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1. 发明申请

US20220248272A1 METHODS AND APPARATUSES FOR PRODUCTION OF CARBON, CARBIDE ELECTRODES, AND CARBON COMPOSITIONS 有权
公开(公告)号：US20220248272A1
公开(公告)日：2022-08-04
申请号：US17717442
申请日：2022-04-11
申请人： West Virginia University Research Corporation
发明人： ALFRED H. STILLER , Christopher Yurchick
IPC分类号： H04W28/26 , H04W72/04 , H04W72/12 , H04W74/00
摘要： Method comprising providing at least one solid carbide chemical compound and reducing a metal cation with use of the solid carbide chemical compound. A method comprising producing elemental carbon material from the oxidation of carbide in at least one carbide chemical compound (e.g., calcium carbide) in at least one anode of an electrochemical cell apparatus, such as a galvanic cell apparatus. The cathode can be a variety of metals such as zinc or tin. The reaction can be carried out at room temperature and normal pressure. An external voltage also can be applied, and different forms of carbon can be produced depending on the reactants used and voltage applied. For carrying out the method, an apparatus comprising at least one galvanic cell comprising: at least one anode comprising at least one carbide chemical compound, and at least one cathode. For carrying out the method and constructing the apparatus, an electrode structure comprising at least one carbide chemical compound, wherein the carbide chemical compound is a salt-like carbide; and at least one electronically conductive element different from the carbide. Carbon compositions of various forms are also prepared by the methods and apparatus and with use of the electrode structure. Large pieces of pure carbon can be produced. Post-reaction processing of the carbon can be carried out such as exfoliation.

2. 发明申请

US20220235474A1 METHODS, APPARATUSES, AND ELECTRODES FOR CARBIDE-TO-CARBON CONVERSION WITH NANOSTRUCTURED CARBIDE CHEMICAL COMPOUNDS 有权
公开(公告)号：US20220235474A1
公开(公告)日：2022-07-28
申请号：US17717544
申请日：2022-04-11
申请人： WEST VIRGINIA UNIVERSITY RESEARCH CORPORATION
发明人： J. Steven RUTT
IPC分类号： C25B11/057 , C01B32/184 , C01B32/25 , C01B32/914 , C25B11/04 , C01B32/942 , C01B32/05 , C25B1/00
摘要： Nanostructured carbide chemical compound is used to convert carbide to carbon. A method comprising: providing at least one carbide chemical compound and reducing a metal cation with use of the carbide chemical compound to form elemental carbon, wherein the carbide chemical compound is nanostructured. The nanostructured carbide chemical compound can be in the form of a nanoparticle, a nanowire, a nanotube, a nanofilm, a nanoline. The reactant can be a metal salt. Electrochemical reaction, or reaction in the melt or in solution, can be used to form the carbon. The nanostructured carbide chemical compound can be an electrode.

3. 发明授权

US11332833B2 Methods, apparatuses, and electrodes for carbide-to-carbon conversion with nanostructured carbide chemical compounds 有权
公开(公告)号：US11332833B2
公开(公告)日：2022-05-17
申请号：US15491715
申请日：2017-04-19
申请人： WEST VIRGINIA UNIVERSITY RESEARCH CORPORATION
发明人： J. Steven Rutt
IPC分类号： C01B31/02 , C25B11/057 , C01B32/184 , C01B32/25 , C01B32/914 , C25B11/04 , C01B32/942 , C01B32/05 , C25B1/00
摘要： Nanostructured carbide chemical compound is used to convert carbide to carbon. A method comprising: providing at least one carbide chemical compound and reducing a metal cation with use of the carbide chemical compound to form elemental carbon, wherein the carbide chemical compound is nanostructured. The nanostructured carbide chemical compound can be in the form of a nanoparticle, a nanowire, a nanotube, a nanofilm, a nanoline. The reactant can be a metal salt. Electrochemical reaction, or reaction in the melt or in solution, can be used to form the carbon. The nanostructured carbide chemical compound can be an electrode.

4. 发明授权

US10906807B2 Methods for production of carbon and hydrogen from natural gas and other hydrocarbons 有权
公开(公告)号：US10906807B2
公开(公告)日：2021-02-02
申请号：US16240422
申请日：2019-01-04
申请人： West Virginia University Research Corporation
发明人： Alfred H. Stiller
IPC分类号： C01B3/24 , B01J21/10 , C01B3/26 , C01B32/05 , B01J37/08 , B01J27/22
摘要： A method for producing elemental carbon and hydrogen gas directly from a hydrocarbon (for example, natural gas or methane) using a chemical reaction or series of reactions. In an aspect, other materials involved such as, for example, elemental magnesium, remain unchanged and function as a catalyst.

5. 发明授权

US10696555B2 Process for pure carbon production 有权
公开(公告)号：US10696555B2
公开(公告)日：2020-06-30
申请号：US16140060
申请日：2018-09-24
申请人： WEST VIRGINIA UNIVERSITY RESEARCH CORPORATION
发明人： Alfred H. Stiller
IPC分类号： C01B32/25 , C01B32/26 , B01J19/24 , C01F11/28 , C01F7/58 , C01B32/05 , C01B32/184 , C01B32/36
摘要： The disclosure provides for methods of oxidizing carbide anions, or negative ions, from salt like carbides at low temperatures below about 600° C. In another aspect, the disclosure provides for reactions with intermediate transition metal carbides. In yet another aspect, the disclosure provides for a system of reactions where salt-like carbide anions and intermediate carbide anions are oxidized to produce pure carbon of various allotropes.

6. 发明授权

US08741574B2 Gene expression signature of genomic instability in breast cancer 有权
标题翻译：乳腺癌基因组不稳定基因表达特征
公开(公告)号：US08741574B2
公开(公告)日：2014-06-03
申请号：US13119101
申请日：2009-09-15
申请人： Karl Thomas Ried , Jens Habermann , Nancy Lan Guo , Gert Auer
发明人： Karl Thomas Ried , Jens Habermann , Nancy Lan Guo , Gert Auer
IPC分类号： C12Q1/68
CPC分类号： G01N33/57415 , C12Q1/6886 , C12Q2600/112 , C12Q2600/118 , C12Q2600/136 , C12Q2600/158 , G01N33/5011
摘要： Methods of assessing genomic instability in breast cancer tissue by measuring the expression level of genes CDKN2A, SCYA18, STK15, NXF1, cDNA Dkfzp762M127, p28 KIAA0882, MYB, Human clone 23948, RERG, HNF3A, and ACADSB or a nucleic acid sequence comprising about 90% or greater sequence identity to SEQ ID NO: 21 in breast cancer tissue, an array suitable for use in such methods, and related methods and compositions.
摘要翻译：通过测量基因CDKN2A，SCYA18，STK15，NXF1，cDNA Dkfzp762M127，p28 KIAA0882，MYB，人克隆23948，RERG，HNF3A和ACADSB或包含约90个核酸的核酸序列的表达水平来评估乳腺癌组织中基因组不稳定性的方法在乳腺癌组织中与SEQ ID NO：21的序列同一性的百分比或更高，适用于这些方法的阵列以及相关的方法和组合物。

7. 发明申请

US20130029293A1 Non-Invasive Ultrasonic Gingival Tissue Diagnosis 有权
标题翻译：非侵入性超声牙龈组织诊断
公开(公告)号：US20130029293A1
公开(公告)日：2013-01-31
申请号：US13560236
申请日：2012-07-27
申请人： Osama M. Mukdadi , Ahmed M. Mahmoud , Eros S. Chaves , Richard Crout
发明人： Osama M. Mukdadi , Ahmed M. Mahmoud , Eros S. Chaves , Richard Crout
IPC分类号： A61B8/14
CPC分类号： A61B8/08 , A61B8/12 , A61B8/4245 , A61B8/483 , A61B8/5207 , G06F19/321 , G06T7/0012
摘要： Disclosed are various embodiments for echoperiodontal imaging. In one embodiment, a system includes a transducer configured to transmit a series of ultrasonic signals at a plurality of corresponding locations along soft tissue of a jaw and receive a plurality of echo signals; and an imaging system controller configured to obtain a plurality of echo signal data of the soft tissue and a plurality of transducer positions, where each echo signal data corresponds to one of the plurality of transducer position.
摘要翻译：公开了用于超声周期成像的各种实施例。在一个实施例中，系统包括被配置为在沿着钳口的软组织的多个对应位置处传送一系列超声波信号并且接收多个回波信号的换能器; 以及成像系统控制器，被配置为获得所述软组织的多个回波信号数据和多个换能器位置，其中每个回波信号数据对应于所述多个换能器位置中的一个。

8. 发明申请

US20060118488A1 Apparatus and method of utilizing a sawed tooth shaped gradient for chromatographic separation 审中-公开
标题翻译：利用锯齿形梯度进行色谱分离的装置和方法
公开(公告)号：US20060118488A1
公开(公告)日：2006-06-08
申请号：US11153862
申请日：2005-06-15
申请人： Aaron Timperman , Daniel Morris
发明人： Aaron Timperman , Daniel Morris
IPC分类号： B01D15/08
CPC分类号： G01N30/34 , B01D15/166 , B01J20/286 , B01J20/287 , B01J20/288 , G01N30/02 , B01D15/34
摘要： The present invention provides an apparatus and a method wherein the movement of analytes on a chromatographic separation column is controlled by the manipulation of isocratic and gradient flow. Such manipulation allows for a distinct set of analytes to be eluted from the chromatography column and delivered downstream for further separation and/or processing while the remainder of the sample remains in a “holding pattern” on the chromatography column. As such, the present invention allows for a small portion of the sample to be processed downstream of the column while substantially eliminating undesirable isocratic elution from the column during such downstream processing. Once the downstream processing has been completed, the column of the present invention elutes a second distinct analyte and the remainder of the sample is maintained in a holding pattern. The process may be repeated until the entire sample has been eluted from the chromatography column.
摘要翻译：本发明提供了一种装置和方法，其中分析物在色谱分离柱上的移动通过等度梯度流的操纵来控制。这样的操作允许从色谱柱洗脱出一组不同的分析物，并在下游进行进一步分离和/或处理，同时样品的其余部分保留在色谱柱上的“保持模式”中。因此，本发明允许样品的一小部分在柱下游进行处理，同时基本上消除了在这种下游处理期间从柱中不期望的等度洗脱。一旦下游处理已经完成，本发明的色谱柱洗脱第二种不同的分析物，并且样品的其余部分保持在保持图案中。可以重复该过程，直到整个样品已经从色谱柱洗脱出来。

9. 发明申请

US20040163961A1 Apparatus and method for using bi-directional capillary electrophoresis 审中-公开
标题翻译：使用双向毛细管电泳的装置和方法
公开(公告)号：US20040163961A1
公开(公告)日：2004-08-26
申请号：US10784352
申请日：2004-02-23
申请人： West Virginia University Research Corporation
发明人： Aaron T. Timperman
IPC分类号： G01N027/453
CPC分类号： G01N27/44756
摘要： The present invention provides an apparatus and method of utilizing bi-directional capillary electrophoresis (nullCEnull) device. In one embodiment, cations are drawn into a first uncharged channel towards a negative electrode and anions are drawn into a second uncharged channel towards a positive electrode. The uncharged channels allows for minimal interaction between the sample and the walls of the channel which allows for minimal sample loss. The present invention also provides a method of separating anions from cations. The method comprises delivering the mixture to a bi-directional CE device. Following delivery, cations are drawn into a first uncharged channel towards a negative electrode and anions are drawn into a second uncharged channel towards a positive electrode. In one aspect of the present invention, the bi-directional CE device engages a microfluidic proteome analysis system.
摘要翻译：本发明提供了利用双向毛细管电泳（“CE”）装置的装置和方法。在一个实施方案中，将阳离子吸引到朝向负极的第一不带电通道中，并将阴离子吸引到朝向正电极的第二不带电通道中。不带电的通道允许样品和通道壁之间的最小交互，从而允许最小的样品损失。本发明还提供了一种从阳离子中分离阴离子的方法。该方法包括将混合物输送到双向CE器件。在递送之后，阳离子被吸入朝向负极的第一不带电通道，阴离子被吸入朝向正电极的第二不带电通道。在本发明的一个方面，双向CE器件接合微流体蛋白质组分析系统。

10. 发明申请

US20030089605A1 Microfluidic system for proteome analysis 审中-公开
标题翻译：用于蛋白质组分析的微流体系统
公开(公告)号：US20030089605A1
公开(公告)日：2003-05-15
申请号：US10273494
申请日：2002-10-18
申请人： West Virginia University Research Corporation
发明人： Aaron T. Timperman
IPC分类号： G01N027/453
CPC分类号： G01N27/44791 , B01L3/5027 , B01L3/502707 , B01L3/502753 , B01L2200/10 , B01L2400/0415 , G01N27/44717 , G01N27/44743 , G01N27/44773 , G01N33/6803
摘要： The invention provides a microfluidic system and method to rapidly analyze large numbers of compounds or complex mixtures of compounds, particularly, low abundance cellular proteins involved in cell signaling pathways. In one aspect, an integrated microfluidic system comprises an upstream separation module (preferably, a multi-dimensional separation device), a microfluidic device for on-device protein digestion of substantially separated proteins received from the upstream separation module, a downstream separation module for separating digestion products of said proteins, a peptide analysis module and a processor for determining the amino acid sequence of said proteins. Preferably, the system comprises an interfacing microfluidic device between the downstream separation module and the peptide analysis module.
摘要翻译：本发明提供了一种微流体系统和方法，用于快速分析大量化合物或化合物的复合混合物，特别是涉及细胞信号通路的低丰度细胞蛋白质。在一个方面，集成的微流体系统包括上游分离模块（优选地，多维分离装置），用于从上游分离模块接收的基本上分离的蛋白质的装置内蛋白质消化的微流体装置，用于分离的下游分离模块所述蛋白质的消化产物，肽分析模块和用于测定所述蛋白质的氨基酸序列的处理器。优选地，该系统包括在下游分离模块和肽分析模块之间的界面微流体装置。

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