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1. 发明公开

US20240343668A1 METHOD FOR PREPARING LINEAR HYDROCARBON DOUBLE ACID WITH CYCLIC HYDROCARBON OXIDATION CATALYST 审中-公开
公开(公告)号：US20240343668A1
公开(公告)日：2024-10-17
申请号：US18251015
申请日：2021-10-28
申请人： KOREA ADVANCED INSTITUTE OF SCIENCE AND TECHNOLOGY , HANWHA SOLUTIONS CORPORATION
发明人： Jae Woo LEE , Jeil PARK , Wonhyeong LEE
IPC分类号： C07C51/31 , B01J23/889 , B01J27/198
CPC分类号： C07C51/313 , B01J23/8892 , B01J27/198 , C07C2601/14
摘要： The present invention relates to a method for preparing hydrocarbon double acids using a cyclic hydrocarbon oxidation catalyst, wherein adipic acid and dodecanedioic acid may be produced with high yield while solving the problem of environmental pollution, the adipic acid and the dodecanedioic acid being prepared by using an oxidation reaction of a cyclohexane-cyclohexanone mixture and an oxidation reaction of a cyclododecane-cyclododecanone mixture, respectively, in the presence of a vanadium phosphate oxide-based catalyst and/or a cobalt-manganese oxide-based catalyst.

2. 发明公开

US20240278222A1 SHAPED CATALYST BODY WITH IMPROVED PROPERTIES, ITS PREPARATION AND USE 审中-公开
公开(公告)号：US20240278222A1
公开(公告)日：2024-08-22
申请号：US17927373
申请日：2021-05-17
申请人： BASF SE
发明人： Nicolas DUYCKAERTS , Kazuhiko AMAKAWA , Jens WEIGUNY , Christian WALSDORFF , Miguel Angel ROMERO VALLE , Gerald MEYER , Rouven WEILER
IPC分类号： B01J27/198 , B01J8/02 , B01J35/40 , B01J35/55 , C07C51/25 , C07D307/60
CPC分类号： B01J27/198 , B01J8/02 , B01J35/40 , B01J35/55 , C07C51/252 , C07D307/60
摘要： A shaped catalyst body for heterogeneously catalyzed reactions of organic compounds in the gas-phase in fixed-bed reactors, containing an element from group 3 to 12 of the Periodic Table of the Elements, and having a three-lobed structure with a lateral surface around the lobes, a top cover and a bottom cover, as well as three continuous holes running from one cover side to the other cover side, wherein each hole is assigned to one lobe and wherein the cover sides have outwardly shaped arches, its production and a process for its use in the heterogeneously catalyzed reaction of an organic compound in the gas phase.

3. 发明申请

US20220111367A1 HYDROGENATION CATALYST FOR USE IN HYDROGENATING AMIDE COMPOUND AND METHOD FOR PRODUCING AMINE COMPOUND USING SAME 有权
公开(公告)号：US20220111367A1
公开(公告)日：2022-04-14
申请号：US17273118
申请日：2019-08-30
申请人： OSAKA UNIVERSITY , N.E. CHEMCAT CORPORATION
发明人： Kiyotomi KANEDA , Takato MITSUDOME , Miho KIMURA , Yukio TAKAGI , Yoshiyuki WADA
IPC分类号： B01J27/185 , B01J27/198 , C07C209/26 , B01J37/04
摘要： Provided is a hydrogenation catalyst for an amide compound, containing hydroxyapatite and platinum and vanadium that are fixed on the hydroxyapatite, 15 to 80% of the surface of the platinum being covered with vanadium. The hydrogenation catalyst can promote a reduction reaction in which an amide compound is converted into an amine compound, can be used under mild conditions, and has such durability that the catalyst can be repeatedly used while retaining a high activity.

4. 发明授权

US10710054B2 Multi-zoned catalyst system for oxidation of o-xylene and/or naphthalene to phthalic anhydride 有权
公开(公告)号：US10710054B2
公开(公告)日：2020-07-14
申请号：US15545532
申请日：2016-01-14
申请人： BASF SE
发明人： Diana Carolina Galeano Nunez , Christian Walsdorff , Jürgen Zühlke , Hans-Martin Allmann
IPC分类号： B01J23/22 , B01J35/00 , B01J37/02 , B01J23/00 , B01J27/198 , B01J35/10 , B01J23/18 , B01J21/06 , C07C51/265 , C07C51/31 , B01J37/08 , C07D307/89 , B01J35/02
摘要： The present invention relates to a catalyst system for oxidation of o-xylene and/or naphthalene to phthalic anhydride (PA) comprising at least four catalyst zones arranged in succession in the reaction tube and filled with catalysts of different chemical composition wherein the active material of the catalysts comprise vanadium and titanium dioxide and the active material of the catalyst in the last catalyst zone towards the reactor outlet has an antimony content (calculated as antimony trioxide) between 0.7 to 3.0 wt. %. The present invention further relates to a process for gas phase oxidation in which a gas stream comprising at least one hydrocarbon and molecular oxygen is passed through a catalyst system which comprises at least four catalyst zones arranged in succession in the reaction tube and filled with catalysts of different chemical composition wherein the active materials of the catalysts comprise vanadium and titanium dioxide and the active material of the catalyst in the last catalyst zone towards the reactor outlet has an antimony content (calculated as antimony trioxide) between 0.7 to 3.0 wt. %.

5. 发明授权

US10435347B2 Method for preparing acrylic acid from glycerin 有权
公开(公告)号：US10435347B2
公开(公告)日：2019-10-08
申请号：US15762868
申请日：2016-12-15
申请人： LG CHEM, LTD.
发明人： Kyung Soo Kim , Jun Seon Choi , Ji Yeon Kim , Joo Young Cheon , Wang Rae Joe , Hye Jeong Ok
IPC分类号： C07C51/25 , C07C45/52 , B01J23/888 , B01J27/198
摘要： The present invention relates to a method for preparing acrylic acid from glycerin. More specifically, the present invention provides a method which can improve the selectivity of acrolein by applying a specific catalyst composition and process conditions to minimize the generation of coke carbon of the catalyst, and can prepare acrylic acid with higher productivity for a longer duration of time because a dehydration reaction can be performed for a longer working period while maintaining catalyst activity at a high level during the reaction.

6. 发明授权

US09931618B2 Alkali metal-modified vanadium-phosphorus oxide (VPO) catalyst 有权
公开(公告)号：US09931618B2
公开(公告)日：2018-04-03
申请号：US14673569
申请日：2015-03-30
申请人： Thomas Cotter , Andreas Reitzmann , Gerhard Mestl , Gabriele Donabauer , Susanne Roehrer
发明人： Thomas Cotter , Andreas Reitzmann , Gerhard Mestl , Gabriele Donabauer , Susanne Roehrer
IPC分类号： B01J27/199 , B01J27/198 , B01J37/28 , C07D307/60 , B01J37/10 , B01J23/00 , B01J37/00
CPC分类号： B01J27/199 , B01J23/002 , B01J27/198 , B01J37/0063 , B01J37/10 , B01J37/28 , B01J2523/00 , C07D307/60 , B01J2523/12 , B01J2523/51 , B01J2523/54 , B01J2523/55 , B01J2523/68
摘要： The present invention relates to a catalyst containing a vanadium-phosphorus oxide and an alkali metal, wherein the proportion by weight of alkali metal in the vanadium-phosphorus oxide is in the range from 10 to 400 ppm, based on the total weight of the vanadium-phosphorus oxide, a process for producing it and also the use of the catalyst for the gas-phase oxidation of hydrocarbons, in particular for preparing maleic anhydride.

7. 发明授权

US09926256B2 Catalytic conversion of lactic acid to acrylic acid 有权
公开(公告)号：US09926256B2
公开(公告)日：2018-03-27
申请号：US13835187
申请日：2013-03-15
申请人： The Procter & Gamble Company
发明人： Janette Villalobos Lingoes , Dimitris Ioannis Collias
IPC分类号： B01J27/00 , C07C51/48 , B01J27/18 , B01J27/187 , B01J27/25 , C07C51/377 , C07C51/09 , C07C57/04 , A61F13/534 , C08F2/10 , B01J27/16 , B01J27/185 , B01J27/186 , B01J27/188 , B01J27/195 , B01J27/198 , B01J35/02 , B01J37/00 , B01J37/04 , B01J37/08 , C07C51/44 , A61F13/53
CPC分类号： C07C51/48 , A61F13/53 , A61F13/534 , A61F2013/530489 , A61F2013/530496 , B01J27/16 , B01J27/1806 , B01J27/1811 , B01J27/1817 , B01J27/1853 , B01J27/1856 , B01J27/186 , B01J27/187 , B01J27/188 , B01J27/195 , B01J27/198 , B01J27/25 , B01J35/023 , B01J37/0036 , B01J37/04 , B01J37/08 , C07C51/09 , C07C51/377 , C07C51/44 , C07C57/04 , C08F2/10
摘要： Disclosed herein is a mixed phosphate catalyst for converting lactic acid to acrylic acid, which is characterized by a high conversion of lactic acid, a high selectivity for acrylic acid, a high yield of acrylic acid, and correspondingly low selectivity and molar yields for undesired by-products. This is achieved with a particular class of catalysts defined by a mixture of metal-containing phosphate salts. Further, the catalyst is believed to be stable and active for lengthy periods heretofore unseen in the art for such dehydration processes.

8. 发明申请

US20180078927A1 PROCESS FOR PREPARING MODIFIED V-TI-P CATALYSTS FOR SYNTHESIS OF 2,3-UNSATURATED CARBOXYLIC ACIDS 审中-公开
公开(公告)号：US20180078927A1
公开(公告)日：2018-03-22
申请号：US15829245
申请日：2017-12-01
申请人： Eastman Chemical Company
发明人： David William Norman , Greg Alan King
IPC分类号： B01J27/199 , B01J23/00 , B01J27/198 , C07C57/04 , B01J37/03 , B01J37/08 , C07C51/353 , B01J21/06 , B01J35/00
CPC分类号： B01J27/199 , B01J21/063 , B01J23/002 , B01J27/198 , B01J35/002 , B01J37/03 , B01J37/086 , B01J2523/00 , B01J2523/13 , B01J2523/47 , B01J2523/51 , B01J2523/55 , C07C51/353 , C07C57/04
摘要： The invention relates to a catalyst composition comprising a mixed oxide of vanadium, titanium, and phosphorus modified with alkali metal. The titanium component is derived from a water-soluble, redox-active organo-titanium compound. The catalyst composition is highly effective at facilitating the vapor-phase condensation of formaldehyde with acetic acid to generate acrylic acid, particularly using an industrially relevant aqueous liquid feed.

9. 发明申请

US20180008962A1 MULTI-ZONED CATALYST SYSTEM FOR OXIDATION OF O-XYLENE AND/OR NAPHTHALENE TO PHTHALIC ANHYDRIDE 审中-公开
公开(公告)号：US20180008962A1
公开(公告)日：2018-01-11
申请号：US15545532
申请日：2016-01-14
申请人： BASF SE
发明人： DIANA CAROLINA GALEANO NUNEZ , Christian WALSDORFF , Jurgen ZQHLKE , Hans-Martin ALLMANN
IPC分类号： B01J23/22 , B01J37/02 , B01J27/198 , B01J23/00 , B01J35/00 , C07D307/89 , B01J37/08
摘要： The present invention relates to a catalyst system for oxidation of o-xylene and/or naphthalene to phthalic anhydride (PA) comprising at least four catalyst zones arranged in succession in the reaction tube and filled with catalysts of different chemical composition wherein the active material of the catalysts comprise vanadium and titanium dioxide and the active material of the catalyst in the last catalyst zone towards the reactor outlet has an antimony content (calculated as antimony trioxide) between 0.7 to 3.0 wt. %. The present invention further relates to a process for gas phase oxidation in which a gas stream comprising at least one hydrocarbon and molecular oxygen is passed through a catalyst system which comprises at least four catalyst zones arranged in succession in the reaction tube and filled with catalysts of different chemical composition wherein the active materials of the catalysts comprise vanadium and titanium dioxide and the active material of the catalyst in the last catalyst zone towards the reactor outlet has an antimony content (calculated as antimony trioxide) between 0.7 to 3.0 wt. %.

10. 发明授权

US09593065B2 Process for preparing acrylic acid from methanol and acetic acid 有权
标题翻译：从甲醇和乙酸制备丙烯酸的方法
公开(公告)号：US09593065B2
公开(公告)日：2017-03-14
申请号：US14794955
申请日：2015-07-09
申请人： BASF SE
发明人： Lukas Schulz , Nicolai Tonio Woerz , Tim Blaschke , Marco Hartmann , Frank Huetten
IPC分类号： C07C51/347 , B01J23/50 , B01J27/198 , C07C57/04 , C07C45/38 , C07C51/353 , C07C45/32 , C07C45/78
CPC分类号： C07C51/347 , B01J23/50 , B01J27/198 , C07C45/32 , C07C45/38 , C07C45/783 , C07C51/353 , C07C57/04 , C07C47/04
摘要： A process for preparing acrylic acid from methanol and acetic acid, comprising (i) contacting a gaseous stream S0 comprising methanol, oxygen and inert gas with an oxidation catalyst to obtain a gaseous stream S1 comprising formaldehyde and inert gas; (ii) removing at least a portion of the inert gas present in S1 from at least a portion of the formaldehyde present in S1 by absorbing this formaldehyde in an absorbent to obtain a gaseous stream S2 comprising the portion of the inert gas removed, and to obtain a stream S3 comprising absorbent and absorbate comprising formaldehyde; (iii) optionally removing a portion or the entirety of the absorbent present in stream S3, such that a stream S3a remains from stream S3, and producing a stream S4 from at least stream S3 or stream S3a and a stream S5 comprising acetic acid; and (iv) contacting stream S4 in gaseous form with an aldol condensation catalyst to obtain a gaseous stream S6 comprising acrylic acid.
摘要翻译：一种从甲醇和乙酸制备丙烯酸的方法，包括（i）使包含甲醇，氧气和惰性气体的气流S0与氧化催化剂接触以获得包含甲醛和惰性气体的气流S1; （ii）通过在吸收剂中吸收该甲醛从S1中存在的甲醛的至少一部分除去S1中存在的至少一部分惰性气体，以获得包含去除部分惰性气体的气流S2，并且获得包含含甲醛的吸收剂和吸收剂的流S3; （iii）任选地除去流S3中存在的吸收剂的一部分或全部，使得流S3a从流S3保留，并从至少流S3或流S3a和包含乙酸的流S5产生流S4; 和（iv）将气态的流S4与醛醇缩合催化剂接触以获得包含丙烯酸的气流S6。

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