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1. 发明授权

US06303099B1 Process for producing pentacyl-type crystalline zeolites and a process for producing &egr;-caprolactam using the same 有权
标题翻译：制备戊酰基型结晶沸石的方法和使用该方法制备ε-己内酰胺的方法
公开(公告)号：US06303099B1
公开(公告)日：2001-10-16
申请号：US09605473
申请日：2000-06-28
申请人： Hiroshi Ichihashi , Keisuke Sugita , Makoto Yako
发明人： Hiroshi Ichihashi , Keisuke Sugita , Makoto Yako
IPC分类号： C01B3936
CPC分类号： C01B39/40 , B01J29/40 , C07D201/04 , Y02P20/52 , Y10S423/22 , Y10S423/29 , Y10S423/34
摘要： A process for producing a pentacyl-type crystalline zeolite is provided which comprises the steps of (i) preparing a mixture of a silicon compound, water and tetrapropyl ammonium hydroxide, (ii) conducting a hydrothermal reaction of the mixture to obtain a reaction mixture containing zeolite crystals, (iii) separating zeolite crystals from the reaction mixture to collect a remaining solution, (iv) calcinating the resulting zeolite crystals, (v) treating the calcinated zeolite crystals with a solution such as ammonia water and (vi) recycling the solution collected in step (iii) to step (i), wherein in the mixture prepared in step (i) a molar ratio of hydroxide ion to silicon is from about 0.1 to about 0.4 and a molar ratio of potassium to silicon is about 0.1 or less. With this process, a zeolite catalyst having good performance can be produced with good reproducibility.
摘要翻译：提供了一种制备五酰基型结晶沸石的方法，其包括以下步骤：（i）制备硅化合物，水和四丙基氢氧化铵的混合物，（ii）进行混合物的水热反应，得到含有沸石晶体，（iii）从反应混合物中分离沸石晶体以收集剩余溶液，（iv）煅烧所得沸石晶体，（v）用溶液如氨水处理煅烧的沸石晶体，和（vi）回收溶液在步骤（iii）至步骤（i）中收集，其中在步骤（i）中制备的混合物中，氢氧根离子与硅的摩尔比为约0.1至约0.4，并且钾与硅的摩尔比为约0.1或更小。通过该方法，可以以良好的再现性制造具有良好性能的沸石催化剂。

2. 发明授权

US06521207B2 Molding of binderless zeolite, method for production thereof, and uses thereof 有权
公开(公告)号：US06521207B2
公开(公告)日：2003-02-18
申请号：US09975472
申请日：2001-10-11
申请人： Tomoharu Oku , Hideaki Tsuneki
发明人： Tomoharu Oku , Hideaki Tsuneki
IPC分类号： C01B3936
CPC分类号： C01B39/02 , B01J29/40 , B01J2229/36 , Y10S423/22 , Y10S423/27 , Y10S423/29
摘要： A method for producing a molding of binderless zeolite by exposing to saturated steam a precursor having a tetraalkylammonium salt component, an alkali metal component, and a metal component incorporated in the crystal skeleton of zeolite supported on a molding using silica as a main component, the molding of binderless zeolite, and use of the molding as a catalyst for the production of an alkanolamine.

3. 发明授权

US06444191B1 Zeolite ZSM-11 and a process for preparing zeolite ZSM-11 using a 3,5-dimethylpiperidinium templating agent 失效
标题翻译：沸石ZSM-11和使用3,5-二甲基哌啶模板剂制备沸石ZSM-11的方法
公开(公告)号：US06444191B1
公开(公告)日：2002-09-03
申请号：US09296019
申请日：1999-04-21
申请人： Yumi Nakagawa
发明人： Yumi Nakagawa
IPC分类号： C01B3936
CPC分类号： C01B39/12 , C01B37/02 , C01B39/365 , Y10S423/29
摘要： The present invention relates to a process for preparing the zeolite ZSM-11 using 3,5-dimethylpiperidinium compounds as an organic templating agent, and to the zeolite ZSM-11 in the pure phase form.
摘要翻译：本发明涉及使用3,5-二甲基哌啶鎓化合物作为有机模板剂制备沸石ZSM-11的方法和纯相形式的沸石ZSM-11。

4. 发明授权

US06419894B1 Process for preparing zeolites having MEL structure using 2,2-diethoxyethyltrimethylammonium structure directing agent 有权
标题翻译：使用2,2-二乙氧基乙基三甲基铵结构导向剂制备具有MEL结构的沸石的方法
公开(公告)号：US06419894B1
公开(公告)日：2002-07-16
申请号：US09823669
申请日：2001-03-30
申请人： Patrick M. Piccione , Mark E. Davis
发明人： Patrick M. Piccione , Mark E. Davis
IPC分类号： C01B3936
CPC分类号： C01B37/005 , C01B37/00 , C01B37/02 , C01B37/04 , C01B37/08 , C01B39/04 , C01B39/12 , Y10S423/29
摘要： Zeolites having the MEL crystal structure are made using 2,2-diethoxyethyltrimethylammonium cation as the structure directing agent.
摘要翻译：具有MEL晶体结构的沸石使用2,2-二乙氧基乙基三甲基铵阳离子作为结构导向剂。

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