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1. 发明授权

US09944584B2 Method for removing mineral acid from levulinic acid 有权
公开(公告)号：US09944584B2
公开(公告)日：2018-04-17
申请号：US15123520
申请日：2015-03-02
申请人： GFBiochemicals Limited
发明人： Brian D. Mullen , Vivek Badarinarayana
IPC分类号： C07C59/00 , C07C51/48 , B01D11/04
CPC分类号： C07C51/48 , B01D11/0426 , B01D11/0492 , C07C59/185
摘要： The invention describes processes to selectively remove or reduce the mineral acid content substantially from compositions comprising a solvent and levulinic acid, wherein the levulinic acid was derived from the reaction between various biomass materials and a mineral acid or an organic acid catalyst.

2. 发明授权

US09796666B2 Aminoacid lipids 有权
公开(公告)号：US09796666B2
公开(公告)日：2017-10-24
申请号：US14385178
申请日：2013-03-11
申请人： Merck Patent GmbH
发明人： Michael Wilhelm Platscher , Raymond Behrendt , Viola Groehn , Simone Rachel Hoertner , Marco Silvio Passafaro , Finn Bauer
IPC分类号： C07C237/30 , C07C271/22 , C07C237/08 , C07C237/10 , A61K9/127 , C07C59/185 , C07C237/06 , C07C237/22
CPC分类号： C07C237/30 , A61K9/1272 , C07C59/185 , C07C237/06 , C07C237/08 , C07C237/10 , C07C237/22 , C07C271/22 , C07C2603/18 , Y02P20/55
摘要： The present invention is directed to a new class of lipids, more specifically ether-lipids having a polar headgroup, as well as vesicles comprising these lipids, methods of their preparation as well as their uses in medical applications, wherein the ether-lipids are represented by general formula I

3. 发明授权

US09598341B2 Process to prepare levulinic acid 有权
公开(公告)号：US09598341B2
公开(公告)日：2017-03-21
申请号：US14748278
申请日：2015-06-24
申请人： GFBiochemicals Limited
发明人： Brian D. Mullen , Dorie Janine Yontz , Cora M. Leibig
IPC分类号： C07C59/00 , C07C51/00
CPC分类号： C07C51/47 , C07C51/00 , C07C59/185
摘要： The invention describes processes to prepare levulinic acid, formic acid and/or hydroxymethyl furfural from various biomass materials.

4. 发明授权

US09403734B2 Method for producing organic acids and organic acid degradation compounds from biomass 有权
标题翻译：从生物质生产有机酸和有机酸降解化合物的方法
公开(公告)号：US09403734B2
公开(公告)日：2016-08-02
申请号：US14487208
申请日：2014-09-16
申请人： Georgia-Pacific LLC
发明人： John Patrick Kelly , Michael Eugene Carroll , Paul Topping
IPC分类号： C07B41/08
CPC分类号： C07B41/08 , C07C51/00 , C07C59/185
摘要： A method and integrated reactor system are provided for producing one or more organic acids, organic acid degradation compounds, and combinations thereof, from various types of biomass, including sludge from a pulp and paper mill.
摘要翻译：提供了一种方法和综合反应器系统，用于从各种类型的生物质（包括来自纸浆和造纸厂的污泥）中生产一种或多种有机酸，有机酸降解化合物及其组合。

5. 发明申请

US20160017540A1 PRETREATMENT AND FRACTIONATION OF LIGNOCELLULOSIC BIOMASS 审中-公开
标题翻译：细菌生物量的预处理和分离
公开(公告)号：US20160017540A1
公开(公告)日：2016-01-21
申请号：US14777326
申请日：2014-03-14
申请人： SUGANIT SYSTEMS, INC.
发明人： Praveen PARIPATI , Anantharam Prasad DADI
IPC分类号： D21C3/02 , C07D307/12 , D21C9/02 , C07C59/185 , D21C3/20 , C12P19/02 , C13K1/02
CPC分类号： D21C3/02 , C07C59/185 , C07D307/12 , C07G1/00 , C08H8/00 , C12P19/02 , C12P19/14 , C12P2201/00 , C12P2203/00 , C13K1/02 , D21C1/00 , D21C1/06 , D21C3/20 , D21C9/02 , Y02E50/343
摘要： Method and apparatus for enhanced production of sugars and lignin via fractionation of lignocellulosic biomass through ionic liquid pretreatment and mild alkaline treatment. The resulting biomass is easily fractionated and amenable to efficient and rapid enzymatic hydrolysis or acid hydrolysis and catalytic conversion to valuable products with high recovery of the enzymes used in the hydrolysis.
摘要翻译：通过离子液体预处理和轻度碱性处理分解木质纤维素生物质来增加糖和木质素生产的方法和装置。所得生物质容易分级，并且适于有效和快速的酶水解或酸水解和催化转化成具有高水解回收率的有价值产物。

6. 发明授权

US09221741B2 Ketocarboxylic acids, ketocarboxylic esters, methods of manufacture and uses thereof 有权
标题翻译：酮羧酸，酮羧酸酯，其制备方法和用途
公开(公告)号：US09221741B2
公开(公告)日：2015-12-29
申请号：US13934368
申请日：2013-07-03
申请人： SEGETIS, Inc.
发明人： Brian D. Mullen , Leo E. Manzer , Cora M. Leibig
IPC分类号： C07C69/66 , C07C69/738 , C07C51/09 , C07C51/493 , C07C67/08 , C07C67/52 , C07C69/716
CPC分类号： C07C69/738 , C07C51/09 , C07C51/493 , C07C67/08 , C07C67/52 , C07C69/716 , Y02P20/582 , C07C59/185
摘要： Ketocarboxylic acids such as levulinic acid can be efficiently purified in high yield by esterification with a hydrocarbon polyol to the corresponding polyketocarboxylic ester, which can be readily purified, for example recrystallized. After purification, the ketocarboxylic ester can be hydrolyzed to provide pure ketocarboxylic acid, or a salt thereof, after removal of the esterifying hydrocarbon polyol, or used for other synthetic transformations. Advantageously, the polyketocarboxylic esters, ketocarboxylic acids, and salts thereof produced by this method are obtained in high purity.
摘要翻译：酮羧酸如乙酰丙酸可以通过用烃多元醇与相应的聚酮羧酸酯酯化而以高收率有效地纯化，其可以容易地纯化，例如重结晶。纯化后，在除去酯化烃多元醇之后，可以将酮羧酸酯水解以提供纯酮羧酸或其盐，或用于其它合成转化。有利地，以高纯度获得通过该方法制备的多酮羧酸酯，酮羧酸及其盐。

7. 发明申请

US20150299087A1 PROCESS FOR THE ISOLATION OF LEVULINIC ACID AND FORMIC ACID 有权
标题翻译：分离酸性和酸性的方法
公开(公告)号：US20150299087A1
公开(公告)日：2015-10-22
申请号：US14648437
申请日：2013-12-09
申请人： DSM IP ASSETS B.V.
发明人： Rudy Francois Maria Jozef PARTON
IPC分类号： C07C51/47 , C07C59/185 , B01D3/40 , C07C51/48
CPC分类号： C07C51/47 , B01D3/40 , C07C51/42 , C07C51/44 , C07C51/48 , C07C59/185 , C07C53/02
摘要： The invention provides a process for the isolation of levulinic acid and formic acid from a composition comprising formic acid and levulinic acid, said process comprising a solid-liquid separation step, a vapor removal step, and a solvent-solvent extraction step, wherein a vapor condensate vapor and/or an aqueous phase from the solvent extraction is used to wash the solid fraction. Washing with vapor condensate results in higher levulinic acid yields (higher levulinic acid recovery) as compared to washing with normal water. Washing with aqueous phase results in a less compressible filter cake. Washing first with aqueous phase and subsequently with condensate results in even higher levulinic acid yields. The process is suitable for isolating levulinic acid and formic acid from compositions made by acid hydrolysis of a lignocellulosic biomass, and also from compositions made by acid hydrolysis of sugars such as glucose and fructose.
摘要翻译：本发明提供从包含甲酸和乙酰丙酸的组合物中分离乙酰丙酸和甲酸的方法，所述方法包括固液分离步骤，蒸气去除步骤和溶剂 - 溶剂萃取步骤，其中蒸气冷凝物蒸气和/或来自溶剂萃取的水相用于洗涤固体部分。与正常水洗涤相比，用蒸气冷凝物洗涤导致更高的乙酰丙酸产量（更高的乙酰丙酸回收率）。用水相洗涤导致较不压缩的滤饼。首先用水相洗涤，随后用冷凝液洗脱得到甚至更高的乙酰丙酸产率。该方法适合于通过木质纤维素生物质的酸水解制备的组合物以及由糖如葡萄糖和果糖的酸水解制备的组合物分离乙酰丙酸和甲酸。

8. 发明申请

US20150246865A1 PROCESS FOR MAKING LEVULINIC ACID 审中-公开
标题翻译：制备维生素A的方法
公开(公告)号：US20150246865A1
公开(公告)日：2015-09-03
申请号：US14705116
申请日：2015-05-06
申请人： ARCHER DANIELS MIDLAND COMPANY
发明人： Alexandra Sanborn , Thomas Binder
IPC分类号： C07C51/31
CPC分类号： C07C51/31 , C07C51/00 , C07C59/185
摘要： A process is described wherein a feed of a six-carbon carbohydrate-containing material or of a furanic dehydration product from a six-carbon carbohydrate-containing material or of a combination of these is supplied to a reactor in a controlled manner over time, and the feed is acid-hydrolyzed to produce levulinic acid. In certain embodiments, derivatives of the levulinic acid are prepared.
摘要翻译：描述了一种方法，其中将含六碳碳水化合物的材料或来自含六碳碳水化合物的材料的呋喃脱水产物或它们的组合的进料以受控的方式随时间供应到反应器，进料被酸水解产生乙酰丙酸。在某些实施方案中，制备乙酰丙酸的衍生物。

9. 发明申请

US20150030670A1 AMINOACID LIPIDS 有权
标题翻译：氨基酸脂肪酸
公开(公告)号：US20150030670A1
公开(公告)日：2015-01-29
申请号：US14385178
申请日：2013-03-11
申请人： MerckPatent GmbH
发明人： Michael Wilhelm Platscher , Raymond Behrendt , Viola Groehn , Simone Rachel Hoertner , Marco Silvio Passafaro , Finn Bauer
IPC分类号： C07C237/30 , C07C59/185 , C07C237/22 , C07C237/06
CPC分类号： C07C237/30 , A61K9/1272 , C07C59/185 , C07C237/06 , C07C237/08 , C07C237/10 , C07C237/22 , C07C271/22 , C07C2603/18 , Y02P20/55
摘要： The present invention is directed to a new class of lipids, more specifically ether-lipids having a polar headgroup, as well as vesicles comprising these lipids, methods of their preparation as well as their uses in medical applications, wherein the ether-lipids are represented by general formula I
摘要翻译：本发明涉及一类新的脂质，更具体地是具有极性头团的醚 - 脂质，以及包含这些脂质的囊泡，其制备方法及其在医学应用中的用途，其中所述醚 - 脂质被代表通过通式I

10. 发明申请

US20140360866A1 Production of Fuel from Chemicals Derived from Biomass 有权
公开(公告)号：US20140360866A1
公开(公告)日：2014-12-11
申请号：US14469878
申请日：2014-08-27
申请人： Ceramatec, Inc.
发明人： Sai Bhavaraju , Mukund Karanjikar
IPC分类号： C25B9/08 , C25B3/00
CPC分类号： C25B9/08 , C07C51/00 , C07C51/09 , C07C51/41 , C07C51/412 , C10L1/02 , C25B3/00 , C25B3/02 , Y02E50/13 , Y02P30/20 , C07C59/185 , C07C53/126 , C07C59/125
摘要： Hydrocarbons may be formed from six carbon sugars. This process involves obtaining a quantity of a hexose sugar. The hexose sugar may be derived from biomass. The hexose sugar is reacted to form an alkali metal levulinate, an alkali metal valerate, an alkali metal 5-hydroxy pentanoate, or an alkali metal 5-alkoxy pentanoate. An anolyte is then prepared for use in a electrolytic cell. The anolyte contains the alkali metal levulinate, the alkali metal valerate, the alkali metal 5-hydroxy pentanoate, or the alkali metal 5-alkoxy pentanoate. The anolyte is then decarboxylated. This decarboxylating operates to decarboxylate the alkali metal levulinate, the alkali metal valerate, the alkali metal 5-hydroxy pentanoate, or the alkali metal 5-alkoxy pentanoate to form radicals, wherein the radicals react to form a hydrocarbon fuel compound.

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