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1. 发明授权

US3923874A Continuous production of esters of glycols or their monoethers with lower fatty acids 失效
标题翻译：连续生产二醇或其单醚与低级脂肪酸的酯
公开(公告)号：US3923874A
公开(公告)日：1975-12-02
申请号：US36732773
申请日：1973-06-06
申请人： BASF AG
发明人： HOHENSCHUTZ HEINZ , HORNBERGER PAUL , GNAD JOSEF , DINKHAUSER GUENTER
IPC分类号： C07C69/02 , B01J27/00 , B01J31/00 , C07B61/00 , C07C67/08
CPC分类号： C07C67/08 , C07C69/08
摘要： Continuous production of substantially or wholly water-soluble esters of glycols or their monoethers with lower fatty acids by reaction of a glycol of the formula (I): HO-A-X (I) in which A is ethylene, propylene or butylene; and X is OH or OR in which R is alkyl of one to four carbon atoms or OAOH or OAOR in which A and R have the meanings given above with a lower saturated fatty acid at elevated temperature in the presence of a catalytic amount of a strong acid while continuously removing the water formed by means of an entrainer followed by treatment with an aqueous alkali. The glycol of the formula (I) is reacted in a first zone with the lower fatty acid, the water formed being distilled off as an azeotrope over the top by means of an entrainer, and the crude glycol ester including the entrainer is removed from the bottoms, mixes with an aqueous alkali, extracted in a second zone while supplying an extractant and water with phase separation and in a third zone the pure glycol ester is recovered from the resulting mixture of glycol ester, entrainer and extractant by rectification. Glycol esters are used as solvents for surface coating agents.
摘要翻译：通过式（I）的二元醇：其中A是乙烯，丙烯或丁烯的HO-A-X（I）的反应连续生产二醇或其单醚与低级脂肪酸的基本上或完全水溶性的酯; 并且X是OH或OR，其中R是1-4个碳原子的烷基或OAOH或OAOR，其中A和R在较高饱和脂肪酸中具有上述含义，在催化剂量的强度存在下，同时连续除去通过夹带剂形成的水，然后用碱水溶液处理。式（I）的二醇在第一区域与低级脂肪酸反应，形成的水通过夹带剂在顶部作为共沸物蒸馏出来，并将包含夹带剂的粗乙醇酯从底部，与碱水溶液混合，在第二区域中提取，同时提供萃取剂和进行相分离的水，在第三区域，通过精馏从所得到的乙二醇酯，夹带剂和萃取剂的混合物中回收纯乙二醇酯。乙二醇酯用作表面涂层剂的溶剂。

2. 发明授权

US3778468A Process for preparing ethylene glycol esters 失效
标题翻译：制备乙烯甘油酯的方法
公开(公告)号：US3778468A
公开(公告)日：1973-12-11
申请号：US3778468D
申请日：1972-06-27
申请人： HALCON INTERNATIONAL INC
发明人： KOLLAR J
IPC分类号： B01J27/08 , C08K5/103 , C07C67/04
CPC分类号： B01J27/08 , C07C67/05 , C08K5/103 , C07C69/16 , C07C69/003 , C07C69/28 , C07C69/08
摘要： ETHYLENE GLYCOL ESTERS ARE PREPARED BY THE MOLECULAR OXYGEN OXIDATION OF ETHYLENE IN THE PRESENCE OF A LIQUID PHASE REACTION MEDIUM CONTAINING A CARBOXYLIC ACID, WITH THE REACTION BEING CATALYZED BY CATIONIC SELENIUM AND AT LEAST ONE MEMBER OF THE GROUP CONSISTING OF ELEMENTAL BROMINE, ELEMENTAL CHLORINE, A BROMINE-CONTAINING COMPOUND AND A CHLORINE-CONTAINING COMPOUND.

3. 发明授权

US3383374A Ethylenically unsaturated 1-acyloxyaliphatic ethers and polymers thereof 失效
标题翻译：烯键式不饱和1-酰氧脂族醚及其聚合物
公开(公告)号：US3383374A
公开(公告)日：1968-05-14
申请号：US41825264
申请日：1964-12-14
申请人： UNION CARBIDE CORP
发明人： MCTEER LUCIAN W
IPC分类号： C08F16/18
CPC分类号： C08F16/18 , C07C67/00 , C07C67/04 , C07C67/10 , C07C67/287 , C07C67/297 , C07C69/16 , C07C69/28 , C07C69/56 , C07C69/708 , C07C69/24 , C07C69/08 , C07C69/533 , C07C69/587 , C07C69/78 , C07C69/145 , C07C69/63 , C07C69/14 , C07C69/54

4. 发明授权

US3335174A Preparation of diols and aliphatic carboxylic acid esters thereof from olefins 失效
标题翻译：由烯烃制备二醇及其脂族羧酸酯
公开(公告)号：US3335174A
公开(公告)日：1967-08-08
申请号：US35590964
申请日：1964-03-30
申请人： MARATHON OIL CO
发明人： NORTON CHARLES J
IPC分类号： C07C33/035
CPC分类号： C07C33/035 , C07C67/05 , C07C67/055 , C07C2601/14 , C07C69/16 , C07C69/28 , C07C69/08

5. 发明授权

US2636046A Preparation of polyfunctional compounds 失效
标题翻译：多官能化合物的制备
公开(公告)号：US2636046A
公开(公告)日：1953-04-21
申请号：US5501648
申请日：1948-10-16
申请人： DU PONT
发明人： GRESHAM WILLIAM F
IPC分类号： C07C29/151 , C07C29/156 , C07C29/157
CPC分类号： C07C29/1514 , C07C29/1512 , C07C29/156 , C07C67/36 , C12C11/02 , C07C31/202 , C07C69/08 , C07C69/18 , C07C69/16

6. 发明申请

US20050143599A1 Process for preparing monoesters 审中-公开
标题翻译：制备单酯的方法
公开(公告)号：US20050143599A1
公开(公告)日：2005-06-30
申请号：US10748939
申请日：2003-12-30
申请人： Markus Wicki , Kent Nielsen
发明人： Markus Wicki , Kent Nielsen
IPC分类号： C07C67/00 , C07C67/08 , C07C67/58 , C07C67/14
CPC分类号： C07C67/58 , C07C67/08 , C07C2601/14 , C07C69/08 , C07C69/16 , C07C69/26
摘要： A process for preparing monoesters comprises the step of reacting at least one diol with at least one carboxylic acid in a biphasic solvent system, the carboxylic acid being sufficiently water soluble to allow esterification to occur, and the biphasic solvent system comprising water and at least one aprotic solvent in which the resulting monoester has greater solubility than in water.
摘要翻译：制备单酯的方法包括在双相溶剂体系中使至少一种二醇与至少一种羧酸反应的步骤，所述羧酸具有足够的水溶性以允许发生酯化，并且所述双相溶剂体系包含水和至少一种非质子溶剂，其中所得单酯具有比在水中更大的溶解度。

7. 发明申请

US20050113604A1 Aldehyde conversion method using a molecular sieve and the use of the molecular sieve as a catalyst in said method 失效
标题翻译：使用分子筛的醛转化方法和在所述方法中使用分子筛作为催化剂
公开(公告)号：US20050113604A1
公开(公告)日：2005-05-26
申请号：US10932564
申请日：2004-09-02
申请人： Avelino Canos , Maria Grau , Sara Chornet , Michael Renz
发明人： Avelino Canos , Maria Grau , Sara Chornet , Michael Renz
IPC分类号： B01J29/03 , B01J29/035 , B01J29/04 , B01J29/70 , C01B37/00 , C01B39/08 , C07C51/235 , C07C51/285 , C07C67/39 , C07C51/16 , C07C45/61
CPC分类号： C07C51/285 , B01J29/0308 , B01J29/035 , B01J29/04 , B01J29/7057 , C01B37/005 , C01B39/085 , C07C51/235 , C07C67/39 , C07C63/04 , C07C65/21 , C07C69/017 , C07C69/08 , C07C69/10
摘要： The inversion relates to an aldehyde conversion method comprising putting an aldehyde into contact with oxygenated water and with a catalyst, under oxidation conditions, wherein the catalyst is a molecular sieve with pores of a diameter of at least 0.52 nm and has an empirical formula in a calcined and dehydrated form of (SnxTiySi1−x−y−zGez) O2wherein x is a molar fraction of the tin and has a value between 0.001 and 0.1; y is a molar fraction of titanium and has a value from zero to 0.1; and z is the molar fraction molar of the germanium and has a value from zero to 0.08.
摘要翻译：反转涉及醛转化方法，其包括在氧化条件下将醛与含氧水和催化剂接触，其中催化剂是直径为至少0.52nm的孔的分子筛，并且具有经验式煅烧和脱水形式的<？in-line-formula description =“In-line Formulas”end =“lead”？（Sn x x Ti x Si x Si α-in-line-formula description =“In-line Formulas”end =“tail”？>其中x（x，y）是锡的摩尔分数，其值在0.001和0.1之间; y是钛的摩尔分数，其值为0至0.1; z是锗的摩尔分数摩尔，其值为零至0.08。

8. 发明授权

US4362636A Crankcase lubricant and method for improving fuel economy of internal combustion engines utilizing same 失效
标题翻译：曲轴箱润滑剂和利用其的内燃机的燃料经济性的提高方法
公开(公告)号：US4362636A
公开(公告)日：1982-12-07
申请号：US215954
申请日：1980-12-12
申请人： Vernon R. Small, Jr.
发明人： Vernon R. Small, Jr.
IPC分类号： C10M129/76 , C07C69/08 , C10N30/00 , C10N30/06 , C10N40/25 , C10M1/26
CPC分类号： C07C69/08 , C10M2207/289 , C10M2209/084 , C10M2215/086 , C10M2215/28 , C10M2219/02 , C10M2219/046 , C10M2223/045 , C10N2210/02 , C10N2270/02
摘要： Lubricating oils containing oil soluble hydroxyalkyl alkanoates have been found to reduce fuel consumption in an internal combustion engine.
摘要翻译：已经发现含有油溶性羟烷基链烷酸酯的润滑油降低了内燃机的燃料消耗。

9. 发明授权

US3671577A Process for producing 1, 4-diacyloxy-2-butene 失效
标题翻译：生产1,4-二氨基-2-丁烯的方法
公开(公告)号：US3671577A
公开(公告)日：1972-06-20
申请号：US3671577D
申请日：1970-03-13
申请人： TOYO SODA MFG CO LTD
发明人： ONO ISAO , FUKABORI KENTARO , SHIMOMURA SEIICHI
IPC分类号： C07C69/025 , B01J23/00 , B01J27/00 , B01J31/00 , C07B61/00 , C07C69/16 , C07C69/527 , C07C67/04
CPC分类号： C07C67/055 , C07C69/16 , C07C69/28 , C07C69/593 , C07C69/08
摘要： 1,4-DIACYLOXY-2-BUTENE IS PRODUCED BY PASSING A GASEOUS MIXTURE OF BUTADIENE, AN ALIPHATIC MONOCARBOXYLIC ACID AND AN OXYGENCONTAINING GAS OVER A CATALYST COMPRISING AT LEAST ONE OF PALLADIUM, IRIDIUM, PLATINUM, RHODIUM AND RUTHENIUM AND CARBOXYLATE AND INORGANIC ACID SALT THEREOF.
摘要翻译： 1,4-二氧化二-2-丁烯是通过引入丁二烯的气体混合物，二氧化硅单羧酸和含氧气体，通过包含至少一种钯，铱，铂，铑和钌以及羧酸和无机物的催化剂生产的其酸盐。

10. 发明授权

US2405936A Formic acid esters 失效
标题翻译：甲酸酯
公开(公告)号：US2405936A
公开(公告)日：1946-08-20
申请号：US51363943
申请日：1943-12-09
申请人： DU PONT
发明人： BARTLETT EDWARD P
IPC分类号： C07C69/08
CPC分类号： C07C69/08

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