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1. 发明授权

US09765167B2 Reverse-phase polymerisation process 有权
公开(公告)号：US09765167B2
公开(公告)日：2017-09-19
申请号：US14908925
申请日：2014-07-29
申请人： BASF SE
发明人： Robert Haschick , Aleksandra Jelicic , John Scott Barratt , Pascal Hesse , Oliver Soetje , Gabriela Eugenia Fonseca Zepeda , Shankara Narayanan Keelapandal Ramamoorthy , Bjoern Langlotz
IPC分类号： C08F2/46 , C08F2/50 , C08G61/04 , C08F220/56 , C08F2/32 , B01J19/12 , B01J19/24 , C08F220/06 , C08F220/20 , C08F226/10 , C08F220/38
CPC分类号： C08F220/56 , B01J19/123 , B01J19/24 , B01J2219/0869 , B01J2219/1203 , B01J2219/24 , C08F2/32 , C08F220/06 , C08F220/20 , C08F226/10 , C08F2220/382 , C08F2220/385 , C08F220/34
摘要： A reverse-phase suspension polymerization process for the manufacture of polymer beads comprising forming aqueous monomer beads comprising an aqueous solution of water-soluble ethylenically unsaturated monomer or monomer blend and polymerizing the monomer or monomer blend to form polymer beads while suspended in a non-aqueous liquid, and recovering polymer beads, in which the process comprises, providing in a vessel (1) a volume (2) of non-aqueous liquid wherein the volume of non-aqueous liquid extends between at least one polymer bead discharge point (3) and at least one monomer feed point (4), feeding the aqueous monomer or monomer blend through orifices (5) into, or onto, the non-aqueous liquid to form aqueous monomer beads, allowing the aqueous monomer beads to flow towards the polymer bead discharge point subjecting the aqueous monomer beads to polymerization conditions to initiate polymerization to form polymerizing beads, wherein the polymerizing beads have formed polymer beads when they reach the polymer bead discharge point, removing a suspension of the polymer beads in non-aqueous liquid from the vessel at the polymer bead discharge point and recovering water soluble or water swellable polymer beads from the suspension. The invention also relates to the apparatus suitable for carrying out a reverse-phase suspension polymerization and polymer beads obtainable by the process or employing the apparatus.

2. 发明授权

US09724670B2 Water absorbent polymers and a process for their preparation 有权
公开(公告)号：US09724670B2
公开(公告)日：2017-08-08
申请号：US15106160
申请日：2014-12-22
申请人： Reliance Industries Limited
发明人： Elango Subramanyam , Manjeet Singh Choudhary , Raksh Vir Jasra , Ashishkumar Indravadan Parekh , Pralhad Ambadas Ganeshpure , Padmavathi Garimella , Jayesh Prafullachandra Vora
IPC分类号： C08F2/00 , C08F20/06 , C08F118/02 , B01J20/26 , C08F2/08 , C08F2/14 , C08F2/32 , C08F6/14 , B01J20/28 , B01J20/30 , C08F220/06
CPC分类号： B01J20/261 , B01J20/267 , B01J20/28016 , B01J20/3028 , C08F2/08 , C08F2/14 , C08F2/32 , C08F6/14 , C08F220/06
摘要： Water absorbent polymers and a process for their preparation are disclosed. The process for preparing water absorbent polymers comprises preparing a slurry with relatively high amounts of polymer particles (in the range of 40 to 55 wt % of the total mass of the slurry) having water absorbed therein. The slurry is then directly spray dried to obtain water absorbent polymers.

3. 发明申请

US20170218096A1 WATER-ABSORBENT RESIN AND ABSORBENT ARTICLE 审中-公开
公开(公告)号：US20170218096A1
公开(公告)日：2017-08-03
申请号：US15324764
申请日：2014-11-04
申请人： Sumitomo Seika Chemicals Co. Ltd.
发明人： Hiroki Yabuguchi , Tetsuhiro Hinayama , Maoki Hama , Hideki Yokoyama
IPC分类号： C08F8/14 , B01J20/26 , A61L15/60 , A61L15/24
CPC分类号： C08F8/14 , A61F13/49 , A61F13/53 , A61L15/24 , A61L15/60 , B01J20/267 , C08F2/32 , C08F8/00 , C08F220/06 , C08J3/24 , C08F220/02 , C08F2222/1013
摘要： Provided are: a water-absorbent resin which, when used as an absorbent material, retains a high water-absorption performance, increases the diffusivity of a to-be-absorbed liquid and makes it possible to effectively decrease the amount of re-wet; and an absorbent article formed using an absorbent material including the water-absorbent resin. The water-absorbent resin according to the present invention is a water-absorbent resin obtained by polymerizing a water-soluble ethylenically monomer in the presence of an internal-crosslinking agent and thereafter post-crosslinking the polymer with a post-crosslinking agent, characterized in that when subjected to a liquid flow test, the water-absorbent resin has an effective absorbent material index (K) indicated by equation (I) of 250 or greater. Effective absorbent material index (K)=[(the amount of liquid flow) (g)]×[(artificial-urine absorption ratio) (g/g)] (I)

4. 发明申请

US20170204212A1 INVERSE DISPERSION COMPRISING A CATIONIC POLYMER, A STABILIZING AGENT AND A TRIFUNCTIONAL AND/OR POLYFUNCTIONAL CROSSLINKER 审中-公开
公开(公告)号：US20170204212A1
公开(公告)日：2017-07-20
申请号：US15327865
申请日：2015-06-26
申请人： BASF SE
发明人： Reinhold J Leyrer , Gledison Fonseca , Volodymyr Boyko , Mark Robert Sivik , Travis Kyle Hodgdon
IPC分类号： C08F220/56 , A61K8/81 , A61Q19/00 , C11D3/00 , A61Q5/00
CPC分类号： C08F220/56 , A61K8/04 , A61K8/8158 , A61K2800/48 , A61K2800/5426 , A61Q5/00 , A61Q19/00 , C08F2/14 , C08F2/32 , C08F220/34 , C11D3/001 , C08F2222/1026 , C08F2222/104 , C08F222/385 , C08F216/125
摘要： The present invention relates to an inverse dispersion including at least one cationic polymer and at least one stabilizing agent as well as at least a tri- and/or polyfunctional crosslinker wherein the stabilizing agent has one or more hydrophobic chains with more than 30 carbon atoms. The polymer is obtainable by polymerizing at least one cationic monomer and optionally at least one nonionic monomer. Furthermore, the present invention relates to a process for manufacturing the inverse dispersion by inverse emulsion polymerization.

5. 发明申请

US20170204210A1 WATER-SOLUBLE HYDROXYALKYL POLYMER OBTAINED BY A METHOD OF INVERSE SUSPENSION OR INVERSE EMULSION POLYMERISATION 有权
公开(公告)号：US20170204210A1
公开(公告)日：2017-07-20
申请号：US15326603
申请日：2015-07-24
申请人： S.P.C.M. SA
发明人： Pierrick CHEUCLE
IPC分类号： C08F220/06 , D21H19/10 , C09K8/035
CPC分类号： C08F220/06 , C08F2/32 , C08F2/38 , C09K8/035 , D21H19/10 , C08F220/20
摘要： This invention relates to a water-soluble polymer in bead or powder form, characterized in that it has a Brookfield viscosity greater than 100 cps, and in that it is obtained by inverse suspension or inverse emulsion polymerization, in the presence of a transfer agent, of monomers where less than 20 mol % is made up of a hydroxyalkyl monomer with formula H2C═CR1R2, R1 being a hydrogen atom or a methyl group and R2 being a hydrocarbon group containing at least one OH pendant group or at least one epoxide group and optionally at least one N or O heteroatom in the hydrocarbon chains; R2 being different from the C(═O)—OH group.

6. 发明申请

US20160376390A1 METHODS OF MAKING ACRYLAMIDE-ACRYLIC ACID COPOLYMERS 审中-公开
标题翻译：制备丙烯酰胺 - 丙烯酸共聚物的方法
公开(公告)号：US20160376390A1
公开(公告)日：2016-12-29
申请号：US15190364
申请日：2016-06-23
申请人： Ecolab USA Inc.
发明人： Stephen Marrou , Xiangyang Zhu , Heqing Huang
IPC分类号： C08F222/38 , C08L71/02
CPC分类号： C08L71/02 , C08F2/32 , C08F220/56 , C09K8/588 , C08F220/06
摘要： A method of making acrylamide-acrylic acid copolymers in water-in-oil latices is described. The method results in a copolymer having randomly distributed carboxylate functionalities and is suitable for ionic crosslinking. The copolymers and their ionically crosslinked counterparts are useful for enhanced oil recovery processes.
摘要翻译：描述了一种在油包水胶乳中制备丙烯酰胺 - 丙烯酸共聚物的方法。该方法产生具有随机分布的羧酸酯官能团并且适用于离子交联的共聚物。共聚物及其离子交联对应物可用于增强采油工艺。

7. 发明授权

US09474990B2 Processes for recovering organic solvent extractant from solid-stabilized emulsions formed in hydrometallurgical solvent extraction circuits 有权
标题翻译：从在湿法冶金溶剂萃取回路中形成的固体稳定乳液中回收有机溶剂萃取剂的方法
公开(公告)号：US09474990B2
公开(公告)日：2016-10-25
申请号：US13600390
申请日：2012-08-31
申请人： Matthew D. Soderstrom , Christopher Sexton
发明人： Matthew D. Soderstrom , Christopher Sexton
IPC分类号： B01D21/01 , C02F1/52 , C22B1/14 , B01D17/04 , C22B3/20 , C22B3/24 , C02F1/56 , C02F1/68 , C22B3/26 , B01D11/00 , C02F1/00 , B03D3/00 , C22B1/00 , C08F2/32 , C08F26/06 , C02F1/40 , C02F103/16
CPC分类号： B01D17/04 , B01D17/047 , C02F1/40 , C02F1/5236 , C02F1/56 , C02F1/681 , C02F2103/16 , C08F2/32 , C08F26/06 , C22B3/0005 , C22B3/20 , C22B3/205 , C22B3/24 , Y02P10/234
摘要： Processes for recovering an organic solvent extractant phase from a solid-stabilized emulsion formed in a hydrometallurgical solvent extraction circuit are disclosed. One such process includes mixing a de-emulsifier comprising an effective amount of a polymeric aggregating agent with the solid-stabilized emulsion, thereby separating the emulsion into its aqueous, organic, and solid phase components; and removing the organic solvent extractant phase from the other components, thereby recovering the organic solvent extractant phase from the solid-stabilized emulsion.
摘要翻译：公开了从在湿法冶金溶剂萃取回路中形成的固体稳定的乳液中回收有机溶剂萃取相的方法。一种这样的方法包括将包含有效量的聚合物聚集剂的去乳化剂与固体稳定的乳液混合，从而将乳液分离成其水相，有机和固相组分; 从其他成分除去有机溶剂萃取相，由固体稳定化乳液中回收有机溶剂萃取相。

8. 发明授权

US09440255B2 Preparation of porous organic polymeric films 有权
标题翻译：多孔有机聚合物膜的制备
公开(公告)号：US09440255B2
公开(公告)日：2016-09-13
申请号：US14534304
申请日：2014-11-06
申请人： Eastman Kodak Company
发明人： Mridula Nair , Joseph Salvatore Sedita
IPC分类号： B05D5/00 , C09D101/18 , B05D3/00 , B05D3/02 , C08F2/32 , C08J5/18 , C08J9/00 , C08J9/28 , A61L15/42 , A61L15/22
CPC分类号： B05D5/00 , A61L15/225 , A61L15/425 , B05D3/007 , B05D3/02 , C08F2/32 , C08J5/18 , C08J9/0061 , C08J9/283 , C08J2201/05 , C08J2367/04 , C08J2375/06 , C09D101/18
摘要： Porous organic polymeric films having multiple discrete cavities can be prepared by applying a water-in-oil emulsion that includes a cavity stabilizing hydrocolloid on the inner walls of the multiple discrete cavities to a substrate. The multiple discrete cavities can also include organic catalytic materials for various catalytic reactions, markers materials for security applications, or the multiple discrete cavities can be used to increase opacity, hydrophobicity, or other desirable properties compared to nonporous organic polymeric films composed of the composition and dry thickness. Water and oil from the applied water-in-oil emulsion can be removed by evaporation in a suitable process, and the applied porous organic polymeric film can be provided as a uniform material or in a patternwise fashion.
摘要翻译：具有多个离散空腔的多孔有机聚合物膜可以通过在多个分立空腔的内壁上施加包含腔稳定水胶体的油包水乳液制成基底。多个分立的空腔还可以包括用于各种催化反应的有机催化材料，用于安全应用的标记材料或多个离散空腔可用于增加不透明度，疏水性或其它所需的性能，与由组合物组成的无孔有机聚合物膜相比，干厚度。可以通过在合适的方法中蒸发除去来自涂覆的油包水乳液的水和油，并且施加的多孔有机聚合物膜可以以均匀的材料或以图案方式提供。

9. 发明授权

US09416615B2 System and method for improving zonal isolation in a well 有权
标题翻译：改善井中区域隔离的系统和方法
公开(公告)号：US09416615B2
公开(公告)日：2016-08-16
申请号：US13640479
申请日：2011-04-11
申请人： Loic Regnault de la Mothe , Sylvaine Le Roy-Delage
发明人： Loic Regnault de la Mothe , Sylvaine Le Roy-Delage
IPC分类号： E21B33/12 , E21B33/10 , C08F220/56 , C09K8/42 , C08F220/38 , C08F220/60
CPC分类号： E21B33/10 , C08F2/32 , C08F220/38 , C08F220/56 , C08F220/60 , C09K8/422 , E21B33/1208
摘要： A system for improving zonal isolation incorporates a tubular having an outer surface and a swellable coating that coats the outer surface. The swellable coating has an external surface, a composition provided in an annular space outside the tubular, or both. The swellable coating is made of a first swellable material that can swell when contacted by a first fluid on the external surface. The composition is made of a second swellable material that can swell when contacted with second fluid. The first swellable material, the second swellable material, or both, include an elastomer that is compounded with an aqueous inverse emulsion of particles of a polymer comprising a betaine group. The elastomer is able to swell when contacted by hydrocarbons and saline aqueous fluids.
摘要翻译：用于改善区带隔离的系统包括具有外表面和涂覆外表面的可溶胀涂层的管状体。可溶胀涂层具有外表面，组合物设置在管外的环形空间中，或两者。可溶胀涂层由第一可溶胀材料制成，该第一可溶胀材料在外表面上被第一流体接触时可膨胀。该组合物由与第二流体接触时可溶胀的第二溶胀材料制成。第一可溶胀材料，第二可溶胀材料或两者包括与包含甜菜碱基团的聚合物颗粒的水性反相乳液复合的弹性体。当烃和盐水水溶液接触时，弹性体能够溶胀。

10. 发明授权

US09290588B2 Process for low-concentration, inverse emulsion polymerization of weakly neutralized polymers 有权
标题翻译：弱中和聚合物的低浓度，反相乳液聚合方法
公开(公告)号：US09290588B2
公开(公告)日：2016-03-22
申请号：US14177463
申请日：2014-02-11
申请人： S.P.C.M. SA
发明人： Frederic Blondel , Lionel Champagnon
IPC分类号： C08J3/00 , C08F20/06 , C08F2/32 , C08F220/06
CPC分类号： C08F220/06 , C08F2/32 , C08F20/06 , C08F220/10 , C08F220/38 , C08F220/56
摘要： The present invention relates to a process for preparing a polymer by polymerization of an aqueous solution of one or more monomers in water-in-oil inverse emulsion, in which one or more of the monomers used comprise(s) at least one acid function, the molar percentage of monomers bearing at least one weak acid function relative to all the monomers used being at least 30%, wherein: i) the polymerization is carried out with a concentration of all the monomers in aqueous solution which falls within the range of from 1.3 mmol to 3.6 mmol per gram of aqueous solution, ii) during the polymerization, at most 20% of the acid functions present on the monomers which have at least one acid function are in neutralized form, and also to the polymers which can be obtained by means of such a process.
摘要翻译：本发明涉及通过在油包水反相乳液中聚合一种或多种单体的水溶液来制备聚合物的方法，其中使用的一种或多种单体包含至少一种酸官能团，相对于使用的所有单体，具有至少一个弱酸功能的单体的摩尔百分比为至少30％，其中：i）聚合反应以水溶液中所有单体的浓度进行，其浓度范围为 1.3mmol至3.6mmol / g水溶液，ii）在聚合过程中，至少具有一个酸性官能团的单体中存在的酸官能度的至多20％是中和形式，以及可获得的聚合物通过这样一个过程。

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