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1. 发明授权

US6037289A Titanium dioxide-based photocatalytic coating substrate, and titanium dioxide-based organic dispersions 失效
标题翻译：二氧化钛基光催化涂层基体和二氧化钛基有机分散体
公开(公告)号：US6037289A
公开(公告)日：2000-03-14
申请号：US43063
申请日：1998-03-12
申请人： Thierry Chopin , Dominique Dupuis , Corinne Lehaut , Pascal Chartier , Xavier Talpaert
发明人： Thierry Chopin , Dominique Dupuis , Corinne Lehaut , Pascal Chartier , Xavier Talpaert
IPC分类号： B01J35/02 , B01J35/00 , C01G23/047 , C03C8/20 , C03C17/00 , C03C17/245 , C03C17/25 , C04B41/50 , C04B41/52 , C09D1/00 , C09D5/00 , C09D17/00 , C23C18/12 , C23C26/00 , C23C30/00 , B01J33/00 , B01J101/50 , B05D5/00
CPC分类号： C23C30/00 , B82Y30/00 , C01G23/047 , C03C17/007 , C03C17/008 , C03C17/2456 , C03C17/256 , C03C8/20 , C04B41/5041 , C04B41/52 , C09D1/00 , C09D17/008 , C23C18/1216 , C23C18/1225 , C23C18/1245 , C23C18/1254 , C23C18/1258 , C23C18/127 , C23C18/1295 , C23C26/00 , B01J35/002 , C01P2002/02 , C01P2002/50 , C01P2004/64 , C01P2004/86 , C01P2006/60 , C01P2006/82 , C03C2217/212 , C03C2217/29 , C03C2217/45 , C03C2217/477 , C03C2217/71 , Y10S502/522
摘要： The invention relates to a substrate provided, on at least a portion of one of its faces, with a coating with a photocatalytic property based on titanium dioxide which is at least partially crystalline and which is incorporated in the said coating partly in the form of particles predominantly crystallized in the anatase form. The invention also relates to a process for the preparation of this substrate and organic dispersions of titanium dioxide particles used in the said process for the preparation of the substrate.
摘要翻译： PCT No.PCT / FR96 / 01419 Sec。 371日期1998年3月12日 102（e）1998年3月12日PCT PCT 1996年9月13日PCT公布。公开号WO97 / 10185 日期1997年3月20日本发明涉及一种在其一个面的至少一部分上具有基于二氧化钛的光催化性能的涂层，该涂层至少部分结晶并且部分地结合到所述涂层中以主要以锐钛矿形式结晶的颗粒的形式。本发明还涉及用于制备该底物的方法和用于制备底物的所述方法中使用的二氧化钛颗粒的有机分散体。

2. 发明授权

US5750459A Sol-gel process for obtaining pure and mixed oxide zirconia spheres, microspheres and washcoats, useful as catalysts or catalyst supports 失效
标题翻译：用于获得纯和混合的氧化锆球体，微球和洗面漆的溶胶 - 凝胶法，可用作催化剂或催化剂载体
公开(公告)号：US5750459A
公开(公告)日：1998-05-12
申请号：US570684
申请日：1995-12-11
申请人： Marcello Marella , Letizia Meregalli , Michele Tomaselli
发明人： Marcello Marella , Letizia Meregalli , Michele Tomaselli
IPC分类号： B01J13/00 , B01J21/06 , B01J23/10 , B01J23/46 , B01J23/72 , B01J37/02 , B01J37/03 , C01G25/00 , C01G25/02 , B01J23/63 , B01J35/08 , B01J101/50
CPC分类号： B82Y30/00 , B01J13/00 , B01J21/066 , B01J37/0215 , B01J37/038 , C01G25/00 , C01G25/006 , C01G25/02 , C01P2002/60 , C01P2004/03 , C01P2004/32 , C01P2004/64 , C01P2006/12 , C01P2006/13 , C01P2006/14 , C01P2006/16 , C01P2006/22 , C01P2006/80 , C01P2006/90
摘要： This invention relates to a process for obtaining pure or mixed oxide zirconia spheres, microspheres or washcoats consisting of: preparing a zirconium solution in water at a concentration, formally expressed as ZrO.sub.2, equal or lower than 400 g/l, starting from a basic zirconium carbonate additioned of conc. nitric acid up to a molar ratio �NO.sub.3.sup.- !/�Zr.sup.4+ ! between 0.8 and 1.1, and eventually preparing one or more solutions of the other oxides when necessary; preparing a sol of zirconium, eventually mixed to other metals, by a thickening agent and, in the case of spheres and microspheres, of a surface active agent too; dripping the sol into an alkaline gelation bath for obtaining gel spheres or microspheres, or sucking the sol into the honeycomb channels in order to obtain the washcoats, with subsequent gelation with gaseous ammonia; ageing the so obtained gel; rinsing with water down to pH=9-10, only in the case of gel spheres or microspheres; drying and calcining.
摘要翻译：本发明涉及一种获得纯氧化锆或混合氧化锆球体，微球或洗面漆的方法，该方法包括：以ZrO 2的正式表示的浓度制备锆溶液，其浓度等于或低于400g / l，从碱性锆碳酸盐添加浓缩物硝酸至0.8〜1.1之间的摩尔比[NO 3 - ] / [Zr 4+]，并在必要时最终制备其它氧化物的一种或多种溶液; 通过增稠剂制备锆的溶胶，最终与其它金属混合，在球体和微球的情况下，也可以制备表面活性剂; 将溶胶滴入碱性凝胶浴中以获得凝胶球或微球，或将溶胶吸入蜂窝通道中以获得洗面漆，随后用气态氨凝胶化; 老化所得凝胶; 用水冲洗至pH = 9-10，仅在凝胶球或微球的情况下; 干燥和煅烧。

3. 发明授权

US6147024A Catalyst systems for improved stereoselectivity and broader molecular weight distribution in polymerization of olefins 有权
标题翻译：用于烯烃聚合中改进的立体选择性和较宽分子量分布的催化剂体系
公开(公告)号：US6147024A
公开(公告)日：2000-11-14
申请号：US351025
申请日：1999-07-12
申请人： Edwar S. Shamshoum , David John Rauscher , Douglas Alan Burmaster
发明人： Edwar S. Shamshoum , David John Rauscher , Douglas Alan Burmaster
IPC分类号： C08F4/646 , C08F4/649 , C08F4/658 , C08F10/00 , B01J101/00 , B01J101/10 , B01J101/40 , B01J101/50
CPC分类号： C08F10/00 , Y02P20/52
摘要： The present invention provides a catalyst for the polymerization of olefin that exhibits improved selectivity and broader molecular weight distribution in the polymer product. The catalyst is a conventional supported Ziegler-Natta catalyst in combination with a mixture of at least two electron donors, both having the general formula SiR.sub.m (OR').sub.4-m where R is selected from the group consisting of an alkyl group, a cycloalkyl group, an aryl group and a vinyl group; R' is an alkyl group; and m is 0-3, wherein when R is an alkyl group, R may be identical with R'; when m is 0, 1 or 2, the R' groups may be identical or different; and when m is 1, 2 or 3, the R groups may be identical or different. This catalyst produces polypropylene having xylene solubles of 1-7 to 5.1 wt % and a molecular weight distribution of about 10.
摘要翻译：本发明提供了一种用于聚合烯烃的催化剂，其在聚合物产品中表现出改进的选择性和较宽的分子量分布。催化剂是与至少两个电子给体的混合物组合的常规负载的齐格勒 - 纳塔催化剂，两者都具有通式SiRm（OR'）4-m，其中R选自烷基，环烷基基团，芳基和乙烯基; R'是烷基; 并且m为0-3，其中当R为烷基时，R可以与R'相同; 当m为0,1或2时，R'可以相同或不同; 当m为1,2或3时，R基团可以相同或不同。该催化剂产生具有1-7至5.1重量％的二甲苯可溶物和约10的分子量分布的聚丙烯。

4. 发明授权

US5723404A Process for the production of mixed oxide powders for catalysts for the removal of nitrogen oxides 失效
标题翻译：用于生产用于除去氮氧化物的催化剂的混合氧化物粉末的方法
公开(公告)号：US5723404A
公开(公告)日：1998-03-03
申请号：US649924
申请日：1996-05-16
申请人： Kai Butje , Jurgen Kischkewitz , Rolf Michael Braun , Udo Holtmann , Peter-Joachim Barenthien
发明人： Kai Butje , Jurgen Kischkewitz , Rolf Michael Braun , Udo Holtmann , Peter-Joachim Barenthien
IPC分类号： B01D53/86 , B01D53/94 , B01J21/06 , B01J23/22 , B01J23/28 , B01J23/30 , B01J37/02 , B01J101/50
CPC分类号： B01J21/063 , B01D53/8628 , B01J37/0236
摘要： A process for the production of a mixed oxide powder, that contains as chief constituent TiO.sub.2 in the form of anatase and as minor constituents at least one of the catalytically active oxides MoO.sub.3, WO.sub.3 and V.sub.2 O.sub.5, suitable for use as a catalyst for the removal of nitrogen oxides, comprising (a) partially neutralizing a titanium dioxide hydrate suspension containing sulphuric acid with an alkaline liquor to a pH value between about 4.0 and 6.0 at temperatures between about 20.degree. and 100.degree. C., (b) filtering the suspension from (a) to produce a filter cake and intensively washing the filter cake, (c) adding to the filter cake from (b) at least one water-soluble salt of at least one of the metals Mo, W and V in solid or dissolved form, and (d) drying the filter cake from (c) and calcining it at a temperature between about 300.degree. and 750.degree. C.
摘要翻译：一种混合氧化物粉末的制造方法，其包含主要成分为锐钛矿形式的TiO 2和作为少量成分的至少一种催化活性氧化物MoO 3，WO 3和V 2 O 5的方法，适合用作除去氮氧化物，其包含（a）在约20℃至100℃的温度下，将含有碱性液的硫酸的二氧化钛水合物悬浮液部分中和至约4.0至6.0之间的pH值，（b）将（ a）生产滤饼并强烈地洗涤滤饼，（c）从（b）至少一种金属Mo，W和V的至少一种水溶性盐固体或溶解形式的滤饼中加入滤饼，（d）将（c）的滤饼干燥，并在约300〜750℃的温度下煅烧。

5. 发明授权

US5686372A Photocatalyst with modified alkyl silicate ester support and process for production thereof 失效
标题翻译：具有改性的烷基硅酸酯酯载体的光催化剂及其制备方法
公开(公告)号：US5686372A
公开(公告)日：1997-11-11
申请号：US451650
申请日：1995-05-26
申请人： Cooper H. Langford , Giuseppe P. Lepore , Lalchan Persaud
发明人： Cooper H. Langford , Giuseppe P. Lepore , Lalchan Persaud
IPC分类号： B01J21/06 , B01J21/08 , B01J23/30 , B01J31/02 , B01J35/00 , B01J35/02 , B01J37/02 , B01J101/42 , B01J101/50
CPC分类号： B01J31/0212 , B01J31/0274 , B01J35/002 , B01J35/004 , B01J21/08 , B01J37/0209 , Y02W10/37
摘要： A photocatalyst compound comprising a silica-based support material having bound thereto a photocatalyst selected from the group consisting of TiO.sub.2, WO.sub.3 and mixtures thereof, the photocatalyst compound having been derivatized by reaction with an alcohol compound. The process for producing the photocatalyst compound comprises the steps of: (i) contacting a silica-based support material having bound thereto a photocatalyst selected from the group consisting of TiO.sub.2, WO.sub.3 and mixtures thereof with an alcohol compound to form a slurry; (ii) maintaining the temperature of the slurry above the boiling point of the slurry to produce a substance having a modified surface consisting essentially of an alkyl silicate ester and esterified photocatalyst; and (iii) subjecting the substance to selective oxidation to oxidize the esterfied photocatalyst thereby producing a photocatalyst compound having a modified surface consisting essentially of an alkyl silicate ester and a photocatalyst substantially free of ester groups. The photocatalyst compound is useful, inter alia, in the treatment of a fluid containing an organic pollutant.
摘要翻译：一种光催化剂化合物，其包含与其结合的二氧化硅基载体材料，所述光催化剂选自TiO 2，WO 3及其混合物，所述光催化剂化合物已经通过与醇化合物的反应衍生化。制备光催化剂化合物的方法包括以下步骤：（i）将结合有光催化剂的二氧化硅基载体材料与选自TiO 2，WO 3的混合物与醇化合物接触以形成浆料; （ii）将浆料的温度保持在浆料沸点之上，以产生具有主要由烷基硅酸酯和酯化的光催化剂组成的改性表面的物质; 和（iii）对物质进行选择性氧化以氧化酯化的光催化剂，从而制备具有基本上由烷基硅酸酯和基本上不含酯基的光催化剂组成的改性表面的光催化剂化合物。光催化剂化合物尤其用于处理含有机污染物的流体。

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