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1. 发明申请

US20150057151A1 MESOPOROUS TITANIUM DIOXIDE NANOPARTICLES AND PROCESS FOR THEIR PRODUCTION 有权
标题翻译：多孔二氧化钛纳米颗粒及其生产工艺
公开(公告)号：US20150057151A1
公开(公告)日：2015-02-26
申请号：US14528259
申请日：2014-10-30
申请人： Cristal USA Inc.
发明人： Guoyi Fu , Mark Watson
IPC分类号： C01G23/053
CPC分类号： C01G23/0538 , B82Y30/00 , B82Y40/00 , C01G23/0536 , C01P2004/03 , C01P2004/32 , C01P2004/64 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/17 , Y10T428/2982
摘要： TiO2 nanoparticles having improved consistent particle morphology, uniform particle size, and which contain uniform intra-particle pores in the mesopore size range are produced by wet chemical hydrolysis.
摘要翻译：通过湿化学水解制备具有改善的一致颗粒形态，均匀粒度并且在中孔尺寸范围内含有均匀的颗粒内孔的TiO 2纳米颗粒。

2. 发明申请

US20070173405A1 Titanium oxide product method for making the same and its use as a photocatalyst 有权
标题翻译：制备相同的氧化钛产品方法及其作为光催化剂的用途
公开(公告)号：US20070173405A1
公开(公告)日：2007-07-26
申请号：US10588216
申请日：2005-02-04
申请人： Saila Karvinen , Ralf-Johan Lamminmaki
发明人： Saila Karvinen , Ralf-Johan Lamminmaki
IPC分类号： B01J23/00
CPC分类号： C01G23/0538 , B01D9/0031 , B01D9/0036 , B01D2255/20707 , B01D2255/802 , B01J35/004 , B01J37/031 , B82Y30/00 , C01P2004/64 , C01P2006/12
摘要： The invention relates to a process for manufacturing a particulate titanium dioxide product, wherein hydrated titanium dioxide is precipitated from an aqueous solution of titanium oxychlioride by adding to the solution titanium dioxide particles as crystal nuclei and the product obtained from the precipitation step is isolated and optionally calcined. The process is characterized by the addition of crystal nuclei to an aqueous solution of titanium oxychloride having a content of >90 g TiO2/l calculated as TiO2 and the performance of precipitation at a temperature below the boiling point of the said aqueous solution and at normal pressure. In addition, the invention relates to a titanium dioxide product prepared by using the process, the use of the product as a photocatalyst, and a photocatalyst, which comprises a titanium dioxide product prepared according to the invention.
摘要翻译：本发明涉及一种制造颗粒状二氧化钛产品的方法，其中通过向该溶液中加入二氧化钛颗粒作为结晶核，其中水合二氧化钛从二氧化钛钛水溶液中沉淀出来，从析出步骤获得的产物被分离并任选地煅烧。该方法的特征在于将晶体核添加到以TiO 2计算的含量> 90g TiO 2 / l的氯氧化钛水溶液中，在低于所述水溶液的沸点的温度下在常压下沉淀。此外，本发明涉及通过使用该方法制备的二氧化钛产品，使用该产物作为光催化剂，以及包含根据本发明制备的二氧化钛产品的光催化剂。

3. 发明授权

US3923968A Method of preparing titanium dioxide pigment 失效
标题翻译：二氧化钛颜料的制备方法
公开(公告)号：US3923968A
公开(公告)日：1975-12-02
申请号：US33697873
申请日：1973-03-01
申请人： DOW CHEMICAL CO
发明人： BASQUE MAX G , MAGNER JAMES E , SURLS JOSEPH P , WEST BEN F
IPC分类号： C01G23/053 , C01G23/04
CPC分类号： B82Y30/00 , C01G23/0538 , C01P2004/54 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2006/60
摘要： Elongate monocrystalline rutile nucleus crystals are mixed with an acidic titanium chloride solution which contains from 0.1 to 60 grams of dissolved titanium per liter, from 0.004 to 9 gram ions of chloride per liter and little or no phosphate, sulphate or bisulphate. The mixture is heated at a temperature of from 80* to 150*C., thereby producing composite titanium dioxide pigment particles consisting each of one or more nucleus crystals surrounded by elongate rutile crystallites in generally parallel array together with interstitial non-rutile titanium dioxide. The pigment particles have aspect ratios of from 3 to 150, effective diameters of from 0.05 to 0.3 microns and contain not more than about 10 weight percent of the non-rutile titanium dioxide.
摘要翻译：细长的单晶金红石核晶体与酸性氯化钛溶液混合，每升含0.1至60克溶解钛，每公升0.004至9克氯离子，少量或不含磷酸盐，硫酸盐或硫酸氢盐。将混合物在80℃至150℃的温度下加热，从而产生复合二氧化钛颜料颗粒，每个复合二氧化钛颜料颗粒由细长金红石晶体包围的一个或多个核晶体组成，大致平行排列与间隙非金红石二氧化钛。颜料颗粒的纵横比为3至150，有效直径为0.05至0.3微米，并且含有不超过约10重量％的非金红石二氧化钛。

4. 发明授权

US3549322A Process for the manufacture of acicular rutile pigments from hydrochloric acid titanium chloride solutions 失效
标题翻译：氯化氢氯化钛溶液制备活性染料的方法
公开(公告)号：US3549322A
公开(公告)日：1970-12-22
申请号：US3549322D
申请日：1969-02-03
申请人： TITAN GMBH
发明人： KLEIN EDGAR , KULLING ACHIM , STEINHAUSEN HELMUT
IPC分类号： C01G23/00 , C01G23/053 , C09C1/00 , C09C1/36 , C01G23/06 , C01G23/08
CPC分类号： C09C1/3692 , C01G23/0538 , C01P2004/10 , C01P2004/54 , C01P2006/60 , C09C1/3607 , C09C3/043 , C09C3/06
摘要： 1,254,729. Titanium dioxide. TITANG.m.b.H. 10 Feb:, 1969 [17 Feb., 1968], No. 7177/69. Heading C1N. 'Needle-shaped TiO 2 particles, or star-shaped agglomerates thereof, are made by (1) heating to 80-100‹ C. an HCl solution of titanium chloride (130-250. g. TiO 2 /l.) in which the molar ratio HCl not bonded to Fe : TiO 2 is 2-5 :1; (2) mixing this solution with a seed solution, heated to 70-100‹.C. and having a Ti content equivalent to 5-30 g. TiO 2 /l., the amount of seed being 1- 4% by wt. of the total amount of TiO 2 ; (3) heating the mixture at about 105‹ C. for 0À5-3 hours to hydrolyse the titanium chloride solution; (4) separating needle-shaped TiO 2 hydrate precipitate and calcining it at 800-900‹ C in presence of a growth-inhibiting compound of one or more of K, Rb, Cs, Ca, Sr, Ba, Al, S, P and Si; (5) grinding the calcined product under such mild conditions that the needles -are not destroyed. The initial titanium chloride solution may be one obtained by digestion of an ore with cone. HCl arid which has been freed of part of the iron initially present by crystallization. In examples, calcination is effected in presence of (1) 0À28% K 2 O and 0À5% SiO 2 ; (2) 0À28% K 2 O ; (3) 0À28% K 2 O and 0À6% P 2 O 5 . The initial titanium chloride solution, derived from ilmenite, contained Fe and Mg.

5. 发明授权

US3329484A Titanium dioxide pigment and method for preparation thereof 失效
标题翻译：二氧化钛颜料及其制备方法
公开(公告)号：US3329484A
公开(公告)日：1967-07-04
申请号：US57952666
申请日：1966-09-15
申请人： DOW CHEMICAL CO
发明人： LONG RAY S , ELLIS DAVID A , COX KENNETH E , MAGNER JAMES E
IPC分类号： C01G23/053 , C09C1/36
CPC分类号： B82Y30/00 , C01G23/0538 , C01P2004/54 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2006/60 , C09C1/3607

6. 发明公开

US20240270596A1 TITANIUM OXIDE PARTICLES AND METHOD FOR PRODUCING SAME 审中-公开
公开(公告)号：US20240270596A1
公开(公告)日：2024-08-15
申请号：US18568296
申请日：2023-06-30
申请人： ISHIHARA SANGYO KAISHA, LTD.
发明人： Takuya HOSOKAWA
IPC分类号： C01G23/053
CPC分类号： C01G23/0538 , C01P2002/02 , C01P2002/72 , C01P2002/88 , C01P2004/03 , C01P2004/50 , C01P2004/64 , C01P2006/12
摘要： The present invention produces titanium oxide particles which have a sufficiently small average aggregate particle diameter (D50), while containing much less amorphous components. According to the present invention, a solution containing titanium (oxy)chloride and a carboxylic acid and/or a salt thereof is heated at a temperature that is not less than 95° C. but not more than the boiling point of the solution (first hydrolysis step); and a solution, which is obtained by mixing a solution that contains a product of the first hydrolysis step with titanium (oxy)chloride and a carboxylic acid and/or a salt thereof, is heated at a temperature that is not less than 95° C. but not more than the boiling point of the solution (second hydrolysis step). In addition, the present invention provides titanium oxide particles which have an average aggregate particle diameter (D50) of 15 nm to 200 nm, while having a content of amorphous components of 7% by mass or less.

7. 发明授权

US09567236B2 Rutile titanium dioxide nanoparticles and ordered acicular aggregates of same 有权
标题翻译：金红石二氧化钛纳米颗粒和有序的针状聚集体相同
公开(公告)号：US09567236B2
公开(公告)日：2017-02-14
申请号：US14775810
申请日：2014-03-14
申请人： Cristal Inorganic Chemicals Switzerland Ltd
发明人： Guoyi Fu , Mark B. Watson
IPC分类号： C01G23/053 , C01G23/047
CPC分类号： C01G23/0538 , C01G23/047 , C01G23/053 , C01G23/0536 , C01P2002/60 , C01P2002/72 , C01P2004/03 , C01P2004/10 , C01P2004/45 , C01P2004/64 , C01P2006/12
摘要： Ordered acicular aggregates of elongated TiO2 crystallites which resemble nano-sized flower bouquets and/or triangular funnels, and process for their preparation by thermally hydrolyzing a soluble TiO2 precursor compound in aqueous solution in the presence of a morphology controlling agent selected from carboxylic acids and amino acids.
摘要翻译：类似于纳米尺寸花束和/或三角形漏斗的细长TiO 2微晶的有序针状聚集体，以及在选自羧酸和氨基的形态控制剂存在下在水溶液中热水解可溶性TiO 2前体化合物的制备方法酸。

8. 发明授权

US09260318B2 Mesoporous titanium dioxide nanoparticles and process for their production 有权
标题翻译：介孔二氧化钛纳米粒子及其生产工艺
公开(公告)号：US09260318B2
公开(公告)日：2016-02-16
申请号：US14528259
申请日：2014-10-30
申请人： Cristal USA Inc.
发明人： Guoyi Fu , Mark Watson
IPC分类号： C22B34/12 , C01G23/053 , B82Y30/00 , B82Y40/00
CPC分类号： C01G23/0538 , B82Y30/00 , B82Y40/00 , C01G23/0536 , C01P2004/03 , C01P2004/32 , C01P2004/64 , C01P2006/12 , C01P2006/14 , C01P2006/16 , C01P2006/17 , Y10T428/2982
摘要： TiO2 nanoparticles having improved consistent particle morphology, uniform particle size, and which contain uniform intra-particle pores in the mesopore size range are produced by wet chemical hydrolysis.
摘要翻译：通过湿化学水解制备具有改善的一致颗粒形态，均匀粒度并且在中孔尺寸范围内含有均匀的颗粒内孔的TiO 2纳米颗粒。

9. 发明申请

US20150299417A1 ORGANIC SOLVENT DISPERSION OF TITANIUM OXIDE SOLID-SOLUTION PARTICLES, MAKING METHOD, AND COATING COMPOSITION 审中-公开
标题翻译：氧化钛固溶体颗粒的有机溶剂分散体，制备方法和涂料组合物
公开(公告)号：US20150299417A1
公开(公告)日：2015-10-22
申请号：US14687344
申请日：2015-04-15
申请人： SHIN-ETSU CHEMICAL CO., LTD.
发明人： Kohei MASUDA , Koichi HIGUCHI , Manabu FURUDATE , Tomohiro INOUE
IPC分类号： C08K3/22 , C09D1/00 , C08K3/36 , C08K3/08 , C08K5/5419
CPC分类号： C08K3/22 , C01G23/04 , C01G23/0538 , C01P2002/52 , C01P2002/86 , C01P2004/64 , C08K3/08 , C08K3/36 , C08K5/5419 , C08K2003/2241 , C09C1/3661 , C09C1/3684 , C09D1/00 , C09D7/62 , C09D7/67
摘要： Core/shell type tetragonal titanium oxide solid-solution particles each consisting of a core of tetragonal titanium oxide having tin and manganese incorporated in solid solution and a shell of silicon oxide are dispersed in an organic solvent. The core/shell type particles have a diameter D50 of 5-50 nm. The amount of tin incorporated in solid solution is to provide a molar ratio Ti/Sn of 10-1,000, and the amount of manganese incorporated in solid solution is to provide a molar ratio Ti/Mn of 10-1,000.
摘要翻译：由固体溶液中含有锡和锰的四方晶氧化钛芯和氧化硅壳组成的核/壳型四方钛氧化物固溶体颗粒分散在有机溶剂中。核/壳型颗粒的直径D50为5-50nm。掺入固溶体中的锡的量为Ti / Sn的摩尔比为10-1,000，并且固溶体中掺入的锰的量为10-1,000的Ti / Mn摩尔比。

10. 发明授权

US09108862B2 Method of making rutile titanium dioxide microspheres containing elongated TiO2-nanocrystallites 有权
标题翻译：制备含有细长TiO 2纳米晶的金红石二氧化钛微球的方法
公开(公告)号：US09108862B2
公开(公告)日：2015-08-18
申请号：US13842608
申请日：2013-03-15
申请人： Cristal Inorganic Chemicals Switzerland Ltd
发明人： Guoyi Fu , Mark B Watson
IPC分类号： C01G23/02 , C01G23/047 , C01G23/053 , B82Y30/00
CPC分类号： C01G23/0538 , B82Y30/00 , C01G23/026 , C01G23/047 , C01G23/053 , C01G23/0536 , C01P2002/72 , C01P2004/03 , C01P2004/04 , C01P2004/32 , C01P2004/45 , C01P2004/61 , C01P2004/62 , C01P2004/64 , C01P2004/90 , C01P2006/12 , C01P2006/14 , Y10T428/2982
摘要： Rutile TiO2 microspheres and microparticles in a botryoidal morphology which form from ordered acicular aggregates of elongated TiO2 crystallites that resemble nano-sized flower bouquets and/or triangular funnels, and process for their preparation by thermally hydrolyzing a soluble TiO2 precursor compound in aqueous solution in the presence of a morphology controlling agent selected from carboxylic acids and amino acids.
摘要翻译：金红石二氧化钛微球体和微粒形态，其形成为类似于纳米尺寸花束和/或三角形漏斗的细长TiO 2微晶的有序针状聚集体，以及通过在水溶液中热解水解可溶性TiO 2前体化合物而制备的方法存在选自羧酸和氨基酸的形态控制剂。

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