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1. 发明授权

US06194616B1 Acylation method for an aromatic compound 失效
标题翻译：芳香族化合物的酰化方法
公开(公告)号：US06194616B1
公开(公告)日：2001-02-27
申请号：US09202666
申请日：1999-04-06
申请人： Michel Spagnol , Laurent Gilbert , Henri Guillot , Philippe-Jean Tirel
发明人： Michel Spagnol , Laurent Gilbert , Henri Guillot , Philippe-Jean Tirel
IPC分类号： C07C4545
CPC分类号： C07C45/46 , C07B41/06 , Y02P20/582
摘要： The present invention concerns a process for acylation of an aromatic compound. The acylation process of the invention consists of reacting the aromatic compound with an acylation agent in the presence of a zeolitic catalyst, and is characterized in that it consists of: mixing the aromatic compound and the acylation compound in any manner; passing said mixture over a catalytic bed comprising at least one zeolite; recirculating the reaction mixture from the catalytic bed over the catalytic bed for a number of times which is sufficient to obtain the desired degree of conversion of the substrate.
摘要翻译：本发明涉及一种酰化芳族化合物的方法。本发明的酰化方法包括在沸石催化剂存在下使芳族化合物与酰化剂反应，其特征在于它包括：将芳族化合物和酰化化合物;将所述混合物通过包含至少一种沸石的催化床;将催化床上的反应混合物在催化床上再循环多次，其足以获得所需的转化率基质。

2. 发明授权

US06420608B1 Process for the preparation of trifluoromethyl acetophenone 失效
标题翻译：制备三氟甲基苯乙酮的方法
公开(公告)号：US06420608B1
公开(公告)日：2002-07-16
申请号：US09446233
申请日：1999-12-16
申请人： Adriano Indolese
发明人： Adriano Indolese
IPC分类号： C07C4545
CPC分类号： C07C45/54 , C07C17/12 , C07C45/513 , C07C45/516 , C07C25/13
摘要： A process for the preparation of a compound of formula I wherein Y is a group that is inert during preparation of the compound and m is from 0 to 4 is described. The process broadly involves the steps of a) reacting a compound of formula II wherein X is chlorine, bromine or iodine, and Y and m are as defined above, with a vinylether or an enamide in a solvent, a base and a catalytic amount of a palladium compound and a phosphine ligand. The resulting intermediate is then hydrolyzed to the compound of formula I.
摘要翻译：制备式I化合物的方法，其中Y是在制备化合物中为惰性的基团，m为0至4。该方法广泛地涉及以下步骤：a）使式II化合物，其中X是氯，溴或碘，Y和m如上定义，与乙烯基醚或烯酰胺在溶剂，碱和催化量的钯化合物和膦配体。然后将所得中间体水解成式I化合物。

3. 发明授权

US06800785B1 Process for the synthesis of estrogen receptor modulators 失效
标题翻译：合成雌激素受体调节剂的方法
公开(公告)号：US06800785B1
公开(公告)日：2004-10-05
申请号：US10685719
申请日：2003-10-15
申请人： Dongfang Meng
发明人： Dongfang Meng
IPC分类号： C07C4545
CPC分类号： C07C49/755 , C07C49/747
摘要： The present invention relates to processes for the synthesis of intermediates useful for the synthesis of estrogen receptor modulators. The process includes new methods for annelating 5-, 6- and 7-membered cycloalkenones onto an indanone.
摘要翻译：本发明涉及合成可用于合成雌激素受体调节剂的中间体的方法。该方法包括将5-，6-和7-元环烯酮缩合到茚酮上的新方法。

4. 发明授权

US06380438B1 Process for the production of 3-hydroxypropanal 失效
标题翻译： 3-羟基丙醛生产工艺
公开(公告)号：US06380438B1
公开(公告)日：2002-04-30
申请号：US09615941
申请日：2000-07-13
申请人： George Robert Winter
发明人： George Robert Winter
IPC分类号： C07C4545
CPC分类号： C07C47/19 , C07C45/64 , C07C45/75 , C07C47/22
摘要： A process for producing 3-hydroxypropanal includes reacting formaldehyde and acetaldehyde to form an aqueous solution of acrolein; and hydrating the aqueous solution of acrolein to form 3-hydroxypropanal, wherein the aqueous solution of acrolein is capable of being hydrated to 3-hydroxypropanal without having to remove excess formaldehyde or acetaldehyde.
摘要翻译：制备3-羟基丙醛的方法包括使甲醛和乙醛反应形成丙烯醛水溶液; 并将丙烯醛水溶液水合形成3-羟基丙醛，其中丙烯醛水溶液能够水合成3-羟基丙醛而不必除去过量的甲醛或乙醛。

5. 发明授权

US06376717B2 Preparation of astaxanthin 有权
标题翻译：虾青素的制备
公开(公告)号：US06376717B2
公开(公告)日：2002-04-23
申请号：US09813685
申请日：2001-03-19
申请人： George C. Schloemer , Jeffery L. Davis
发明人： George C. Schloemer , Jeffery L. Davis
IPC分类号： C07C4545
CPC分类号： C07C403/24
摘要： The present invention provides a method for preparing astaxanthin from zeaxanthin. Specifically, the present invention provides a method for said conversion using a halogenating agent with the salt of chloric or bromic acid in an inert solvent.
摘要翻译：本发明提供了从玉米黄质制备虾青素的方法。具体地说，本发明提供了一种在惰性溶剂中使用卤化剂与氯酸或溴酸的盐进行所述转化的方法。

6. 发明授权

US06262313B1 Thermal conversion of fatty acid salts to ketones 有权
标题翻译：脂肪酸盐对酮的热转化
公开(公告)号：US06262313B1
公开(公告)日：2001-07-17
申请号：US09469245
申请日：1999-12-22
申请人： Mark T. Holtzapple , Richard R. Davison
发明人： Mark T. Holtzapple , Richard R. Davison
IPC分类号： C07C4545
CPC分类号： C12P7/40 , C07C29/145 , C07C45/54 , C07C49/04 , C07C31/08 , C07C31/10 , C07C31/12 , C07C31/125
摘要： This invention provides a method for thermally converting volatile fatty acid (VFA) salts to ketones by mixing dry calcium salts of VFAs with hot heat transfer agent in an evacuated container, thereby causing thermal decomposition of the calcium salts of VFAs to form ketone-containing vapor and calcium carbonate; and separating the ketone-containing vapor from the calcium carbonate and heat transfer agent by condensing a mixture of ketones from the ketone-containing vapor. This invention also provides a process for conversion of VFA salts, produced by anaerobic fermentation of cellulosic biomass, into liquid fuels, volatile fatty acids, aldehydes, alcohols, and lactic acid.
摘要翻译：本发明提供了一种通过将疏水性容器中的VFAs的干钙盐与热传热剂混合而将挥发性脂肪酸（VFA）盐热转化为酮的方法，从而引起VFA的钙盐的热分解以形成含酮蒸汽和碳酸钙; 并通过将来自含酮蒸气的酮的混合物冷凝来分离含酮蒸汽与碳酸钙和传热剂。本发明还提供了将通过纤维素生物质的厌氧发酵生产的VFA盐转化为液体燃料，挥发性脂肪酸，醛，醇和乳酸的方法。

7. 发明授权

US06459000B1 Process for the liquid phase acylation of aromatic compounds 失效
标题翻译：芳香族化合物的液相酰化方法
公开(公告)号：US06459000B1
公开(公告)日：2002-10-01
申请号：US09817747
申请日：2001-03-26
申请人： Vasant Ramchandra Choudhary , Suman Kumar Jana
发明人： Vasant Ramchandra Choudhary , Suman Kumar Jana
IPC分类号： C07C4545
CPC分类号： C07C45/46 , Y02P20/582 , C07C49/784 , C07C49/788 , C07C49/825 , C07C49/83 , C07C49/84
摘要： The present invention provides a liquid phase process for the acylation of aromatic compound by an acylating agent of the formula (R5R6R7)—Y—Z to obtain the corresponding acylated compound using a solid catalyst comprising a metal oxide of the formula AOx with or without a catalyst support, wherein A is a metallic element selected from Ga, In, Ti, Fe and a mixture of two or more thereof, and x is the number of oxygen atoms required to fulfil the valance requirement of A, wherein the catalyst is pretreated with a dry gas comprising a hydrogen halide in the presence or absence of the aromatic compound to be acylated, contacting the hydrogen halide pretreated catalyst with a liquid reaction mixture comprising the aromatic compound and the acylating agent, cooling the reaction mixture, removing the catalyst from the reaction mixture and then separating the reaction products from the reaction mixture.
摘要翻译：本发明提供了通过式（R5R6R7）-YZ的酰化剂使芳族化合物酰化的液相方法，以使用包含具有或不具有催化剂载体的式AOx的金属氧化物的固体催化剂获得相应的酰化化合物其中A是选自Ga，In，Ti，Fe及其两种或更多种的混合物的金属元素，x是满足A的价格要求所需的氧原子数，其中催化剂用干燥在待酰化的芳族化合物存在或不存在下，将卤化氢气体与卤化氢预处理的催化剂与包含芳族化合物和酰化剂的液体反应混合物接触，冷却反应混合物，从反应混合物中除去催化剂然后将反应产物与反应混合物分离。

8. 发明授权

US06392099B1 Method and apparatus for the preparation of ketones 失效
标题翻译：用于制备酮的方法和装置
公开(公告)号：US06392099B1
公开(公告)日：2002-05-21
申请号：US09394583
申请日：1999-09-13
申请人： Jack S. Warren
发明人： Jack S. Warren
IPC分类号： C07C4545
CPC分类号： C07D261/08 , C07C45/00 , C07C45/48 , C07C49/293
摘要： A method for continuously producing a ketone in a tube reactor at elevated weight hourly space velocities and in the presence of a catalyst from feed material comprised of a first carboxylic acid or aldehyde or their derivatives and a second carboxylic acid and a method for using the ketone production method to produce herbicidal or other agricultural compounds.
摘要翻译：一种在升高的重量时空速下和在由第一羧酸或醛或其衍生物和第二羧酸组成的原料的催化剂存在下在管式反应器中连续生产酮的方法和使用该酮生产除草剂或其他农用化合物的方法。

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