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1. 发明授权

US10138433B2 Method and apparatus for purifying a mixture comprising oil and wax 有权
公开(公告)号：US10138433B2
公开(公告)日：2018-11-27
申请号：US15579456
申请日：2016-06-10
申请人： Sulzer Chemtech AG
发明人： Mathias Pfeil
IPC分类号： C10G73/06 , B01D9/00 , C10G73/12 , C10G73/14 , C10G73/10 , C10G73/16
摘要： The present invention relates to a method for fractionating a crude mixture comprising at least one oil and at least one wax, which comprises the following steps: (a) mixing the crude mixture with a solvent to obtain a crude solvent-mixture, (b) carrying out at least one crystallization stage with the solvent-mixture obtained in step (a) to prepare a first fraction containing dewaxed oil and a second fraction containing slack wax, (c) carrying out at least one crystallization stage with the second fraction obtained in step (b) in a layer crystallizer, wherein to the second fraction prior to the crystallization in step (c) no solvent or at most 100% by weight of solvent relative to the weight of the second fraction are added, to prepare a third fraction containing hard wax having an oil content of at most 1.5% by weight and a fourth fraction containing soft wax having an oil content of more than 1.5% by weight and (d) circulating at least a part of the fourth fraction into at least one of the at least one crystallization stage of step (b).

2. 发明授权

US09045702B2 Method for producing lubricant base oil 有权
标题翻译：润滑油基础油生产方法
公开(公告)号：US09045702B2
公开(公告)日：2015-06-02
申请号：US13146700
申请日：2010-03-08
申请人： Chikako Hirohashi , Yuichi Tanaka
发明人： Chikako Hirohashi , Yuichi Tanaka
IPC分类号： C10G45/64 , C10G45/60 , C10G73/06 , C10G45/58 , C10G21/00 , C10G45/62 , C10G67/04
CPC分类号： C10G45/58 , C10G21/003 , C10G45/60 , C10G45/62 , C10G67/0454 , C10G2300/1022 , C10G2300/301 , C10G2300/302 , C10G2300/304 , C10G2400/10
摘要： A process for production of a lubricating base oil whereby a lubricating base oil is obtained by a first step in which a stock oil containing normal paraffins of C20 or more is subjected to isomerization reaction so that the content of the normal paraffins of C20 or more is 6-20 wt % based on the total weight of hydrocarbons of C20 or more in the obtained reaction product, a second step in which a lube-oil fraction containing hydrocarbons of C20 or more is separated from the reaction product of the first step, and a third step in which the lube-oil fraction obtained in the second step is separated into a dewaxed oil and a wax by a solvent dewaxing treatment.
摘要翻译：一种润滑油基油的制造方法，其中通过第一步获得润滑油基油，其中使含有C20以上的正链烷烃的原料油进行异构化反应，使得C20以上的正链烷烃的含量为在所得反应产物中基于C 20或更多烃的总重量为6-20重量％，第二步是将含有C20以上烃的润滑油馏分与第一步反应产物和将通过溶剂脱蜡处理将第二工序中得到的润滑油馏分分离为脱蜡油和蜡的第三工序。

3. 发明授权

US07838709B2 Lubricating base oil and lubricating oil composition 有权
标题翻译：润滑基础油和润滑油组成
公开(公告)号：US07838709B2
公开(公告)日：2010-11-23
申请号：US11822408
申请日：2007-07-05
申请人： Shigeki Matsui , Akira Yaguchi , Kazuo Tagawa , Shinichi Shirahama
发明人： Shigeki Matsui , Akira Yaguchi , Kazuo Tagawa , Shinichi Shirahama
IPC分类号： C07C7/20 , C10L1/16 , C10G73/06
CPC分类号： C10M101/00 , C10M109/02 , C10N2220/02 , C10N2220/022 , C10N2220/024 , C10N2220/025 , C10N2230/06 , C10N2230/08 , C10N2230/74 , C10N2270/00
摘要： The invention provides a lubricating base oil with a saturated component content of 90% by mass or greater, a proportion of cyclic saturated components of no greater than 40% by mass of the saturated components, a viscosity index of 110 or greater, an aniline point of 106 or greater and an ε-methylene proportion of 14-20% of the total constituent carbons, as well as a lubricating oil composition comprising the lubricating base oil.
摘要翻译：本发明提供饱和成分含量为90质量％以上的润滑油基础油，饱和成分不大于40质量％的环状饱和成分的比例，粘度指数为110以上，苯胺点为106以上，亚甲基占总组成碳的14〜20％，以及含有润滑油基础油的润滑油组合物。

4. 发明申请

US20070227944A1 System and a method for extracting wax from pulp fibers and paper products 审中-公开
标题翻译：系统和从纸浆纤维和纸制品中提取蜡的方法
公开(公告)号：US20070227944A1
公开(公告)日：2007-10-04
申请号：US11393477
申请日：2006-03-30
申请人： Roger Campbell
发明人： Roger Campbell
IPC分类号： C10G73/06
CPC分类号： C10G73/06
摘要： A system and a method for extracting wax from pulp fibers and/or paper products are provided. The system and method may implement a continuous extraction vessel that can have one or more extraction stages. A single or multi-staged continuous extractor would provide solvent flow which counters the cellulosic materials within the vessel so that the solvent becomes more concentrated with the dissolved wax. This will reduce the volume of solvent necessary to achieve the same extraction efficiency and reduce the energy necessary to remove the solvent from the wax. In another embodiment, the temperature of the solvent can be increased by operating the extractor under a pressure greater than atmospheric pressure.
摘要翻译：提供了一种用于从纸浆纤维和/或纸制品中提取蜡的系统和方法。该系统和方法可以实现可以具有一个或多个提取阶段的连续提取容器。单级或多级连续萃取器将提供与容器内的纤维素材料相反的溶剂流，使得溶剂变得与溶解的蜡更浓缩。这将减少实现相同萃取效率所需的溶剂体积并降低从蜡中除去溶剂所需的能量。在另一个实施方案中，通过在大于大气压的压力下操作萃取器可以提高溶剂的温度。

5. 发明申请

US20050054775A1 Novel dewaxing aid 有权
标题翻译：新型脱蜡助剂
公开(公告)号：US20050054775A1
公开(公告)日：2005-03-10
申请号：US10504685
申请日：2002-10-25
申请人： Naoki Haga , Akiyuki Hiraide
发明人： Naoki Haga , Akiyuki Hiraide
IPC分类号： C10G73/12 , C10G73/06 , C08K5/07
CPC分类号： C10G73/06
摘要： The present invention relates to dewaxing aids comprising the mixture of two or more polyalkyl(meth)acrylates having an exothermic heat initiation temperature within the specific range when chilled at 30° C./minute rate, to be added together with the wax-containing hydrocarbon oil to the dewaxing solvent. The dewaxing aid according to the present invention can be used in the solvent dewaxing method containing the stage in which the chilling rate during the chilling is 30° C./minute or higher, is effective for heavy type wax-containing hydrocarbon oils, and is chlorine-free.
摘要翻译：本发明涉及脱蜡助剂，其包含两种或更多种（甲基）丙烯酸烷基酯的混合物，其具有在30℃/分钟速度下冷却的特定范围内的放热热引发温度，并与含蜡烃油到脱蜡溶剂。根据本发明的脱蜡助剂可以用于含有冷冻冷冻速度为30℃/分钟以上的阶段的溶剂脱蜡方法，对于重型含蜡烃油是有效的，并且是无氯。

6. 发明授权

US6096940A Biodegradable high performance hydrocarbon base oils 失效
标题翻译：可生物降解的高性能烃基油
公开(公告)号：US6096940A
公开(公告)日：2000-08-01
申请号：US121320
申请日：1998-07-22
申请人： Robert Jay Wittenbrink , Richard Frank Bauman , Daniel Francis Ryan
发明人： Robert Jay Wittenbrink , Richard Frank Bauman , Daniel Francis Ryan
IPC分类号： B01J23/88 , B01J23/89 , C10G2/00 , C10G45/58 , C10G45/60 , C10G45/62 , C10G47/02 , C10G47/12 , C10G47/14 , C10G65/04 , C10G65/12 , C10G67/04 , C10G67/14 , C10G73/06 , C10M101/02 , C10M107/02 , C10N40/25 , C10G57/00 , C10G47/00 , C10G47/20
CPC分类号： C10G45/58 , C10G67/04 , C10M107/02 , C10G2400/10 , C10G2400/12 , C10G2400/14 , C10M2205/173 , C10N2220/028 , C10N2270/00
摘要： Discloses novel biodegradable high performance hydrocarbon base oils useful as lubricants in engine oil and industrial compositions, and process for their manufacture. A waxy, or paraffinic feed, particularly a Fischer-Tropsch wax, is reacted over a dual function catalyst to produce hydroisomerization and hydrocracking reactions, at 700.degree. F.+ conversion levels ranging from about 20 to 50 wt. %, preferably about 25-40 wt. %, sufficient to produce a crude fraction, e.g., a C.sub.5 -1050.degree. F.+ crude fraction, containing 700.degree. F.+ isoparaffins having from about 6.0 to about 7.5 methyl branches per 100 carbon atoms in the molecule. The methyl paraffins containing crude fraction is topped via atmospheric distillation to produce a bottoms fraction having an initial boiling point between about 650.degree. F. and 750.degree. F. which is then solvent dewaxed, and the dewaxed oil is then fractionated under high vacuum to produce biodegradable high performance hydrocarbon base oils.
摘要翻译：公开了可用作发动机油和工业组合物中的润滑剂的新型可生物降解的高性能烃基油及其制造方法。蜡状或石蜡原料，特别是费 - 托蜡在双重功能催化剂上反应，在700°F下进行加氢异构化和加氢裂化反应。转化率范围为约20至50wt。％，优选约25-40wt。％，足以产生粗分馏，例如含有分子中每100个碳原子的约6.0至约7.5个甲基支链的含有700°F +异链烷烃的C5-1050°F +粗级分。含有粗馏分的甲基链烷烃通过常压蒸馏来顶部，产生沸点在约650°F至750°F之间的塔底馏分，然后进行溶剂脱蜡，然后将脱蜡油在高真空下分馏，可生物降解的高性能烃基油。

7. 发明授权

US6096189A Hydroconversion process for making lubricating oil basestocks 失效
标题翻译：润滑油基础油的加氢转化工艺
公开(公告)号：US6096189A
公开(公告)日：2000-08-01
申请号：US768252
申请日：1996-12-17
申请人： Ian A. Cody , Douglas R. Boate , Sandra J. Alward , William J. Murphy , John E. Gallagher , Alberto Ravella , Richard A. Demmin
发明人： Ian A. Cody , Douglas R. Boate , Sandra J. Alward , William J. Murphy , John E. Gallagher , Alberto Ravella , Richard A. Demmin
IPC分类号： C10G45/58 , C10G65/04 , C10G65/12 , C10G67/04 , C10G73/06 , C10M177/00 , C10G1/04 , C10G71/00
CPC分类号： C10G67/0418 , C10G65/04 , C10G65/043 , C10G2300/1062 , C10G2300/301 , C10G2300/302 , C10G2300/4006 , C10G2300/4012 , C10G2300/4018 , C10G2400/10
摘要： A process for producing a lubricating oil basestock having at least 90 wt. % saturates and a VI of at least 105 by selectively hydroconverting a raffinate from a solvent extraction zone in a two step hydroconversion zone followed by a hydrofinishing zone.
摘要翻译：一种制备具有至少90wt。％的润滑油基础油的方法。通过在两步加氢转化区中随后加氢精制区选择性地将来自溶剂萃取区的萃余液加氢转化至少为105的饱和物。

8. 发明授权

US6024862A Petroleum-wax separation 失效
标题翻译：石油蜡分离
公开(公告)号：US6024862A
公开(公告)日：2000-02-15
申请号：US221064
申请日：1998-12-28
申请人： Michael D. Ackerson , Seyed-Hamid Arabshahi , Robert E. Babcock
发明人： Michael D. Ackerson , Seyed-Hamid Arabshahi , Robert E. Babcock
IPC分类号： C10G73/02 , C10G73/06
CPC分类号： C10G73/025 , C10G73/06
摘要： A process for dewaxing including the steps of mixing a waxy feedstock near its pour point with an ambient or below ambient temperature solvent essentially free of a selected cosolvent, to form a solvent/feedstock mixture, essentially free of a selected cosolvent, and subsequently adding the cosolvent to the solvent/feedstock mixture to cause instantaneous precipitation of wax on addition of cosolvent with the amount of wax precipitation being controlled by the quantity and temperature of cosolvent added. The cosolvent is essentially completely miscible with the solvent, but immiscible with the oil and wax. For example, alcohols (methanol, ethanol, propanol), ketones (ketene, acetone), amines, etc. The process of the present invention provides the advantages of lower solvent ratios (higher solvent recovery), higher filtration temperatures, "environmentally compatible" solvents, rapid filtration rates, and debottlenecking of existing dewaxing plants.
摘要翻译：一种脱蜡方法，包括以下步骤：在其倾点附近将蜡质原料与基本上不含所选助溶剂的环境温度或低于环境温度的溶剂混合，形成基本上不含所选助溶剂的溶剂/原料混合物，随后将共溶剂加入到溶剂/原料混合物中，引起蜡在加入共溶剂时的瞬间沉淀，蜡沉淀量由加入的助溶剂的量和温度控制。共溶剂基本上与溶剂完全混溶，但与油和蜡不混溶。例如，醇（甲醇，乙醇，丙醇），酮（乙烯酮，丙酮），胺等。本发明的方法提供了较低溶剂比（更高的溶剂回收），更高的过滤温度，“环境相容” 溶剂，快速过滤速率和现有脱蜡设备的脱瓶。

9. 发明授权

US5976353A Raffinate hydroconversion process (JHT-9601) 失效
标题翻译：残液加氢转化法（JHT-9601）
公开(公告)号：US5976353A
公开(公告)日：1999-11-02
申请号：US678382
申请日：1996-06-28
申请人： Ian A. Cody , Douglas R. Boate , Sandra J. Alward , William J. Murphy , John E. Gallagher , Gary L. Harting
发明人： Ian A. Cody , Douglas R. Boate , Sandra J. Alward , William J. Murphy , John E. Gallagher , Gary L. Harting
IPC分类号： C10G73/06 , C10G45/60 , C10G65/04 , C10G65/08 , C10G65/12 , C10G67/04 , C10G73/32 , C10G1/04 , C10G11/02 , C10G25/00
CPC分类号： C10G67/0418 , C10G65/04 , C10G65/043 , C10G65/08 , C10G2400/10
摘要： A process for producing a high VI/low volatility lubricating oil basestock. The process comprises subjecting the raffinate from a solvent extraction step to a two step, single stage hydroconversion process wherein the first step involves severe hydroconversion of the raffinate followed by a cold hydrofinishing step.
摘要翻译：一种生产高VI /低挥发性润滑油基础油的方法。该方法包括使萃余液从溶剂萃取步骤进行到两步，单阶段加氢转化方法，其中第一步骤涉及萃余液的严格加氢转化，然后进行冷加氢精制步骤。

10. 发明授权

US5935417A Hydroconversion process for making lubricating oil basestocks 失效
标题翻译：润滑油基础油的加氢转化工艺
公开(公告)号：US5935417A
公开(公告)日：1999-08-10
申请号：US23573
申请日：1998-02-13
申请人： Ian A. Cody , Douglas R. Boate , William J. Murphy , Daniel P. Leta
发明人： Ian A. Cody , Douglas R. Boate , William J. Murphy , Daniel P. Leta
IPC分类号： C10G45/58 , C10G1/04 , C10G3/00 , C10G17/00 , C10G21/00 , C10G47/02 , C10G65/04 , C10G65/12 , C10G67/04 , C10G71/00 , C10G73/06 , C10M177/00 , C10G11/04
CPC分类号： C10G65/04 , C10G65/043 , C10G67/0418 , C10G2400/10 , Y02P30/20
摘要： A process for producing a lubricating oil basestock having at least 90 wt. % saturates and a VI of at least 105 by selectively hydroconverting a raffinate from a solvent extraction zone in a two step hydroconversion zone followed by a hydrofinishing zone and a dewaxing zone.
摘要翻译：一种制备具有至少90wt。％的润滑油基础油的方法。通过在两步加氢转化区中随后加氢精制区和脱蜡区选择性地将来自溶剂萃取区的残液选择性地加氢转化至少为105的饱和物。

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