND HYDROGEN FLUORIDE (HF) 审中-公开
标题翻译： 1,3,3-三氯-3-氟-1-烯（HCFO-1231zd）和氟化氢（HF）的共沸或类共沸组合物
公开(公告)号：WO2018044560A1
公开(公告)日：2018-03-08
申请号：PCT/US2017/046969
申请日：2017-08-15
申请人： HONEYWELL INTERNATIONAL INC.
发明人： MERKEL, Daniel C. , POKROVSKI, Konstantin A , TUNG, Hsueh Sung , WANG, Haiyou , HULSE, Ryan J. , PHAM, Hang T.
IPC分类号： C07C21/04 , C01B7/19
摘要： Azeotropic or azeotrope-like mixtures of 1,3,3-trichloro-3-fluoroprop-1-ene (HCFO-1231zd) and hydrogen fluoride (HF). Such compositions are useful as a feed stock or intermediate in the production of 1,1,1,3,3-pentafluoropropane (HFC-245fa),1-chloro-3,3,3-trifluoropropene (HCFO-1233zd), and 1,3,3,3-tetrafluoropropene (HFO-1234ze).
摘要翻译： 1,3,3-三氯-3-氟丙-1-烯（HCFO-1231zd）和氟化氢（HF）的共沸或类共沸混合物。这样的组合物可用作生产1,1,1,3,3-五氟丙烷（HFC-245fa），1-氯-3,3,3-三氟丙烯（HCFO-1233zd）和1 ，3,3,3-四氟丙烯（HFO-1234ze）。

66. 发明申请

WO2014165094A1 STAGED FLUORINATION PROCESS AND REACTOR SYSTEM 审中-公开
标题翻译：标准荧光法和反应器系统
公开(公告)号：WO2014165094A1
公开(公告)日：2014-10-09
申请号：PCT/US2014/024358
申请日：2014-03-12
申请人： HONEYWELL INTERNATIONAL INC.
发明人： CHIU, Yuon , KOPKALLI, Haluk , SMITH, Robert A. , MERKEL, Daniel C.
IPC分类号： C07C17/38 , C07C19/10 , C07C17/07
CPC分类号： C07C17/087 , C07C17/25 , C07C19/10 , C07C21/18
摘要： The invention relates to a process to produce 244bb from 1233xf in multiple reaction zones whereby the 1233xf starting material is at least 95% converted to 244bb and by-product such as 245cb forms in amounts less than about 2%.
摘要翻译：本发明涉及在多个反应区中从1233xf产生244bb的方法，其中1233xf原料至少95％转化为244bb，副产物如245cb形式的量小于约2％。

67. 发明申请

WO2014164611A1 A METHOD FOR MITIGATING HFC-245CB FORMATION DURING HCFO-1233XF HYDROFLUORINATION TO HCFC-244BB 审中-公开
标题翻译：在HCFO-1233XF氢化HCFC-244BB中减缓HFC-245CB形成的方法
公开(公告)号：WO2014164611A1
公开(公告)日：2014-10-09
申请号：PCT/US2014/023000
申请日：2014-03-11
申请人： HONEYWELL INTERNATIONAL INC.
发明人： WANG, Haiyou , MERKEL, Daniel C. , TUNG, Hsueh Sung , KOPKALLI, Haluk
IPC分类号： C07C17/25 , C07C17/42 , C07C19/08
CPC分类号： C07C17/23 , C07C17/087 , C07C17/206 , C07C17/25 , C07C19/10 , C07C21/18
摘要： The present process relates to a method for minimizing the formation of 1,1,1,2,2-pentafluoropropane in a liquid phase reaction of 2-chloro-3,3,3-trifluoropropene and HF in the presence of a hydrofluorination catalyst comprising: (a) reacting HF with sufficient amount of 2-chloro-3,3,3-trifluoropropene in the presence of a hydrofluorination catalyst under conditions effective to form 2-chloro-1,1,1,2-tetrafluoropropane, the hydrofluorination catalyst being present in sufficient amounts to catalyze said reaction and the 2-chloro-1,1,1,2-tetrafluoropropane being formed with both a conversion of greater than 80% and a 1,1,1,2,2-pentafluoropropane selectivity lower than 20%; and (b) maintaining the 2-chloro-1, 1, 1, 2-tetrafluoropropane being formed with both a conversion of about 80% or more and a 1,1,1,2,2-pentafluoropropane selectivity of about 20% or less by adding said hydrofluorination catalyst to the reactor in small increments.
摘要翻译：本方法涉及在含氟氢化催化剂存在下，在2-氯-3,3,3-三氟丙烯和HF的液相反应中使1,1,1,2,2-五氟丙烷的形成最小化的方法，包括：（a）在氢氟化催化剂存在下，在有效形成2-氯-1,1,1,2-四氟丙烷的条件下，使HF与足够量的2-氯-3,3,3-三氟丙烯反应，氢氟化催化剂以足够的量存在以催化所述反应，形成的2-氯-1,1,1,2-四氟丙烷的转化率大于80％，1,1,1,2,2-五氟丙烷选择性降低超过20％; 和（b）保持2-氯-1,1,1,2-四氟丙烷的转化率为约80％以上，1,1,1,2,2-五氟丙烷选择性为约20％，或较少的是通过以小的增量将所述氢氟化催化剂加入到反应器中。

68. 发明申请

WO2014159009A1 PROCESS TO SUPRESS THE FORMATION OF 3,3,3-TRIFLUOROPROPYNE IN FLUOROCARBON MANUFACTURE 审中-公开
标题翻译：增加氟化硼制造中3,3,3-三氟乙烯的方法
公开(公告)号：WO2014159009A1
公开(公告)日：2014-10-02
申请号：PCT/US2014/021469
申请日：2014-03-07
申请人： HONEYWELL INTERNATIONAL INC.
发明人： KOPKALLI, Haluk , BALL, Jeffrey A. , CHIU, Yuon , TUNG, Hsueh Sung , POKROVSKI, Konstantin A. , MERKEL, Daniel C.
IPC分类号： C07C17/383 , C07C21/18 , B01J19/18
CPC分类号： C07C17/38 , C07B2200/09 , C07C17/206 , C07C17/25 , C07C17/383 , C07C17/389 , Y02P20/582 , C07C21/18
摘要： This invention relates to a process for the suppression of 3,3,3-trifluoropropyne during the manufacture of fluorocarbons, fluoroolefins, hydrochlorofluoroolefins. More particularly, this invention is directed to a process to suppress the formation of 3,3,3-trifluoropropyne during processes for the manufacture of HCFO-1233zd(E), HCFO-1233zd(Z), HFO-1234ze(E), and/or HFO-1234ze(Z).
摘要翻译：本发明涉及在制备氟代烃，氟烯烃，氢氯氟烯烃期间抑制3,3,3-三氟丙炔的方法。更具体地说，本发明涉及抑制在制造HCFO-1233zd（E），HCFO-1233zd（Z），HFO-1234ze（E）的方法中制备3,3,3-三氟丙炔的方法和 /或HFO-1234ze（Z）。

69. 发明申请

WO2014158887A1 AZEOTROPIC COMPOSITIONS OF 1,1,3,3-TETRACHLOROPROP-1-ENE AND HYDROGEN FLUORIDE 审中-公开
标题翻译： 1,1,3,3-四氯丙烯-1-酮和氢氟酸的AZEOTROPIC组合物
公开(公告)号：WO2014158887A1
公开(公告)日：2014-10-02
申请号：PCT/US2014/020688
申请日：2014-03-05
申请人： HONEYWELL INTERNATIONAL INC.
发明人： MERKEL, Daniel C. , POKROVSKI, Konstantin A. , TUNG, Hsueh Sung , WANG, Haiyou , COTTRELL, Stephen A. , PHAM, Hang T.
IPC分类号： C09K5/04 , C07C21/04
CPC分类号： C07C19/08 , C07C21/04 , C07C21/18 , C09K3/00
摘要： Provided are azeotropic or azeotrope-like mixtures of 1,1,3,3-tetrachloroprop-1-ene (HCO-1230za) and hydrogen fluoride. Such compositions are useful as feed stock in the production of HFC-245fa and HCFO-1233zd.
摘要翻译：提供1,1,3,3-四氯丙-1-烯（HCO-1230za）和氟化氢的共沸或类共沸混合物。这样的组合物可用作生产HFC-245fa和HCFO-1233zd中的原料。

70. 发明申请

WO2014121171A1 PROCESS FOR THE PREPARATION OF 1-CHLORO-3,3,3-TRIFLUOROPROPENE USING A PHASE TRANSFER CATALYST 审中-公开
标题翻译：使用相转移催化剂制备1-氯-3,3,3-三氟丙烯的方法
公开(公告)号：WO2014121171A1
公开(公告)日：2014-08-07
申请号：PCT/US2014/014360
申请日：2014-02-03
申请人： HONEYWELL INTERNATIONAL INC.
发明人： TUNG, Hsueh Sung , WANG, Haiyou , MERKEL, Daniel C. , COTTRELL, Stephen A. , POKROVSKI, Konstantin A. , SHANKLAND, Ian
IPC分类号： C07C17/25 , C07C21/18
CPC分类号： C07C17/204 , C07C17/206 , C07C17/21 , C07C17/25 , C07C21/18
摘要： Disclosed is a process in which the fluorination of an organic reactant comprising 1,1,1,3,3-pentachloropropane (240fa) with anhydrous HF is conducted in the presence of an effective amount of a phase-transfer catalyst which facilitates the reaction between these incompatible reaction components to produce 1-chloro-3,3,3-trifluoro-propene (1233zd). Other organic reactant materials include 1,1,3,3-tetrachloropropene (HCO-1230za), 1,3,3,3-tetrachloropropene (HCO-1230zd), and various mixtures with or without 240fa.
摘要翻译：公开了在有效量的相转移催化剂的存在下进行含有1,1,1,3,3-五氯丙烷（240fa）的无水HF的有机反应物的氟化的方法，该相转移催化剂有利于这些不相容的反应组分产生1-氯-3,3,3-三氟丙烯（1233zd）。其它有机反应物料包括1,1,3,3-四氯丙烯（HCO-1230za），1,3,3,3-四氯丙烯（HCO-1230zd）以及各种混合物，其中有或没有240fa。

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