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1. 发明申请

WO2007060115A1 POLYETHYLENE COMPOSITION SUITABLE FOR THE PREPARATION OF FILMS AND PROCESS FOR PREPARING THE SAME 审中-公开
标题翻译：适用于制备薄膜的聚乙烯组合物及其制备方法
公开(公告)号：WO2007060115A1
公开(公告)日：2007-05-31
申请号：PCT/EP2006/068444
申请日：2006-11-14
申请人： BASELL POLYOLEFINE GMBH , KIPKE, Jennifer , MIHAN, Shahram , KARER, Rainer , AUFFERMANN, Jörg , HECKER, Manfred , DE LANGE, Paulus , SCHMITZ, Harald
发明人： KIPKE, Jennifer , MIHAN, Shahram , KARER, Rainer , AUFFERMANN, Jörg , HECKER, Manfred , DE LANGE, Paulus , SCHMITZ, Harald
IPC分类号： C08L23/04
CPC分类号： C08L23/04 , C08L23/06 , C08L23/0815 , C08L2205/02 , C08L2205/025 , C08L2205/035 , C08L2308/00 , C08L2314/06 , C08L2666/06 , C08L2666/02
摘要： A polyethylene composition, in particular suitable for the preparation of films, and a process for preparing the same are described. The polyethylene composition of the invention comprises from 50 to 89 % by weight of a first polyethylene component comprising at least one multimodal polyethylene including a plurality of ethylene polymer fractions having distinct molecular weights and comonomer contents, at least one of said plurality of ethylene polymer fractions being prepared by the use of a single site catalyst, and from 50 to 11 % by weight of a second polyethylene component comprising a low or medium density polyethylene.
摘要翻译：描述了特别适用于制备薄膜的聚乙烯组合物及其制备方法。本发明的聚乙烯组合物包含50至89重量％的第一聚乙烯组分，其包含至少一种多峰聚乙烯，其包含具有不同分子量和共聚单体含量的多种乙烯聚合物级分，所述多种乙烯聚合物级分中的至少一种通过使用单中心催化剂制备，以及50至11重量％的包含低密度或中密度聚乙烯的第二聚乙烯组分。

2. 发明申请

WO2013186299A1 METHOD FOR COOLING A GAS-PHASE REACTOR FOR THE POLYMERIZATION OF OLEFINS 审中-公开
标题翻译：用于冷却气相反应器的方法用于烯烃的聚合
公开(公告)号：WO2013186299A1
公开(公告)日：2013-12-19
申请号：PCT/EP2013/062236
申请日：2013-06-13
申请人： BASELL POLYOLEFINE GMBH
发明人： STRECKER, Holger , HECKER, Manfred , KARER, Rainer , HAMANN, Axel , DE LANGE, Paulus
IPC分类号： B01J8/18 , C08F10/00 , G05D7/06
CPC分类号： B01J8/1836 , B01J8/1809 , B01J2208/00256 , C08F10/02 , C08F110/02 , C08F210/16 , G05D7/0652 , G05D23/1931 , C08F2/34
摘要： A method for controlling the temperature in a polymerization reactor equipped with a cycle gas line for withdrawing reactor gas from the reactor, leading the reactor gas through a heat- exchanger, which is cooled by a cooling medium, which is conveyed in a cooling system through the heat-exchanger, and feeding the reactor gas back to the reactor by adjusting the temperature of the cooling medium entering the heat exchanger, wherein the temperature of the cooling medium entering the heat exchanger is controlled by adjusting the flow rate of the cooling medium in a part of the cooling system by a flow control system comprising two continuously operating flow control devices of different size, which are connected in parallel, a process for polymerizing olefins comprising feeding at least one olefin and at least one polymerization catalyst to a polymerization reactor equipped with a cycle gas line for withdrawing reactor gas from the reactor, leading it through a heat-exchanger for cooling and feeding it back to the reactor, polymerizing the olefins in the presence of the polymerization catalyst and withdrawing the obtained polyolefin from the polymerization reactor, wherein the temperature in the polymerization reactor is controlled by such a method, and a process for controlling the flow rate of a fluid medium by a flow control system comprising two continuously operating flow control devices of different size, which are connected in parallel, wherein the flow control system is controlled by a controller combination comprising a controller controlling the smaller flow control device and a controller controlling the larger flow control device, in which the output of the controller controlling the smaller flow control device is not only fed to the smaller flow control device but also twice to the controller controlling the larger flow control device, once directly as actual value of the controller controlling the larger flow control device and once, after having passed a limiting device, which limits a signal to a centered range, as setpoint of the controller controlling the larger flow control device.
摘要翻译：一种用于控制聚合反应器中的温度的方法，该聚合反应器配备有用于从反应器中排出反应器气体的循环气体管线，引导反应器气体通过由冷却介质冷却的热交换器，冷却介质在冷却系统中通过热交换器，并且通过调节进入热交换器的冷却介质的温度将反应器气体反馈回反应器，其中进入热交换器的冷却介质的温度通过调节冷却介质的流量来控制通过流量控制系统的一部分冷却系统，该流量控制系统包括两个并联连接的不同尺寸的连续操作的流量控制装置，用于聚合烯烃的方法，包括将至少一种烯烃和至少一种聚合催化剂进料到装备有聚合反应器具有用于从反应器中排出反应器气体的循环气体管线，使其通过用于冷却的热交换器并将其送回反应器，在聚合催化剂存在下使烯烃聚合并从聚合反应器中取出所得的聚烯烃，其中通过这种方法控制聚合反应器中的温度，以及控制流速的方法流体介质由包括两个并联连接的不同尺寸的连续操作的流量控制装置的流量控制系统组成，其中流量控制系统由控制器组合控制，该控制器组合包括控制较小流量控制装置的控制器和控制器较大的流量控制装置，其中控制较小流量控制装置的控制器的输出不仅被馈送到较小的流量控制装置，而且还控制着控制较大流量控制装置的控制器的两倍，一次直接作为控制器的实际值控制较大的流量控制装置，并经过一次限制装置将信号限制在居中范围内，作为控制较大流量控制装置的控制器的设定点。

3. 发明申请

WO2012072605A1 METHOD FOR ACTIVATION OF CHROMIUM CONTAINING CATALYST PRECURSOR POLYMERIZATION AND THE RESULTING POLYMERIZATION CATALYST 审中-公开
标题翻译：用于活化含铬催化剂前体聚合和结晶聚合催化剂的方法
公开(公告)号：WO2012072605A1
公开(公告)日：2012-06-07
申请号：PCT/EP2011/071232
申请日：2011-11-29
申请人： BASELL POLYOLEFINE GMBH , HECKER, Manfred , DE LANGE, Paulus , KARER, Rainer
发明人： HECKER, Manfred , DE LANGE, Paulus , KARER, Rainer
IPC分类号： B01J23/26 , C08F10/00 , B01J38/14 , B01J37/14 , B01J38/30 , B01J8/24 , B01J38/32
CPC分类号： C08F4/24 , B01J23/26 , B01J37/14 , B01J38/14 , B01J38/30 , B01J38/32 , C08F10/00 , Y02P20/584 , C08F4/69
摘要： The instant invention relates to an activation of a polymerization catalyst precursor by heat treatment comprising a support material and a catalyst precursor deposited thereon in a fluidized bed activator and to the use of the activated polymerization catalyst in the manufacture of polyolefins. The activation involves heat treatment in the presence of oxygen. After that activation the oxygen in the activator is replaced by inert gas via flushing until the fluidization gas ermerging from the activator comprises oxygen in a maximum amount of up to 5 ppm. The catalyst prepared by that method is improved with respect to prevent reactor fouling during gas-phase polymerization or slurry polymerization either in stirred vessel or loop.
摘要翻译：本发明涉及通过热处理的聚合催化剂前体的活化，其包括在流化床活化剂中沉积在其上的载体材料和催化剂前体，以及活性聚合催化剂在制备聚烯烃中的用途。活化包括在氧气存在下的热处理。在该活化之后，通过冲洗将活化剂中的氧替代为惰性气体，直到来自活化剂的流化气体含量最高达5ppm的氧气。通过该方法制备的催化剂相对于在搅拌容器或循环中的气相聚合或淤浆聚合期间防止反应器结垢而改进。

4. 发明申请

WO2008074467A1 PROCESS FOR PRODUCING PHILLIPS CATALYSTS 审中-公开
标题翻译：生产PHILLIPS催化剂的方法
公开(公告)号：WO2008074467A1
公开(公告)日：2008-06-26
申请号：PCT/EP2007/011112
申请日：2007-12-18
申请人： BASELL POLYOLEFINE GMBH , KÖLLING, Lars , DE LANGE, Paulus , MEIER, Gerhardus
发明人： KÖLLING, Lars , DE LANGE, Paulus , MEIER, Gerhardus
IPC分类号： B01J23/26 , B01J37/08 , C08F10/00 , C08F10/02 , C08F4/24
CPC分类号： B01J23/26 , B01J37/08 , B01J37/26 , C08F10/02 , C08F210/16 , C08F4/24 , C08F4/78 , C08F210/14 , C08F2500/12 , C08F2500/17 , C08F2500/04
摘要： Process for producing chromium catalysts, comprising the steps of: a) applying one or more chromium compound(s) to a finely divided inorganic support to form a catalyst precursor; b) thermally treating the catalyst precursor, the step of thermally treating the catalyst precursor being carried out for at least part of the time in an oxidizing atmosphere and in such a manner that a maximum temperature of from 350°C to 1050°C is not exceeded. The duration of the thermal treatment step at a temperature of above 300°C is, according to the invention, at least 1500 minutes.
摘要翻译：制备铬催化剂的方法，包括以下步骤：a）将一种或多种铬化合物施加到细碎的无机载体上以形成催化剂前体; b）对催化剂前体进行热处理，在氧化气氛中至少部分时间进行催化剂前体的热处理，并且以350℃至1050℃的最高温度不进行热处理超标。根据本发明，在300℃以上的温度下的热处理步骤的持续时间至少为1500分钟。

5. 发明申请

WO2012072618A1 METHOD FOR ACTIVATION OF CHROMIUM CONTAINING CATALYST PRECURSOR FOR POLYMERIZATION AND THE RESULTING POLYMERIZATION CATALYST 审中-公开
标题翻译：用于活化含有催化剂前体用于聚合和结晶聚合催化剂的铬的方法
公开(公告)号：WO2012072618A1
公开(公告)日：2012-06-07
申请号：PCT/EP2011/071248
申请日：2011-11-29
申请人： BASELL POLYOLEFINE GMBH , DE LANGE, Paulus , HECKER, Manfred
发明人： DE LANGE, Paulus , HECKER, Manfred
IPC分类号： B01J23/26 , B01J38/32 , B01J8/18 , C08F10/00
CPC分类号： C08F4/24 , B01J8/1836 , B01J8/22 , B01J23/26 , B01J38/32 , B01J2208/00212 , C08F10/00 , Y02P20/584
摘要： Method for activation of chromium containing catalyst precursor for polymerization and improved polymerization catalyst resulting The instant invention relates to an activation of a polymerization catalyst precursor by heat treatment comprising a support material and a catalyst precursor deposited thereon in a fluidized bed activator and to the use of the activated polymerization catalyst in the manufacture of polyolefins. The Method is performed in a cylindrical activator (1) arranged vertically comprising tubular activator walls, a fluidization gas inlet (2) near the bottom, a fluidization gas outlet (3) near the top and a heat exchange jacket (4) outside the tubular activator walls, wherein the heating jacket covers the complete outer surface of the walls of the activator. The catalyst prepared by that method is improved with respect to its minor content of impurities and causes less interruptions during gas-phase polymerization or slurry polymerization either in stirred vessel or loop.
摘要翻译：活化用于聚合的含铬催化剂前体和改进的聚合催化剂的方法本发明涉及通过热处理活化聚合催化剂前体，其包括在流化床活化剂中沉积在其上的载体材料和催化剂前体，以及使用活性聚合催化剂在制备聚烯烃时。该方法在垂直布置的柱状活化剂（1）中进行，该活化剂垂直地包括管状活化剂壁，靠近底部的流化气体入口（2），顶部附近的流化气体出口（3）和管状外部的热交换夹套活化剂壁，其中加热套覆盖活化剂壁的整个外表面。通过该方法制备的催化剂相对于其少量杂质而改进，并且在搅拌容器或环路中的气相聚合或淤浆聚合期间引起较少的中断。

6. 发明申请

WO2012016971A1 PROCESS AND APPARATUS FOR MIXING AND SPLITTING FLUID STREAMS 审中-公开
标题翻译：混合和分流流体流的方法和装置
公开(公告)号：WO2012016971A1
公开(公告)日：2012-02-09
申请号：PCT/EP2011/063266
申请日：2011-08-02
申请人： BASELL POLYOLEFINE GMBH , OLMSCHEID, Michael , HECKER, Manfred , KARER, Rainer , DE LANGE, Paulus
发明人： OLMSCHEID, Michael , HECKER, Manfred , KARER, Rainer , DE LANGE, Paulus
IPC分类号： B01F3/08 , B01F15/00 , B01J4/00 , B01J8/00 , C08F2/01 , C08F2/34 , C08F10/00
CPC分类号： B29B7/007 , B01F3/0803 , B01F15/00162 , B01F15/00253 , B01F15/00344 , B01J4/008 , C08F10/00 , C08F110/02 , C08F2/01
摘要： A process for continuously mixing at least two fluid streams and splitting the stream of the mixture into at least two partial streams, comprising a) providing streams of the at least two fluids via separated conduits; b) combining the streams of the fluids and forming a homogeneous mixture; c) measuring the pressure in the conduit conveying the mixture of the fluids; d) splitting the stream of the mixture of the fluids into at least two partial streams and feeding each of the partial streams to a conduit equipped with a flow control device controlled by a controller; and e) adjusting the flow rates of the partial streams of the mixture of the fluids by feeding the pressure information measured in step c) as process variable to the controllers controlling the flow control devices, a process for feeding a mixture of at least two fluids via at least two feeding points, an apparatuses for carrying out such processes and a process for polymerizing olefins.
摘要翻译：一种用于连续混合至少两种流体流并将混合物流分解为至少两个部分流的方法，包括a）经由分离的导管提供所述至少两种流体的流; b）组合流体流并形成均匀的混合物; c）测量输送流体混合物的管道中的压力; d）将流体混合物的流分成至少两个部分流，并将每个部分流送入配备有由控制器控制的流量控制装置的导管; 以及e）通过将在步骤c）中测量的压力信息作为过程变量输入到控制流量控制装置的控制器，来调节流体混合物的部分流的流速;将至少两种流体通过至少两个进料点，用于进行这些方法的装置和聚合烯烃的方法。

7. 发明申请

WO2006050919A1 APPARATUS FOR THE GAS-PHASE POLYMERIZATION OF OLEFINS, IN PARTICULAR ETHYLENE 审中-公开
标题翻译：用于气相聚合的装置，特别是乙烯
公开(公告)号：WO2006050919A1
公开(公告)日：2006-05-18
申请号：PCT/EP2005/011956
申请日：2005-11-09
申请人： BASELL POLYOLEFINE GMBH , HERRMANN, Eberhard , SPERBER, Axel , HECKER, Manfred , KARER, Rainer , BERHALTER, Klaus , DE LANGE, Paulus , HALPAP, Jörg , AHMADZADE-YOUSSEFI, Cyrus
发明人： HERRMANN, Eberhard , SPERBER, Axel , HECKER, Manfred , KARER, Rainer , BERHALTER, Klaus , DE LANGE, Paulus , HALPAP, Jörg , AHMADZADE-YOUSSEFI, Cyrus
IPC分类号： C08F10/00 , B01J8/00 , C08F2/34
CPC分类号： B01J8/1872 , B01J8/0055 , B01J8/24 , B01J2208/00256 , B01J2208/00274 , B04C5/081 , C08F6/02 , C08F10/00 , C08F10/02 , C08F110/02 , C08L23/04 , C08F2/34
摘要： An apparatus for the polymerization of olefins, in particular ethylene, comprising a gas-phase fluidized-bed reactor (1), a recycle gas line (2) connected to the reactor for discharging and recirculating the recycle gas stream comprising the unpolymerized olefin and a cyclone (3) located in the recycle gas line for the reduction and precipitation of the solid particles entrained in the recycle gas from the reactor, with the cyclone comprising an upper section (3a) which has an essentially vertical central axis, whose wall extends along a rotationally symmetric body and which is provided with a cyclone inlet (4) arranged eccentrically relative to the central axis, a middle section (3b) which adjoins the upper section (3a) and whose wall extends along a rotationally symmetric body which tapers in a downward direction, a lower section (3c) for discharging the solid particles precipitated from the recycle gas which adjoins the middle section (3b) and whose wall extends along a rotationally symmetric body and a tube (5) extending essentially axially symmetrically down into the upper section and, if appropriate, the middle section for discharging the recycle gas which has been freed of the particles. According to the invention the ratio H; of the distance h; from the lower end of the tube (5) extending downward into the cyclone to the intersection (6) of an imaginary extension of the wall of the downwardextending tube (5) with the wall of the middle section (3b) to the diameter d; of the downwardextending tube (5) is from 3 to 8, in particular from 4 to 7.
摘要翻译：用于烯烃聚合的装置，特别是乙烯，包括气相流化床反应器（1），连接到反应器的再循环气体管线（2），用于排出和再循环包含未聚合烯烃的循环气流和旋风分离器（3）位于循环气体管线中，用于还原和沉淀夹带在来自反应器的再循环气体中的固体颗粒，其中旋风分离器包括具有基本垂直的中心轴线的上部分（3a），其上壁沿着旋转对称体，并且设置有相对于中心轴偏心布置的旋风入口（4），邻接上部（3a）的中间部分（3b），并且其壁沿着旋转对称的体用于排出邻近中间部分（3b）的循环气体沉淀的固体颗粒的下部（3c），并且其壁沿旋转方向延伸对称体和管（5），其基本上轴向对称地延伸到上部，并且如果适当的话，中间部分用于排出已经没有颗粒的循环气体。根据本发明，比率H; 的距离h; 从管（5）的下端向下延伸到旋风分离器中，向下延伸管（5）的壁的假想延伸部与中间部分（3b）的壁的交叉点（6）延伸到直径d; 的下延伸管（5）为3至8，特别是4至7。

8. 发明申请

WO2006050907A1 APPARATUS AND PROCESS FOR THE GAS-PHASE POLYMERIZATION OF OLEFINS 审中-公开
标题翻译：油相气相聚合的装置和方法
公开(公告)号：WO2006050907A1
公开(公告)日：2006-05-18
申请号：PCT/EP2005/011935
申请日：2005-11-08
申请人： BASELL POLYOLEFINE GMBH , HERRMANN, Eberhard , HECKER, Manfred , KARER, Rainer , BERHALTER, Klaus , DE LANGE, Paulus , HALPAP, Jörg , AHMADZADE-YOUSSEFI, Cyrus
发明人： HERRMANN, Eberhard , HECKER, Manfred , KARER, Rainer , BERHALTER, Klaus , DE LANGE, Paulus , HALPAP, Jörg , AHMADZADE-YOUSSEFI, Cyrus
IPC分类号： C08F10/00 , B01J19/18
CPC分类号： B01J8/003 , B01J8/006 , B01J8/1872 , B01J2208/00256 , B01J2208/00274 , B01J2208/00761 , C08F10/00 , C08F110/02 , C08F2/34
摘要： Apparatus for the polymerization of olefins, in particular ethylene, comprising a gas-phase fluidized-bed reactor (1), a product offtake line (15) for taking polymer particles either continuously or discontinuously from the reactor (1), which line (15) is connected to a depressurization vessel (2) for separating polymer particles and gas, a recycle gas filter (3) for freeing the gas of entrained fine particles connected to the depressurization vessel (2), a compressor which compresses the gas which has been freed of fine particles and recirculates it into the reactor (1), with the recycle gas filter (3) having an inlet chamber (4) provided with a gas inlet (6), an outlet chamber (5) provided with a gas outlet (7), an essentially vertical sheet-like filter medium (9) for retaining the fine particles which separates the inlet chamber (4) from the outlet chamber (5) and a particle outlet (8). The inlet chamber (4) has a dividing wall (10) which is arranged essentially parallel to the filter medium (9) and separates the inlet chamber (4) into an inflow region (4a), which is connected to the gas inlet (6), and a filter region (4b) in which the filter medium is located and has an upper opening and a lower opening which are dimensioned so that from 60 to 90% of the volume flow flows through the upper opening so that flow along the filter medium (9) from the top downward results.
摘要翻译：用于烯烃聚合的装置，特别是乙烯，包括气相流化床反应器（1），用于从反应器（1）连续或不连续地获取聚合物颗粒的出口管线（15），该管线（15））连接到用于分离聚合物颗粒和气体的减压容器（2），用于释放与减压容器（2）连接的夹带的细颗粒的气体的循环气体过滤器（3），压缩已经被释放细颗粒并将其再循环到反应器（1）中，循环气体过滤器（3）具有设置有气体入口（6）的入口室（4），设置有气体出口的出口室（5） 7），用于保持将入口室（4）与出口室（5）分离的细颗粒和颗粒出口（8）的基本垂直的片状过滤介质（9）。入口室（4）具有基本上与过滤介质（9）平行布置的分隔壁（10），并将入口室（4）分离成入口区域（4a），该入口区域连接到气体入口）和过滤器区域（4b），其中过滤介质定位并具有上开口和下开口，其尺寸使得体积流量的60％至90％流过上开口，使得沿着过滤器的流动中等（9）从上方下降。

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