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    • 5. 发明授权
    • Method of and apparatus for the recirculation of fluids in a closed
circuit
    • 封闭回路中流体再循环的方法和装置
    • US4150563A
    • 1979-04-24
    • US851783
    • 1977-11-15
    • Milan MinarikMilan PoplJiri Mostecky
    • Milan MinarikMilan PoplJiri Mostecky
    • G01N30/44G01N31/08
    • G01N30/44
    • Method of and appartus for liquid recirculation in at least substantially closed circuit which is particularly suitable for recycled liquid chromatography. The circulating liquid is brought into motion in the circuit inlet by working fluid supplied under pressure, e.g. from a pump, pressure gas cylinder, or the like. Circulating liquid approaching the end of the circuit beyond the circuit outlet is mechanically and at regular intervals repeatedly transported in the form of slugs into the beginning of the circuit in advance of the circuit inlet where these slugs are again forced into the circuit inlet by means of working fluid. The injection of one slug into the circuit inlet and the pushing of the following slug of equal volume out from the circuit outlet are carried out simultaneously.
    • 在至少基本封闭的电路中进行液体再循环的方法和装置,其特别适用于再循环液相色谱。 循环液体通过在压力下供给的工作流体在电路入口中运动。 来自泵,压力气瓶等。 在电路出口之外接近电路端部的循环液体以机械方式并且以规则的间隔重复地以电池形式传输到电路的开头,在电路入口之前,这些电池块再次被迫进入电路入口,借助于 工作流体 将一个塞子注入电路入口并从电路出口推出等体积的以下塞子同时进行。