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1. 发明授权

US06153661A Onium borates/borates of organometallic complexes and cationic initiation of polymerization therewith 失效
公开(公告)号：US06153661A
公开(公告)日：2000-11-28
申请号：US851713
申请日：1997-05-06
申请人： Frederic Castellanos , Jacques Cavezzan , Jean-Pierre Fouassier , Christian Priou
发明人： Frederic Castellanos , Jacques Cavezzan , Jean-Pierre Fouassier , Christian Priou
IPC分类号： C07F5/02 , C07F9/50 , C07F19/00 , C08F2/46 , C08F2/50 , C08F4/00 , C08F4/52 , C08G59/24 , C08G59/68 , C08G59/72 , G03F7/004 , G03F7/029 , G03F7/038
CPC分类号： C08G59/72 , C07F5/022 , C08F2/50 , C08F4/52 , C08G59/24 , C08G59/68 , G03F7/0042 , G03F7/0045 , G03F7/029 , G03F7/038
摘要： Novel onium borates of an element of Groups 15 to 17 of the Periodic Table, or borates of an organometallic complex of an element of Groups 4 to 10 of the Periodic Table, well suited for the photochemical/electron beam cationic initiation of polymerization/crosslinking, the anionic borate moiety of which having the formula:[BX.sub.a R.sub.b ].sup.-in which a and b are integers ranging from 0 to 4 and a+b=4; the symbols X are each a halogen atom when a ranges up to 3 and an OH functional group when a ranges up to 2; and the symbols R, which may be identical or different, are each a phenyl radical substituted by at least one element or electron-withdrawing substituent or by at least two halogen atoms, or an aryl radical containing at least two aromatic ring members, or such aryl radical bearing at least one electron-withdrawing substituent.

2. 发明授权

US6124235A Accelerator system for crosslinking polymers which harden on exposure to the moisture in air 失效
标题翻译：用于交联聚合物的促进剂体系，其在暴露于空气中的水分时变硬
公开(公告)号：US6124235A
公开(公告)日：2000-09-26
申请号：US888323
申请日：1997-07-03
申请人： Michel Letoffe , Jean-Marc Pujol
发明人： Michel Letoffe , Jean-Marc Pujol
IPC分类号： C08L83/04 , C08J3/24 , C08K3/32 , C08K3/38 , C08K5/00 , C08K5/54 , C08K13/02 , C08L101/00 , C08L101/02 , C08L101/10 , B01J23/00 , B01J21/02 , B01J21/08 , B01J23/32
CPC分类号： C08K5/54 , C08K3/32 , C08K3/38 , C08K5/0025
摘要： An accelerator system for the cold crosslinking of polymers which harden on exposure to moisture by hydrolysis/condensation, comprising: (C) x parts by weight of a catalyst for crosslinking the said polymers by polycondensation, x ranging from 0.01 to 10; (E) Y parts by weight of a solid inorganic compound containing an amount y of water in the form of water of hydration and/or water adsorbed by capillary condensation, this amount y ranging from 0.5 to 40 parts by weight, and which can represent up to 70% of the weight of the said solid inorganic compound; (F) z parts by weight of fillers, z ranging from 0 to 50; (D) 100-(x+Y+z) parts by weight of a diluent or of a solvent of the said catalyst (C), the diluent or solvent having a dynamic viscosity at 25.degree. C. of the order of 50 to 200,000 mPa.s; the respective amounts of the four constituents (C), (E), (F) and (D) being such that the system obtained exists in the form of a manipulable paste. The accelerator system is used for accelerating silicone compositions which harden on exposure to the moisture in air.
摘要翻译：用于通过水解/缩合使得在暴露于水分时硬化的聚合物的冷交联的加速剂体系包括：（C）x重量份用于通过缩聚交联所述聚合物的催化剂，x为0.01至10; （E）Y重量份含有以水分和/或毛细管冷凝吸附的水的形式的水的y的固体无机化合物，该量y为0.5〜40重量份，并且可以代表高达70％的所述固体无机化合物的重量; （F）z重量份的填料，z为0至50; （D）100-（x + Y + z）重量份稀释剂或所述催化剂（C）的溶剂，稀释剂或溶剂在25℃下的动态粘度为50至200,000 mPa.s; 四种成分（C），（E），（F）和（D）的相应量使得所获得的体系以可操作的糊剂的形式存在。加速器系统用于加速在暴露于空气中的水分时变硬的硅酮组合物。

3. 发明授权

US6093487A Polymer/CaCO.sub.3 composite core/sheath particulates and hollow . CaCO.sub3 microbeads prepared therefrom 失效
标题翻译：聚合物/ CaCO 3复合芯/鞘颗粒和由其制备的中空CaCO 3微珠
公开(公告)号：US6093487A
公开(公告)日：2000-07-25
申请号：US55271
申请日：1998-04-06
申请人： Dominique Dupuis , Dominique Labarre , Gilles Mur
发明人： Dominique Dupuis , Dominique Labarre , Gilles Mur
IPC分类号： C08J3/12 , B01J13/02 , C01F11/18 , C08J3/20 , C08J3/21 , C08J3/22 , C08K7/16 , C08K7/24 , C08K9/02 , B32B5/16
CPC分类号： B82Y30/00 , C01F11/18 , C08J3/20 , C08J3/21 , C08J3/226 , C01P2004/34 , C01P2004/62 , C01P2004/64 , C01P2006/12 , Y10T428/258 , Y10T428/2991 , Y10T428/2998
摘要： Composite core/sheath particulates comprising an organic polymer core at least partly coated with calcium carbonate, these core/sheath particulates having a mean particle size not exceeding 5 .mu.m, well suited for reinforcing plastic/elastomer substrates, are conveniently converted, e.g., via calcination, into hollow calcium carbonate microbeads which comprise CaCO.sub.3 shells having a mean particle size not exceeding 5 .mu.m; such hollow microbeads are themselves well suited for enhancing the low-temperature flexibility of elastomer substrates, notably vehicle tires.
摘要翻译：复合芯/皮颗粒包含至少部分涂覆有碳酸钙的有机聚合物芯，这些非常适合于增强塑料/弹性体基材的平均粒度不超过5μm的核/皮颗粒可以方便地转化，例如通过煅烧成包含平均粒径不超过5μm的CaCO 3壳的中空碳酸钙微珠; 这样的空心微珠本身非常适合于提高弹性体基材，特别是车辆轮胎的低温柔韧性。

4. 发明授权

US5916482A Use of a compound based on a rare-earth phosphate as a luminophor in plasma systems 失效
公开(公告)号：US5916482A
公开(公告)日：1999-06-29
申请号：US970285
申请日：1997-11-14
申请人： Denis Huguenin
发明人： Denis Huguenin
IPC分类号： C09K11/77 , C09K11/81 , C09K4/46
CPC分类号： C09K11/7777 , C09K11/7795
摘要： The invention relates to the use as a luminophor in plasma systems of a compound based on an yttrium, lanthanum, gadolinium or lutecium phosphate doped with at least one rare earth chosen from the group comprising terbium, praseodymium, europium and cerium.

5. 发明授权

US5864049A Process for the preparation of mono- and dicarboxylic acids from unsaturated fatty acids and/or their derivatives 失效
标题翻译：从不饱和脂肪酸和/或其衍生物制备单羧酸和二羧酸的方法
公开(公告)号：US5864049A
公开(公告)日：1999-01-26
申请号：US935546
申请日：1997-09-23
申请人： Emmanuel Dos Santos , Pascal Metivier
发明人： Emmanuel Dos Santos , Pascal Metivier
IPC分类号： B01J27/13 , B01J27/188 , B01J27/19 , B01J31/04 , C07B61/00 , C07C51/16 , C07C51/27 , C07C51/285 , C07C53/124 , C07C55/00 , C07C55/16 , C07C55/18 , C07C69/24 , C07C69/347 , C07C69/44 , C11C3/00
CPC分类号： C07C51/27 , C07C51/285
摘要： The present invention relates to a process for the preparation of carboxylic acids from unsaturated fatty acids and/or their derivatives.The process of the invention is characterized in that it comprises the following stages:a stage which consists in oxidizing an unsaturated fatty acid in the form of acid and/or of ester using hydrogen peroxide, in the presence of a metal oxide or of a carboxylic acid optionally used in combination with a ruthenium-based catalyst,a stage which consists in reacting the reaction mixture originating from the preceding stage with nitric acid in the presence of a vanadium-based catalyst, optionally used in combination with a cocatalyst, and thena stage of recovery of the mono- and dicarboxylic acids.It is particularly well suited for the preparation of saturated mono- and dicarboxylic acids obtained from unsaturated fatty acids such as oleic acid or from oils and fats.
摘要翻译：本发明涉及从不饱和脂肪酸和/或其衍生物制备羧酸的方法。本发明的方法的特征在于其包括以下阶段：在金属氧化物或羧酸存在下，使用过氧化氢氧化酸和/或酯形式的不饱和脂肪酸的阶段任选地与钌基催化剂组合使用的酸，这一阶段，其包括在钒基催化剂存在下将来自前一阶段的反应混合物与硝酸反应，任选与助催化剂组合使用，然后将单羧酸和二羧酸的回收阶段。特别适用于制备由不饱和脂肪酸如油酸或油脂获得的饱和单羧酸和二羧酸。

6. 发明授权

US5856577A Process for the preparation of fluoroanilines from fluorinated nitrated benzene compounds 失效
标题翻译：由氟化硝化苯化合物制备氟苯胺的方法
公开(公告)号：US5856577A
公开(公告)日：1999-01-05
申请号：US849144
申请日：1997-05-28
申请人： Georges Cordier , Gilbert Guidot , Philippe Marion , Claude Mercier
发明人： Georges Cordier , Gilbert Guidot , Philippe Marion , Claude Mercier
IPC分类号： C07B61/00 , C07C209/36 , C07C211/52
CPC分类号： C07C209/36
摘要： The instant invention relates to a process for the preparation of fluoroanilines of formula (I) wherein a fluorinated nitrated benzene compound of formula (II) is subjected to a catalytic hydrogenation in a liquid medium containing a catalyst, under hydrogen pressure, carrying out a catalytic reduction reaction and, optionally, a hydrogenolysis reaction, wherein the compound of formula (II) is introduced gradually into the said medium so that the content of compound of formula (II) in the liquid remains less than or equal to 1000 ppm by mass, in order selectively to form the compound of formula (I).
摘要翻译： PCT No.PCT / FR95 / 01575 Sec。 371日期1997年5月28日 102（e）日期1997年5月28日PCT提交1995年11月29日PCT公布。公开号WO96 / 16926 日本1996年6月6日本发明涉及制备式（I）的氟代苯胺的方法，其中将式（II）的氟化硝化苯化合物在氢气压力下在含有催化剂的液体介质中进行催化氢化，进行催化还原反应和任选的氢解反应，其中将式（II）化合物逐渐引入所述介质中，使得液体中式（II）化合物的含量保持小于或等于为了选择性地形成式（I）的化合物，为1000质量ppm。

7. 发明授权

US5824820A Process for the preparation of citraconic anhydride 失效
标题翻译：制备柠康酸酐的方法
公开(公告)号：US5824820A
公开(公告)日：1998-10-20
申请号：US668027
申请日：1996-06-19
申请人： Michel Alas
发明人： Michel Alas
IPC分类号： C12P7/26 , B01J31/02 , C07B61/00 , C07C51/56 , C07D307/26 , C07D307/60 , C12P7/44 , C12R1/66 , C07C45/66 , C12P17/04
CPC分类号： C07C51/56
摘要： The present invention relates to a novel process for the preparation of citraconic anhydride. More precisely, the invention relates to a process for the preparation of citraconic anhydride from a starting material comprising itaconic acid. The process for the preparation of citraconic anhydride may be performed continuously starting from itaconic acid, or continuously or in a batchwise manner starting directly from a fermentation broth of itaconic acid or of by-products from the manufacture of itaconic acid.
摘要翻译：本发明涉及一种制备柠康酸酐的新方法。更准确地说，本发明涉及从包含衣康酸的原料制备柠康酸酐的方法。制备柠康酸酐的方法可以从衣康酸开始连续地或以间歇方式从衣康酸的发酵液或衣康酸的副产物开始连续进行。

8. 发明授权

US5820764A Treatment/removal of byproduct aqueous effluents comprising hydroxynitro-aromatic compounds 失效
标题翻译：包含羟基硝基芳族化合物的副产物含水废水的处理/除去
公开(公告)号：US5820764A
公开(公告)日：1998-10-13
申请号：US959731
申请日：1997-10-28
申请人： Faouzi Joulak , Louis Le Bris , Philippe Marion
发明人： Faouzi Joulak , Louis Le Bris , Philippe Marion
IPC分类号： C02F1/66 , C02F9/00 , C07C201/16 , C02F1/52
CPC分类号： C02F1/66 , C07C201/16 , C02F2103/36 , Y10S210/909
摘要： Objectionable byproduct aqueous effluents containing contaminating amounts of hydroxynitroaromatic compounds, in particular those aqueous effluents produced during the synthesis of nitroaromatic compounds, e.g., dinitrotoluenes, via reaction of an aromatic compound with nitric acid in the presence of sulfuric acid, are efficiently, facilely and economically treated/removed by (a) intimately contacting a mixture of at least one nitroaromatic compound and at least one hydroxynitroaromatic compound with an aqueous wash medium containing a neutralizing agent, (b) separating the resulting admixture into an organic phase and an aqueous phase, (c) recycling a fraction of the separated aqueous phase to the aqueous wash medium to thus constitute a portion thereof, and (d) periodically draining a fraction of the wash medium, whether to destruction thereof or to waste.
摘要翻译：含有污染量的羟基硝基芳族化合物的有害副产物含水废水，特别是在硫酸存在下通过芳族化合物与硝酸的反应合成硝基芳族化合物（例如二硝基甲苯）期间产生的含水废水，是有效，便利和经济的通过（a）使至少一种硝基芳族化合物和至少一种羟基硝基芳族化合物的混合物与含有中和剂的水性洗涤介质紧密接触来处理/除去，（b）将所得混合物分离成有机相和水相（ c）将分离的水相的一部分循环到水性洗涤介质中，从而构成其一部分，和（d）定期排出洗涤介质的一部分，不管其是否破坏或浪费。

9. 发明授权

US5814145A Cementation slurries for improvedly encasing reinforcing elements therefor 失效
公开(公告)号：US5814145A
公开(公告)日：1998-09-29
申请号：US407628
申请日：1995-03-21
申请人： Jerome Dugat , Laurent Frouin , Evelyne Prat , Pierre Richard
发明人： Jerome Dugat , Laurent Frouin , Evelyne Prat , Pierre Richard
IPC分类号： E04C5/01 , B28C5/00 , C04B7/13 , C04B12/00 , C04B14/06 , C04B20/02 , C04B22/06 , C04B28/02 , C04B40/00 , C04B111/70 , C04B14/04
CPC分类号： C04B14/06 , C04B14/062 , C04B20/026 , C04B28/02 , C04B40/0028 , C04B2111/70
摘要： Cementation slurries well suited for encasing reinforcing elements therefor, for example prestressed steel cable, while reducing the risk of embrittlement thereof, contain from about 1.5% to 3% by weight of homogenizing and exudation-reducing hydrophilic particulates (e.g., precipitated silica particles) that are inert in respect of liquids, have a specific surface area of greater than about 200 m.sup.2 /g and which are fragmentable during mixing and/or injection into multiple fragments having particle sizes ranging from about 5 to 300 nanometers.

10. 发明授权

US5811587A Process for the hydroxyalkylation of a carbocyclic aromatic ether 失效
标题翻译：碳环芳族醚的羟烷基化方法
公开(公告)号：US5811587A
公开(公告)日：1998-09-22
申请号：US776495
申请日：1997-01-23
申请人： Claude Moreau , Sylvie Razigade-Trousselier , Annie Finiels , Francois Fajula , Laurent Gilbert
发明人： Claude Moreau , Sylvie Razigade-Trousselier , Annie Finiels , Francois Fajula , Laurent Gilbert
IPC分类号： B01J29/06 , C07B41/02 , C07B61/00 , C07C41/30 , C07C43/23 , C07C45/38 , C07C47/575 , C07C45/36
CPC分类号： C07C45/38 , C07B41/02 , C07C41/30
摘要： The present invention concerns a process for the hydroxyalkylation of a carbocyclic aromatic ether. The invention preferably relates to the preparation of 3-methoxy-4-hydroxybenzyl alcohol by the hydroxymethylation of guaiacol. It also concerns the oxidation of the hydroxyalkylated ethers obtained, in particular the oxidation of 3-methoxy-4-hydroxybenzyl alcohol to 3-methoxy-4-hydroxybenzaldehyde, commonly known as "vanillin". The process for the hydroxyalkylation of a carbocyclic aromatic ether of the invention consists of reacting the aromatic ether with a carbonyl compound in the presence of a catalyst and is characterized in that the hydroxyalkylation reaction is carried out in the presence of an effective quantity of a zeolite.
摘要翻译： PCT No.PCT / FR96 / 00778 Sec。 371日期1997年1月23日 102（e）日期1997年1月23日PCT提交1996年5月24日PCT公布。 WO96 / 37452 PCT公开号日期：1996年11月28日本发明涉及碳环芳族醚的羟烷基化方法。本发明优选涉及通过愈创木酚的羟甲基化制备3-甲氧基-4-羟基苄醇。它还涉及所获得的羟烷基化醚的氧化，特别是3-甲氧基-4-羟基苄醇氧化为3-甲氧基-4-羟基苯甲醛，通常称为“香草醛”。本发明的碳环芳族醚的羟基烷基化方法包括在催化剂存在下使芳族醚与羰基化合物反应，其特征在于羟烷基化反应在有效量的沸石存在下进行。

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