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    • 4. 发明授权
    • Processes for preparing copolymers
    • 制备共聚物的方法
    • US6124409A
    • 2000-09-26
    • US929457
    • 1992-08-12
    • T. Hwee NgHadi K. MahabadiMan C. TamGregory J. KovacsEric M. PetersRafik O. Loutfy
    • T. Hwee NgHadi K. MahabadiMan C. TamGregory J. KovacsEric M. PetersRafik O. Loutfy
    • C08F2/00C08F2/06C08F2/18C08F4/38
    • C08F2/001C08F2/06Y10S526/921
    • Disclosed is a process for preparing copolymers which comprises, in the order stated: (1) adding monomers containing unsaturated carbon-to-carbon bonds, a first polymerization initiator, a second polymerization initiator, and a solvent to a reaction vessel; (2) purging the resulting solution with an inert gas; (3) sealing the reaction vessel and pressurizing it by addition of an inert gas to a pressure of from about 20 to about 600 kilopascals over ambient atmospheric pressure; (4) maintaining the temperature within the pressurized reaction vessel at a temperature of from about 50 to about 100.degree. C. for a period of from about 60 to about 300 minutes; (5) thereafter maintaining the temperature within the pressurized reaction vessel at a temperature of from about 80 to about 115.degree. C. for a period of from about 30 to about 300 minutes, wherein the temperature in step (5) is higher than the temperature in step (4); and (6) subsequently maintaining the temperature within the pressurized reaction vessel at a temperature of from about 115 to about 160.degree. C. for a period of from about 30 to about 180 minutes, wherein the temperature in step (6) is higher than the temperature in step (5). Polymers prepared according to the process of the present invention can be particularly useful in migration imaging members.
    • 公开了一种制备共聚物的方法,其顺序包括:(1)向反应容器中加入含有不饱和碳 - 碳键的单体,第一聚合引发剂,第二聚合引发剂和溶剂; (2)用惰性气体吹扫所得溶液; (3)密封反应容器并通过在环境大气压下加入约20至约600千帕斯卡的惰性气体对其加压; (4)将加压反应容器内的温度维持在约50至约100℃的温度下约60至约300分钟; (5)之后将加压反应容器内的温度保持在约80至约115℃的温度下约30至约300分钟的时间,其中步骤(5)中的温度高于温度 在步骤(4)中; 和(6)随后将加压反应容器内的温度保持在约115至约160℃的温度下约30至约180分钟的时间,其中步骤(6)中的温度高于 步骤(5)中的温度。 根据本发明的方法制备的聚合物可以在迁移成像构件中特别有用。