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    • 16. 发明申请
    • METHOD OF PREPARING TONER HAVING CONTROLLED MORPHOLOGY
    • 制备具有控制形态的调色剂的方法
    • WO2010074720A1
    • 2010-07-01
    • PCT/US2009/006534
    • 2009-12-14
    • EASTMAN KODAK COMPANYYANG, Xiqiang
    • YANG, Xiqiang
    • G03G9/08C08J3/03G03G9/087
    • G03G9/0804C08J3/16G03G9/0827G03G9/08755
    • A method for the preparation of shaped polymeric particles, and in a particular embodiment shaped electrostatographic toner particles, of controlled morphology including the following steps. A selected solvent or solvent mixture is used to dissolve a polyester polymer material to form an organic phase, wherein the polyester material is formed from at least one diol and at least one multicarboxylic aromatic acid and has a solubility parameter of greater than 9.0 (cal/cm3)1/2, the selected solvent or solvent mixture includes at least a first solvent having a solubility parameter of less than 9.0 (cal/cm3)1/2, and the difference in solubility parameters for the polyester material and the at least first solvent is between 1.0 and 3.0 (cal/cm3)1/2. The organic phase is dispersed in an aqueous phase containing a particulate stabilizer to form a dispersion, which is then homogenized. The organic solvent is evaporated from the dispersion to form shaped polymeric particles, and the resultant product is recovered, washed and dried.
    • 一种用于制备成形聚合物颗粒的方法,并且在特定实施方案中形成具有受控形态的形状的静电调色剂颗粒,包括以下步骤。 使用选择的溶剂或溶剂混合物来溶解聚酯聚合物材料以形成有机相,其中聚酯材料由至少一种二醇和至少一种多元芳族酸形成,并且具有大于9.0的溶解度参数(cal / cm 3)1/2,所选择的溶剂或溶剂混合物至少包括溶解度参数小于9.0(cal / cm 3)1/2的第一溶剂,以及聚酯材料和至少第一溶剂参数的差异 溶剂为1.0-3.0(cal / cm3)1/2。 将有机相分散在含有颗粒稳定剂的水相中以形成分散体,然后将其均化。 从分散体蒸发有机溶剂以形成成型的聚合物颗粒,并将所得产物回收,洗涤和干燥。