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1. 发明授权

US3288853A Method for the preparation of dicyclohexyl ketone 失效
标题翻译：二环己基酮的制备方法
公开(公告)号：US3288853A
公开(公告)日：1966-11-29
申请号：US28943263
申请日：1963-06-20
申请人： SNIA VISCOSA
发明人： WERNER MUENCH , FRANCESCO SICLARI , GIULIANA SILVERSTRI , TERESA ARGENZIANO , ROBERTO IACUONE
IPC分类号： C07C45/48 , C07C49/317
CPC分类号： C07C49/317 , C07C45/48

2. 发明授权

US5629455A Process for preparing cyclopropyl alkyl ketones and 4,5-dihydroalkylfurans 失效
标题翻译：制备环丙基烷基酮和4,5-二氢烷基呋喃的方法
公开(公告)号：US5629455A
公开(公告)日：1997-05-13
申请号：US589952
申请日：1996-01-23
申请人： Manfred Kaufhold , Marcel Feld
发明人： Manfred Kaufhold , Marcel Feld
IPC分类号： C07C45/59 , C07C45/67 , C07C49/293 , C07C49/317 , C07C49/792 , C07D307/28 , C07C45/54
CPC分类号： C07D307/28 , C07C45/676
摘要： The invention relates to a novel process for the simultaneous preparation of cyclopropyl alkyl ketones and 4,5-dihydroalkylfurans from 3-acyltetrahydrofuran-2-ones using a metal salt according to the diagram ##STR1## In the reaction, N-alkyllactams and/or N-acylmorpholines which are high-boiling and only slightly miscible with water are used. By charging the solvent, the metal salt and the 3-acyltetrahydrofuran-2-one in a molar excess with respect to the metal salt, heating the mixture to 160.degree. to 220.degree. C. and metering in further 3-acyl-tetrahydrofuran-2-one, the desired products are obtained in high yields. The metal salt can moreover be recovered in a simple manner by washing with water.
摘要翻译：本发明涉及一种根据图中使用金属盐从3-酰基四氢呋喃-2-酮同时制备环丙基烷基酮和4,5-二氢烷基呋喃的新方法。在反应中，N - 烷基内酰胺和/或N-酰基吗啉，它们是高沸点且仅与水轻微混溶。通过将溶剂，金属盐和3-酰基四氢呋喃-2-酮相对于金属盐摩尔过量地加入，将混合物加热至160℃至220℃，并进一步计量3-酰基 - 四氢呋喃-2 - 一种，以高产率获得所需的产物。此外，金属盐可以通过用水洗涤以简单的方式回收。

3. 发明授权

US4432885A Decalins 失效
标题翻译：十进制
公开(公告)号：US4432885A
公开(公告)日：1984-02-21
申请号：US328979
申请日：1981-12-09
申请人： Martin Petrzilka , Kuno Schleich
发明人： Martin Petrzilka , Kuno Schleich
IPC分类号： C07C1/22 , C07C1/32 , C07C13/28 , C07C13/50 , C07C17/12 , C07C25/02 , C07C25/22 , C07C29/14 , C07C29/143 , C07C29/19 , C07C37/055 , C07C43/115 , C07C43/172 , C07C43/18 , C07C43/21 , C07C45/29 , C07C45/44 , C07C45/46 , C07C45/51 , C07C45/62 , C07C45/68 , C07C49/313 , C07C49/317 , C07C49/792 , C07C63/00 , C07C63/49 , C07C69/157 , C07C69/24 , C07C69/75 , C07C69/76 , C07C255/45 , C07C255/49 , C07C255/50 , C09K19/00 , C09K19/32 , C07C13/47 , C07C49/30 , C07C103/22 , C07C121/64 , C09K3/34
CPC分类号： C07C17/12 , C07C1/22 , C07C1/322 , C07C13/50 , C07C25/22 , C07C255/00 , C07C29/14 , C07C29/143 , C07C29/19 , C07C37/0555 , C07C43/18 , C07C43/21 , C07C45/292 , C07C45/44 , C07C45/46 , C07C45/513 , C07C45/62 , C07C45/68 , C07C49/313 , C07C49/792 , C07C63/49 , C09K19/322 , C07B2200/07 , C07C2101/14 , C07C2102/28 , C09K2019/326
摘要： Decalins of the formula ##STR1## wherein ring A is aromatic or a trans-1,4-disubstituted cyclohexane ring; R.sup.2 is methyl, --CH.sub.2 R', --OR', --CO--R', --CN, --COOH, --CO--OR', --CO--SR' or --O--CO--R'; R.sup.1 is hydrogen, methyl, --CH.sub.2 R, --OR or --CH.sub.2 OR, or when R.sup.2 is methyl, --CH.sub.2 R', --OR' or --CO--R', R.sup.1 also can be --CN, --COOH, --CO--OR, --CO--SR or --O--CO--R; R and R' each are alkyl; and R.sup.1 and R.sup.2 each have up to 12 carbon atoms and together have at most 14 carbon atoms,their racemates and optically active antipodes, are described. Liquid crystalline mixtures comprising Compound I as well as their use in electro-optical devices also are disclosed.
摘要翻译：其中环A是芳族或反式-1,4-二取代的环己烷环; R 2是甲基，-CH 2 R'，-OR'，-CO-R'，-CN，-COOH，-CO-OR'，-CO-SR'或-O-CO-R' R1是氢，甲基，-CH2R，-OR或-CH2OR，或当R2是甲基时，-CH2R'，-OR'或-CO-R'，R1也可以是-CN，-COOH，-CO-OR， -CO-SR或-O-CO-R; R和R'各自为烷基; 并且R1和R2各自具有至多12个碳原子并且共有至多14个碳原子，它们的外消旋体和光学活性对映体。还公开了包含化合物I的液晶混合物以及它们在电光器件中的用途。

4. 发明授权

US4089986A Flavoring with norbornanol derivatives 失效
标题翻译：用降冰片烷醇衍生物调味
公开(公告)号：US4089986A
公开(公告)日：1978-05-16
申请号：US834399
申请日：1977-09-19
申请人： Kenneth K. Light , Manfred Hugo Vock , Edward J. Shuster , Frederick Louis Schmitt
发明人： Kenneth K. Light , Manfred Hugo Vock , Edward J. Shuster , Frederick Louis Schmitt
IPC分类号： C07C69/02 , A23G4/00 , A23G4/06 , A23L27/20 , A61K8/33 , A61K8/34 , A61K8/35 , A61K8/37 , A61Q13/00 , C07C27/00 , C07C31/137 , C07C33/05 , C07C35/29 , C07C41/00 , C07C43/115 , C07C43/162 , C07C43/305 , C07C45/00 , C07C49/317 , C07C49/527 , C07C67/00 , C07C239/00 , C07C251/44 , C07D303/04 , C11B9/00 , A23L1/226
CPC分类号： A23G4/06 , C07C35/29 , C11B9/0046 , C11D3/0084
摘要： Processes and compositions are described for the use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma and perfume aroma augmenting, enhancing, modifying and imparting compositions and as foodstuff, chewing gum, toothpaste, medicinal product, perfume and perfumed article aroma imparting materials of 3,3-dimethyl-2(3-butenyl) norbornanol-2 (hereinafter referred to as the "norbornanol derivative" having the structure: ##STR1## (which structure is intended to cover both the "endo" and the "exo" isomers thereof) produced by a process which comprises reacting an allylic Grignard reagent having the structure: wherein X is chloro, bromo or iodo with camphene oxide having the structure: ##STR2## by either "exo" camphene oxide or "endo" camphene oxide or a mixture of "exo" and "endo" camphene oxide. Addition of the said norbornanol derivative to consumable materials is indicated to produce:(a) In foodstuffs, foodstuff flavorings, chewing gums, toothpastes and medicinal products, sweet, fruity, berry-like aromas with woody, incense-like, cedarwood-like, tea-like and floral nuances and incense-like and cedarwood-like flavors with rosey, berry and tea-like nuances; and(b) In perfumes, colognes and perfumed articles, sweet, woody, thujone-like aromas with strong fir-balsam, armoise, cedarleaf, piney, earthy and camphoraceous nuances.
摘要翻译：描述了用于食品，口香糖，牙膏和药用产品风味和芳香和香料香气的方法和组合物，其增强，增强，改性和赋予组合物以及作为食品，口香糖，牙膏，药用产品，香料和香料制品香气赋予 3,3-二甲基-2（3-丁烯基）降冰片烷醇-2的材料（以下称为“降冰片醇衍生物”，具有以下结构：（该结构旨在涵盖“endo”和“exo 通过包括使具有以下结构的烯丙基格利雅试剂（其中X为氯，溴或碘）与具有以下结构的camp氧化物反应的方法制得的：其异构体：通过“外部”camp oxide或“内氧化camp oxide oxide or：camp camp camp camp camp camp camp camp camp camp camp camp：：：：：：：：：：：：：：：：：

5. 发明授权

US08524952B2 Modified naphthalene formaldehyde resin, tricyclodecane skeleton-containing naphthol compound and ester compound 有权
标题翻译：改性萘甲醛树脂，含三环癸烷骨架的萘酚化合物和酯化合物
公开(公告)号：US08524952B2
公开(公告)日：2013-09-03
申请号：US13423962
申请日：2012-03-19
申请人： Seiji Kita , Masashi Ogiwara , Mitsuharu Kitamura , Dai Oguro , Gou Higashihara
发明人： Seiji Kita , Masashi Ogiwara , Mitsuharu Kitamura , Dai Oguro , Gou Higashihara
IPC分类号： C07C49/317 , C07C49/323 , C07C49/345
CPC分类号： C07C45/68 , C07C67/14 , C07C69/753 , C07C2603/68 , C08G8/28 , G03F7/094 , C07C49/83
摘要： A modified dimethylnaphthalene formaldehyde resin obtained by modifying a polyfunctional dimethylnaphthalene formaldehyde resin having a constituent unit represented by the following general formula [1] in a molecule thereof with at least one member selected from the group consisting of a phenol represented by the following general formula [2], a naphthol represented by the following general formula [3] and a naphthol represented by the following general formula [4] provided that at least any of the naphthol represented by the general formula [3] or the naphthol represented by the general formula [4] must be included.
摘要翻译：通过将分子中具有下述通式[1]表示的构成单元的多官能二甲基萘甲醛树脂与选自下述通式[1]所示的苯酚中的至少一种进行改性而得到的改性二甲基萘甲醛树脂， 2]，由以下通式[3]表示的萘酚和由以下通式[4]表示的萘酚，条件是至少任何由通式[3]表示的萘酚或由通式 [4]必须包括在内。

6. 发明授权

US4107094A 3,3-Dimethyl 2(3-butenyl) norbornanol-2 perfume compositions 失效
标题翻译： 3,3-二甲基2（3-丁烯基）降冰片烷醇-2香料组合物
公开(公告)号：US4107094A
公开(公告)日：1978-08-15
申请号：US834400
申请日：1977-09-19
申请人： Kenneth K. Light , Manfred Hugo Vock , Edward J. Shuster , Frederick Louis Schmitt
发明人： Kenneth K. Light , Manfred Hugo Vock , Edward J. Shuster , Frederick Louis Schmitt
IPC分类号： C07C69/02 , A23G4/00 , A23G4/06 , A23L27/20 , A61K8/33 , A61K8/34 , A61K8/35 , A61K8/37 , A61Q13/00 , C07C27/00 , C07C31/137 , C07C33/05 , C07C35/29 , C07C41/00 , C07C43/115 , C07C43/162 , C07C43/305 , C07C45/00 , C07C49/317 , C07C49/527 , C07C67/00 , C07C239/00 , C07C251/44 , C07D303/04 , C11B9/00
CPC分类号： A23G4/06 , C07C35/29 , C11B9/0046 , C11D3/0084
摘要： Processes and compositions are described for the use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma and perfume aroma augmenting, enhancing, modifying and imparting compositions and as foodstuff, chewing gum, toothpaste, medicinal product, perfume and perfumed article aroma imparting materials of 3,3-dimethyl-2(3-butenyl) norbornanol-2 (hereinafter referred to as the "norbornanol derivative" having the structure: ##STR1## (which structure is intended to cover both the "endo" and the "exo" isomers thereof) produced by a process which comprises reacting an allylic Grignard reagent having the structure: ##STR2## wherein X is chloro, bromo or iodo with camphene oxide having the structure: ##STR3## by either "exo" camphene oxide or "endo" camphene oxide or a mixture of "exo" and "endo" camphene oxide. Addition of the said norbornanol derivative to perfumes and colognes is indicated to produce sweet, woody, thujone-like aromas with strong fir-balsam, armoise, cedarleaf, piney, earthy and camphoraceous nuances.
摘要翻译：描述了用于食品，口香糖，牙膏和药用产品风味和芳香和香料香气的方法和组合物，其增强，增强，改性和赋予组合物以及作为食品，口香糖，牙膏，药用产品，香料和香料制品香气赋予 3,3-二甲基-2（3-丁烯基）降冰片烷醇-2的材料（以下称为“降冰片醇衍生物”，具有以下结构：（该结构旨在涵盖“endo”和“exo 通过包括使具有以下结构的烯丙基格利雅试剂（其中X为氯，溴或碘）与具有以下结构的camp氧化物反应的方法制得的：其异构体：通过“外部”camp oxide或“内 “camp hene oxide oxide oxide ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar ar 叶，松，泥土和樟脑的细微差别。

7. 发明申请

US20100174042A1 AROMATIC COMPOUND AND SULFONATED POLYARYLENE POLYMER 有权
标题翻译：芳香化合物和磺化聚亚烷基聚合物
公开(公告)号：US20100174042A1
公开(公告)日：2010-07-08
申请号：US12298385
申请日：2007-04-24
申请人： Yoshitaka Yamakawa , Yousuke Konno , Teruhiko Umehara
发明人： Yoshitaka Yamakawa , Yousuke Konno , Teruhiko Umehara
IPC分类号： C08G8/02 , C07C49/317 , C07C255/51 , C08G75/24
CPC分类号： C07C49/84 , C07C45/71 , C07C255/54 , C07C2603/18 , C08G65/40 , C08G65/4012 , C08G65/4031 , C08J5/2231 , C08J2365/02 , H01M8/0289 , H01M8/1025 , H01M8/1027 , H01M8/103 , H01M8/1032 , H01M8/1039 , Y02E60/523
摘要： Sulfonated polymers have excellent processability and methanol resistance.An aromatic compound is represented by Formula (1) below: wherein A, D and E are each at least one structure selected from the group consisting of a direct bond, —O—, —S—, —CO—, —SO2—, —SO—, —CONH—, —COO—, —(CF2)f— (wherein f is an integer of 1 to 10), —(CH2)h— (wherein h is an integer of 1 to 10), —CR′2— (wherein R′ is an aliphatic hydrocarbon group, an aromatic hydrocarbon group or a halogenated hydrocarbon group), a cyclohexylidene group and a fluorenylidene group; each B is independently an oxygen atom or a sulfur atom; X is an atom or a group selected from halogen atoms other than fluorine, —OSO2CH3 and —OSO2CF3; R1 to R28 are the same or different from one another and are each at least one atom or group selected from the group consisting of a hydrogen atom, a fluorine atom, alkyl groups, partially or completely halogenated alkyl groups, allyl groups, aryl groups, nitro group and nitrile group; l and o are each an integer of 0 to 4; m is an integer of 1 to 4; q is an integer of 2 or greater; n and p indicate a composition ratio of the respective units and are each a number ranging from 0 to 1; n+p=1; and n is not 0.
摘要翻译：磺化聚合物具有优异的加工性和耐甲醇性。芳族化合物由下式（1）表示：其中A，D和E各自为至少一个选自直接键，-O - ， - S-，-CO-，-SO 2 - 的结构， - （CH 2）h - （其中h为1至10的整数），-CR（CH 2）n - ， - （CF 2）f - （其中f为1至10的整数） '2-（其中R'是脂族烃基，芳族烃基或卤代烃基），亚环己基和亚芴基; 每个B独立地是氧原子或硫原子; X是选自氟以外的卤素原子，-OSO 2 CH 3和-OSO 2 CF 3的原子或基团; R1至R28彼此相同或不同，并且各自为至少一个选自氢原子，氟原子，烷基，部分或完全卤化的烷基，烯丙基，芳基，硝基和腈基; l和o分别为0〜4的整数; m为1〜4的整数。 q是2或更大的整数; n和p表示各单元的组成比，分别为0〜1的数。 n + p = 1; 并且n不为0。

8. 发明授权

US4448712A Perfume compositions and perfumed articles containing spiro-undecanones and -undecenones as perfume base 失效
标题翻译：香料组合物和含有螺十一酮和十一酮作为香料基质的香料制品
公开(公告)号：US4448712A
公开(公告)日：1984-05-15
申请号：US417207
申请日：1982-09-13
申请人： Antonius J. A. van der Weerdt , Willem Apeldoorn
发明人： Antonius J. A. van der Weerdt , Willem Apeldoorn
IPC分类号： A61K8/35 , A61Q13/00 , C07C45/62 , C07C45/68 , C07C45/73 , C07C49/427 , C07C49/623 , C11B9/00 , C07C49/317
CPC分类号： C11B9/0057 , C07C45/62 , C07C45/68 , C07C45/73 , C07C49/427 , C07C49/623
摘要： Perfume compositions, perfumed materials and perfumed articles containing derivatives of spiro [5.5] undecane-3-one and/or undecene-3-one having the following formula ##STR1## wherein R.sub.1 and R.sub.2 are hydrogen or methyl and the dotted line is a single or double bond with the proviso that when this dotted line is a double bond R.sub.1 and R.sub.2 are both hydrogen.The use of one or more derivatives of spiro [5.5] undecane-3-one and/or -undecene-3-one having formula 1 as a perfume component in perfume compositions and in imparting fragrance to materials and articles for example soaps, cleaning preparations and cosmetic preparations.
摘要翻译：包含具有下式（1）的螺[5.5]十一碳烷-3-酮和/或十一碳烯-3-酮的衍生物的香料组合物，加香材料和香料制品其中R1和R2是氢或甲基，虚线是单键或双键，条件是当该虚线为双键时，R 1和R 2均为氢。使用一种或多种具有式1的螺[5.5]十一烷-3-酮和/或 - 十一烯-3-酮的一种或多种衍生物作为香料组合物中的香料组分并赋予材料和制品例如肥皂，清洁制剂的香料和化妆品制剂。

9. 发明授权

US4100110A Isolongifolene Prins reaction compounds in perfumery 失效
标题翻译：异龙龙烯香料中的反应化合物
公开(公告)号：US4100110A
公开(公告)日：1978-07-11
申请号：US603908
申请日：1975-08-11
申请人： Hifzur Rahman Ansari , Neville Unwin , Horst Richard Wagner
发明人： Hifzur Rahman Ansari , Neville Unwin , Horst Richard Wagner
IPC分类号： C07C69/02 , A61K8/34 , A61K8/35 , A61L9/01 , A61Q13/00 , C07C27/00 , C07C31/137 , C07C33/05 , C07C33/14 , C07C45/00 , C07C47/115 , C07C47/225 , C07C47/347 , C07C47/445 , C07C49/317 , C07C49/323 , C07C49/553 , C07C49/643 , C07C67/00 , C09K3/00 , C11B9/00 , C11D3/50 , C11D9/44 , D06M13/00 , D06M23/06
CPC分类号： C11B9/0042 , C07C47/347 , C07C47/445 , C07C49/323 , C07C49/553
摘要： Novel compounds of use in perfumery are obtained by performing a Prins reaction on isolongifolene. They include novel primary and secondary alcohols, their esters and the corresponding aldehydes and ketones.
摘要翻译：用于香料的新型化合物是通过对异龙脑烯进行Prins反应而获得的。它们包括新的伯醇和仲醇，它们的酯和相应的醛和酮。

10. 发明授权

US4064184A Norbornanol derivatives 失效
标题翻译：降冰片糖醇衍生物
公开(公告)号：US4064184A
公开(公告)日：1977-12-20
申请号：US740937
申请日：1976-11-11
申请人： Kenneth K. Light , Manfred Hugo Vock , Edward J. Shuster , Frederick Louis Schmitt
发明人： Kenneth K. Light , Manfred Hugo Vock , Edward J. Shuster , Frederick Louis Schmitt
IPC分类号： C07C69/02 , A23G4/00 , A23G4/06 , A23L27/20 , A61K8/33 , A61K8/34 , A61K8/35 , A61K8/37 , A61Q13/00 , C07C27/00 , C07C31/137 , C07C33/05 , C07C35/29 , C07C41/00 , C07C43/115 , C07C43/162 , C07C43/305 , C07C45/00 , C07C49/317 , C07C49/527 , C07C67/00 , C07C239/00 , C07C251/44 , C07D303/04 , C11B9/00 , C07C35/21
CPC分类号： A23G4/06 , C07C35/29 , C11B9/0046 , C11D3/0084
摘要： Processes and compositions are described for the use in foodstuff, chewing gum, toothpaste and medicinal product flavor and aroma and perfume aroma augmenting, enhancing, modifying and imparting compositions and as foodstuff, chewing gum, toothpaste, medicinal product, perfume and perfumed article aroma imparting materials of 3,3-dimethyl-2(3-butenyl) norbornanol-2 (hereinafter referred to as the "norbornanol derivative" having the structure: ##STR1## (which structure is intended to cover both the "endo" and the "exo" isomers thereof) produced by a process which comprises reacting an allylic Grignard reagent having the structure: ##STR2## wherein X is chloro, bromo or iodo with camphene oxide having the structure: ##STR3## by either "exo" camphene oxide or "endo" camphene oxide or a mixture of "exo" and "endo" camphene oxide. Addition of the said norbornanol derivative to consumable materials is indicated to produce:A. In foodstuffs, foodstuff flavorings, chewing gums, toothpastes and medicinal products, sweet, fruity, berry-like aromas with woody, incense-like, cedarwood-like, tea-like and floral nuances and incense-like and cedarwood-like flavors with rosey, berry and tea-like nuances; andB. In perfumes, colognes and perfumed articles, sweet, woody, thujone-like aromas with strong fir-balsam, armoise, cedarleaf, piney, earthy and camphoraceous nuances.
摘要翻译：描述了用于食品，口香糖，牙膏和药用产品风味和芳香和香料香气的方法和组合物，其增强，增强，改性和赋予组合物以及作为食品，口香糖，牙膏，药用产品，香料和香料制品香气赋予 3,3-二甲基-2（3-丁烯基）降冰片烷醇-2的材料（以下称为“降冰片醇衍生物”，具有以下结构：（该结构旨在涵盖“endo”和“exo 通过包括使具有以下结构的烯丙基格利雅试剂（其中X为氯，溴或碘）与具有以下结构的camp氧化物反应的方法制得的：其异构体：通过“外部”camp oxide或“内氧化camp oxide oxide or：camp camp camp camp camp camp camp camp camp camp camp camp：：：：：：：：：：：：：：：：：

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