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1. 发明授权

US4429161A Process for preparing organic tertiary polyphosphine monooxides 失效
标题翻译：制备有机三聚磷酸一氧化物的方法
公开(公告)号：US4429161A
公开(公告)日：1984-01-31
申请号：US293145
申请日：1981-08-17
申请人： Anthony G. Abatjoglou , Louis A. Kapicak
发明人： Anthony G. Abatjoglou , Louis A. Kapicak
IPC分类号： C07F9/53 , C07F9/54
CPC分类号： C07F9/5421 , C07F9/5312 , C07F9/5316
摘要： Process for producing organic tertiary polyphosphine monooxides which comprises reacting an organic tertiary polyphosphine with an organic monofunctional alkylating agent to form an intermediate monophosphonium salt of the polyphosphine starting material and then hydrolyzing the salt so produced to the desired polyphosphine monooxide product.
摘要翻译：制备有机三聚磷膦一氧化物的方法，其包括使有机三聚磷化氢与有机单官能烷基化剂反应以形成多膦原料的中间体单鏻盐，然后水解所生产的盐至所需的一膦一氧化物产物。

2. 发明授权

US3701817A Halogenated phosphorus compounds containing the atom skeleton p-(c-p)2 or p-(c-p)3 and preparation 失效
标题翻译：含有ATOM SKELETON P-（C-P）2或P-（C-P）3的制备的磷酸化合物和制备
公开(公告)号：US3701817A
公开(公告)日：1972-10-31
申请号：US3701817D
申请日：1969-03-28
申请人： MONSANTO CO
发明人： MAIER LUDWIG
IPC分类号： C07F9/38 , C07F9/40 , C07F9/53 , C07F9/32
CPC分类号： C07F9/5312 , C07F9/3808 , C07F9/4006
摘要： COMPOUNDS OF THE FORMULA

P(3EA(OC2H5)B(C(H)CX2-CP(O)(OC2H5)2)3-B

AND PROCESSES FOR MAKING BY HALOGENATING A COMPOUND OF THE FORMULA

P(O)A(OC2H5)B(CH2P(O)OC2H5)2)3-B

THE COMPOUNDS ARE USED AS COMLESING AGENTS AND FLAME-PROOFING AGENTS.

3. 发明授权

US3458581A Tris(disubstituted phosphinylethyl)-phosphine oxides 失效
标题翻译：磷酸三苯酯（DISISTITUTED PHOSPHYYLETHYL）-PHOSPHINE OXIDES
公开(公告)号：US3458581A
公开(公告)日：1969-07-29
申请号：US3458581D
申请日：1968-07-02
申请人： UNION CARBIDE CORP
发明人： WU CHISUNG
IPC分类号： C07F9/53 , C08K5/5397 , C11D1/79 , C07F9/28
CPC分类号： C07F9/5312 , C07F9/5329 , C08K5/5397 , C11D1/79

4. 发明申请

US20150099857A1 CATALYST FOR SYNTHESIZING POLYOLEFINS 有权
标题翻译：用于合成聚烯烃的催化剂
公开(公告)号：US20150099857A1
公开(公告)日：2015-04-09
申请号：US14400188
申请日：2013-04-30
申请人： THE UNIVERSITY OF TOKYO , SHOWA DENKO K.K.
发明人： Kyoko Nozaki , Brad Carrow , Yoshikuni Okumura , Junichi Kuroda
IPC分类号： C08F4/80
CPC分类号： C08F4/80 , C07F9/5312 , C07F9/5325 , C07F15/006 , C08F4/619 , C08F110/02 , C08F210/02 , C08F218/08 , C08F214/14 , C08F218/12 , C08F220/44 , C08F4/7014 , C08F2500/10 , C08F2500/03 , C08F220/14 , C08F216/18 , C08F2500/02 , C08F4/7019
摘要： The present invention relates to a method for producing a high-molecular-weight copolymer of polar group-containing allyl monomers comprising monomer units represented by formulae (3) and (4) (in the formulae, R1 represents a hydrogen atom (H) or hydrocarbon group having 1 to 6 carbon atoms; R2 represents —OH, —OCOR3 (R3 represents hydrocarbon group having 1 to 5 carbon atoms), —N(R4)2 (R4 represents a hydrogen atom or hydrocarbon group having 1 to 5 carbon atoms); and n and m are a value representing the molar ratio of each of the monomer units), which has few branches and unsaturated group at the molecular end, by copolymerizing olefin and an allyl compound using a metal complex of group 10 elements in the periodic system represented by formula (I) as a catalyst.The present invention enables providing a high-molecular-weight copolymer of polar group-containing allyl monomers, which copolymer has a novel structure, is available for various applications and has been considered to be difficult to synthesize by other polymerization methods such as radical polymerization; and a method for producing the same.
摘要翻译：本发明涉及含有由式（3）和（4）表示的单体单元的含极性基团的烯丙基单体的高分子量共聚物的制造方法（式中，R1表示氢原子（H）或具有1至6个碳原子的烃基; R 2表示-OH，-OCOR 3（R 3表示具有1至5个碳原子的烃基），-N（R 4）2（R 4表示氢原子或具有1至5个碳原子的烃基）; n和m是表示分子末端具有很少分支和不饱和基团的单体单元的摩尔比的值，通过使用第10族元素的金属络合物使烯烃和烯丙基化合物共聚，由式（I）表示的周期性体系作为催化剂。本发明能够提供含有极性基团的烯丙基单体的高分子量共聚物，该共聚物具有新颖的结构，可用于各种应用，并且被认为难以通过其它聚合方法如自由基聚合合成; 及其制造方法。

5. 发明授权

US4668809A Transition metal complex catalysts 失效
标题翻译：过渡金属络合催化剂
公开(公告)号：US4668809A
公开(公告)日：1987-05-26
申请号：US742127
申请日：1985-06-06
申请人： Alexis A. Oswald , Torris G. Jermasen , Andrew A. Westner , I-Der Huang
发明人： Alexis A. Oswald , Torris G. Jermasen , Andrew A. Westner , I-Der Huang
IPC分类号： C07C45/49 , C07C45/50 , C07F9/50 , C07F9/53 , C07F9/572 , C07F15/00
CPC分类号： C07F15/008 , C07C45/49 , C07C45/50 , C07F9/5004 , C07F9/5009 , C07F9/5022 , C07F9/5312 , C07F9/5721
摘要： Compositions of matter are disclosed which are highly useful in hydroformylation processes. The compositions are non-charged, non-chelated bis- and tris-(alkyl diaryl phosphine) rhodium carbonyl hydrides. The substituents of the alkyl group includes heteroorganic radicals containing ether, ester, keto and hydroxy oxygen, phosphine oxide and phosphorus ester phosphorus, amine, amide, amine oxide and heterocyclic nitrogen groups.These compositions are highly stable and selective catalysts for the hydroformylation of olefins under certain conditions. The disclosed catalyst systems contain a large excess of phosphine ligand and employ alpha-olefin plus synthesis gas reactant mixtures having a high H.sub.2 /CO ratio at relatively low pressures. They produce moslty aldehydes derived from terminal attack on the alpha-olefin reactant. In the case of low olefins, such as butene-1, the products can be advantageously removed in a continuous manner, as distillate components from a ligand reaction mixture kept at an elevated temperature and continuously fed by an appropriate mixture of the reactants.
摘要翻译：公开了在加氢甲酰化方法中非常有用的物质组合物。组合物是无电荷的，非螯合的双 - 和三 - （烷基二芳基膦）羰基氢化铑。烷基的取代基包括含有醚，酯，酮和羟基氧的杂有机基团，氧化膦和磷酯磷，胺，酰胺，氧化胺和杂环氮基团。这些组合物是在某些条件下用于烯烃加氢甲酰化的高度稳定和选择性的催化剂。所公开的催化剂体系含有大量过量的膦配体，并且在相对低的压力下使用具有高H 2 / CO比的α-烯烃加合成气反应物混合物。它们产生从α-烯烃反应物的末端攻击得到的清除醛。在低烯烃（例如丁烯-1）的情况下，可以有利地以连续的方式除去产物，因为来自配体反应混合物的馏出物组分保持在升高的温度，并通过反应物的适当混合物连续进料。

6. 发明授权

US3632634A Phosphorus compounds having the skeleton structure 失效
标题翻译：具有骨架结构的磷化合物
公开(公告)号：US3632634A
公开(公告)日：1972-01-04
申请号：US3632634D
申请日：1968-08-16
申请人： MAIER LUDWIG
发明人： MAIER LUDWIG
IPC分类号： C07F9/40 , C07F9/50 , C07F9/53 , C10L1/26 , C07F9/30
CPC分类号： C07F9/40 , C07F9/50 , C07F9/5312 , C10L1/2608
摘要： PHOSPHORUS COMPOUNDS HAVING THE SKELTON STRUCTURE

P-(C(-(C)N)-P)2 OR P-(C(-(C)N)-P)3

OF THE FORMULA

P-(C(-(C)N)-P)2 OR P-(C(-(C)N)-P)3

WHERE A AND B ARE 0 OR 1, AND PROCESS FOR MAKING BY REACTING A COMPOUND OF THE FORMULA

P(O)A(R1)B(CH(-R4)P(O)(R2)R3)(3-B)

WITH AN ORGANIC HALIDE OF THE FORMULA R4X. THE PRESENT COMPOUNDS ARE USEFUL AS COMPLECING AGENTS, SURFACTANTS. PLASTICIZERS, HYDRAULIC FLUIDS, CORROSION, INHIBITORS, STABILIZERS FOR PEROXIDES AND HYDROPEROXIDES, ADDITIVES TO ELECTROLYTIC BATHS, HEAT TRANSFER AGENTS, LUBRICANTS, OIL ADDITIVES, AND GASOLINE ADDITIVES TO DETERGENTS.

7. 发明授权

US09303101B2 Catalyst for synthesizing polyolefins 有权
标题翻译：聚烯烃合成催化剂
公开(公告)号：US09303101B2
公开(公告)日：2016-04-05
申请号：US14400188
申请日：2013-04-30
申请人： THE UNIVERSITY OF TOKYO , SHOWA DENKO K.K.
发明人： Kyoko Nozaki , Brad Carrow , Yoshikuni Okumura , Junichi Kuroda
IPC分类号： C08F4/80 , C07F9/53 , C07F15/00 , C08F110/02 , C08F4/619
CPC分类号： C08F4/80 , C07F9/5312 , C07F9/5325 , C07F15/006 , C08F4/619 , C08F110/02 , C08F210/02 , C08F218/08 , C08F214/14 , C08F218/12 , C08F220/44 , C08F4/7014 , C08F2500/10 , C08F2500/03 , C08F220/14 , C08F216/18 , C08F2500/02 , C08F4/7019
摘要： The present invention relates to a method for producing a high-molecular-weight copolymer of polar group-containing allyl monomers comprising monomer units represented by formulae (3) and (4) (in the formulae, R1 represents a hydrogen atom (H) or hydrocarbon group having 1 to 6 carbon atoms; R2 represents —OH, —OCOR3 (R3 represents hydrocarbon group having 1 to 5 carbon atoms), —N(R4)2 (R4 represents a hydrogen atom or hydrocarbon group having 1 to 5 carbon atoms); and n and m are a value representing the molar ratio of each of the monomer units), which has few branches and unsaturated group at the molecular end, by copolymerizing olefin and an allyl compound using a metal complex of group 10 elements in the periodic system represented by formula (I) as a catalyst.The present invention enables providing a high-molecular-weight copolymer of polar group-containing allyl monomers, which copolymer has a novel structure, is available for various applications and has been considered to be difficult to synthesize by other polymerization methods such as radical polymerization; and a method for producing the same.
摘要翻译：本发明涉及含有由式（3）和（4）表示的单体单元的含极性基团的烯丙基单体的高分子量共聚物的制造方法（式中，R1表示氢原子（H）或具有1至6个碳原子的烃基; R 2表示-OH，-OCOR 3（R 3表示具有1至5个碳原子的烃基），-N（R 4）2（R 4表示氢原子或具有1至5个碳原子的烃基）; n和m是表示分子末端具有很少分支和不饱和基团的单体单元的摩尔比的值，通过使用第10族元素的金属络合物使烯烃和烯丙基化合物共聚，由式（I）表示的周期性体系作为催化剂。本发明能够提供含有极性基团的烯丙基单体的高分子量共聚物，该共聚物具有新颖的结构，可用于各种应用，并且被认为难以通过其它聚合方法如自由基聚合合成; 及其制造方法。

8. 发明授权

US3849523A Phosphorus compounds containing the atom skeleton p-(c-p)2 or p-(c-p)3 失效
标题翻译：含有ATOM SKELETON P-（C-P）2或P-（C-P）3的磷化合物
公开(公告)号：US3849523A
公开(公告)日：1974-11-19
申请号：US69041867
申请日：1967-12-14
申请人： MONSANTO CO
发明人： MAIER L
IPC分类号： C07C407/00 , C07F7/28 , C07F9/30 , C07F9/32 , C07F9/38 , C07F9/40 , C07F9/53 , C09K15/32 , C11D1/34 , C11D3/39 , C11D3/395
CPC分类号： C07C71/00 , C07F7/28 , C07F9/30 , C07F9/305 , C07F9/32 , C07F9/3235 , C07F9/3821 , C07F9/40 , C07F9/4012 , C07F9/5312 , C07F9/5329 , C09K15/322 , C11D1/34 , C11D3/39 , C11D3/394 , C11D3/3951
摘要： 1. A COMPOSITION OF MATTER HAVING THE FORMULA:

((RO)2P(:O)CH2)XP(:O)(OR'')3-X

WHEREIN X IS 2 AND R AND R'' ARE INDEPENDENTLY SELECTED FROM THE GROUP CONSISTING OF H AND ALKYL OF 1 TO 12 CARBONS.

9. 发明授权

US3420917A Tris(disubstituted phosphenyl ethyl) phosphine oxides 失效
标题翻译： TRIS（分散的磷酸乙酯）磷酸盐氧化物
公开(公告)号：US3420917A
公开(公告)日：1969-01-07
申请号：US3420917D
申请日：1965-12-02
申请人： UNION CARBIDE CORP
发明人： WU CHISUNG
IPC分类号： C07F9/53 , C08K5/5397 , C11D1/79 , C07F9/02
CPC分类号： C07F9/5312 , C07F9/5329 , C08K5/5397 , C11D1/79

10. 发明授权

US4687866A Ligand exchange process for producing alkyl diaryl phosphine rhodium carbonyl hydrides 失效
标题翻译：用于制备烷基二芳基膦铑羰基氢化物的配体交换方法
公开(公告)号：US4687866A
公开(公告)日：1987-08-18
申请号：US749807
申请日：1985-06-28
申请人： Alexis A. Oswald , Torris G. Jermasen , Andrew A. Westner , I-Der Huang
发明人： Alexis A. Oswald , Torris G. Jermasen , Andrew A. Westner , I-Der Huang
IPC分类号： C07C45/49 , C07C45/50 , C07C45/62 , C07C45/73 , C07C45/74 , C07F9/50 , C07F9/53 , C07F9/572 , C07F15/00
CPC分类号： C07F15/008 , C07C45/49 , C07C45/50 , C07C45/62 , C07C45/73 , C07C45/74 , C07F9/5004 , C07F9/5009 , C07F9/5022 , C07F9/5312 , C07F9/5721
摘要： Compositions of matter are disclosed which are highly useful in hydroformylation processes. The compositions are non-charged, non-chelated bis- and tris-(alkyl diaryl phosphine) rhodium carbonyl hydrides. The substituents of the alkyl group include heteroorganic radicals containing silane, silicone, ether, ester, keto and hydroxy oxygen, phosphine oxide and phosphorus ester phosphorus, amine, amide, amine oxide and heterocyclic nitrogen groups.These compositions are highly stable and selective catalysts for the hydroformylation of olefins under certain conditions. The disclosed catalyst systems contain a large excess of phosphine ligand and employ alpha-olefin plus synthesis gas reactant mixtures having a high H.sub.2 /CO ratio at relatively low pressures. They produce mostly aldehydes derived from terminal attack on the alpha-olefin reactant. In the case of low olefins, such as butene-1, the products can be advantageously removed in a continuous manner, as distillate components from a ligand reaction mixture kept at an elevated temperature and continuously fed by an appropriate mixture of the reactants.
摘要翻译：公开了在加氢甲酰化方法中非常有用的物质组合物。组合物是无电荷的，非螯合的双 - 和三 - （烷基二芳基膦）羰基氢化铑。烷基的取代基包括含有硅烷，硅氧烷，醚，酯，酮和羟基氧的杂有机基团，氧化膦和磷酯磷，胺，酰胺，氧化胺和杂环氮基团。这些组合物是在某些条件下用于烯烃加氢甲酰化的高度稳定和选择性的催化剂。所公开的催化剂体系含有大量过量的膦配体，并且在相对低的压力下使用具有高H 2 / CO比的α-烯烃加合成气反应物混合物。它们主要产生源自α-烯烃反应物的末端攻击的醛。在低烯烃（例如丁烯-1）的情况下，可以有利地以连续的方式除去产物，因为来自配体反应混合物的馏出物组分保持在升高的温度，并通过反应物的适当混合物连续进料。

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