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1. 发明授权

US4980501A Production of secondary-butyl fluoroester and secondary-butyl alcohol obtained therefrom 失效
标题翻译：制备由其获得的仲丁基氟酯和仲丁醇
公开(公告)号：US4980501A
公开(公告)日：1990-12-25
申请号：US523585
申请日：1990-03-19
申请人： John A. Scheben
发明人： John A. Scheben
IPC分类号： C07C69/63
CPC分类号： C07C67/055
摘要： A process for the production of secondary-butyl perfluoroester is provided by reacting ethylene with a perfluorocarboxylic acid in the presence of oxygen.
摘要翻译：通过在氧气存在下使乙烯与全氟羧酸反应来提供生产仲丁基全氟酯的方法。

2. 发明授权

US4866188A Synthesis of cyclic ethers 失效
标题翻译：环醚的合成
公开(公告)号：US4866188A
公开(公告)日：1989-09-12
申请号：US637370
申请日：1984-08-03
申请人： John A. Scheben
发明人： John A. Scheben
IPC分类号： C07D307/08 , C07D313/04
CPC分类号： C07D313/04 , C07D307/08
摘要： A process is disclosed for preparing a cyclic ether which comprises cyclodehydrating a polyhydroxy compound of the general formulaHOR.sup.1 HC--R.sup.2 --CHR.sup.3 OHin which R.sup.1 and R.sup.3, each of which is the same or different, is hydrogen or a lower aliphatic, cycloaliphatic or aryl group and R.sup.2 is a divalent aliphatic group of 1 to 10 carbon atoms containing 0, 1 or 2 etheric oxygen atoms or 0, 1 or 2 secondary or tertiary amine nitrogen atoms and 0, 1 or more lower aliphatic, cycloaliphatic and/or aryl groups containing 0 or 1 hydroxyl groups at elevated temperatures in the presence of a catalytically effective amount of a Group VIII metal catalyst or a Group VIII metal-containing material to provide a cyclic ether of the general formula ##STR1## in which R.sup.1, R.sup.2 and R.sup.3 are as defined above. The process is especially useful for preparing the commercially important cyclic ethers tetrahydrofuran and 1,4-dioxane which are derived from 1,4-butanediol and ethylene glycol and/or diethylene glycol, respectively.
摘要翻译：公开了一种制备环醚的方法，该方法包括将通式为HOR1HC-R2-CHR3OH的多羟基化合物环化脱水，其中R 1和R 3各自相同或不同，为氢或低级脂族，脂环族或芳基并且R 2是含有0,1或2个醚性氧原子或0,1或2个仲胺或叔胺氮原子和0,1或更多个低级脂族，脂环族和/或芳基的含1至10个碳原子的二价脂族基团， 0或1个羟基，在催化有效量的第VIII族金属催化剂或含Ⅷ族金属的物质存在下，在高温下提供通式为“IMAGE”的环醚，其中R 1，R 2和R 3为如上所述。该方法特别可用于制备分别衍生自1,4-丁二醇和乙二醇和/或二甘醇的商业上重要的环醚四氢呋喃和1,4-二恶烷。

3. 发明授权

US4831183A Conjugated alkadiene telomerization to organooxyalkadienes 失效
标题翻译：共轭二烯聚合到有机氧化烯二烯
公开(公告)号：US4831183A
公开(公告)日：1989-05-16
申请号：US259475
申请日：1988-10-17
申请人： Ronnie M. Hanes
发明人： Ronnie M. Hanes
IPC分类号： C07C41/06
CPC分类号： C07C41/06
摘要： A process for the telomerization of a conjugated alkadiene with an organic hydroxy compound to produce an organo-oxyalkadiene is disclosed. A palladium catalyst having an ionic ligand is employed in a substantially oxygen-free environment in the presence of an aprotic polar solvent so that the reaction products may be separated from the catalyst by solvent extraction with a hydrocarbon solvent.
摘要翻译：公开了一种用共轭二烯与有机羟基化合物调聚以产生有机 - 氧化烯的方法。具有离子配体的钯催化剂在非质子极性溶剂的存在下在基本上无氧的环境中使用，使得反应产物可以通过用烃溶剂的溶剂萃取与催化剂分离。

4. 发明授权

US4806584A Phase transfer compounds as accelerators of soap/sulfur vulcanization 失效
标题翻译：相转移化合物作为皂/硫硫化的促进剂
公开(公告)号：US4806584A
公开(公告)日：1989-02-21
申请号：US938668
申请日：1986-12-05
申请人： John M. Hoyt , Steven D. Blazey
发明人： John M. Hoyt , Steven D. Blazey
IPC分类号： C08K3/06 , C08K5/098 , C08K5/19 , C08K5/50 , C08K5/06
CPC分类号： C08K5/19 , C08K3/06 , C08K5/098 , C08K5/50
摘要： A composition of matter is disclosed comprising (1) a saturated elastomer having an active halogen-containing cure site, (2) a soap/sulfur cure system, and (3) a phase transfer compound. The phase transfer catalyst comprises a quaternary ammonium or phosphonium salt of a mineral acid or an alkylene oxide polymer. The phase transfer compounds accelerate soap/sulfur cures and make it possible to obtain acceptable cure rates with higher fatty acid soaps.
摘要翻译：公开了一种物质组合物，其包含（1）具有活性含卤素固化部位的饱和弹性体，（2）皂/硫固化体系，和（3）相转移化合物。相转移催化剂包括无机酸或烯化氧聚合物的季铵盐或鏻盐。相转移化合物加速皂/硫固化，并且可以用高级脂肪酸皂获得可接受的固化速度。

5. 发明授权

US4762724A Compositions and process for alfalfa drying 失效
公开(公告)号：US4762724A
公开(公告)日：1988-08-09
申请号：US26090
申请日：1987-03-16
申请人： Donald D. Staker , William S. Kain
发明人： Donald D. Staker , William S. Kain
IPC分类号： A23K1/00 , A23K3/02 , A23K3/03 , A23P1/08
CPC分类号： A23K30/15 , Y10S426/807
摘要： Aqueous compositions suitable for the treatment of alfalfa are provided herein. The aqueous compositions contain a hydrocarbon, a lower alkyl ester of a fatty acid and/or alkali metal carbonate. A process for applying said aqueous compositions to the alfalfa at the time of cutting to reduce drying time is also provided.

6. 发明授权

US4752866A Ozonator power supply employing a current source inverter 失效
标题翻译：使用电流源逆变器的臭氧发生器电源
公开(公告)号：US4752866A
公开(公告)日：1988-06-21
申请号：US12983
申请日：1987-02-10
申请人： Anh N. Huynh , Phoivos D. Ziogas
发明人： Anh N. Huynh , Phoivos D. Ziogas
IPC分类号： H02M3/156 , H02M5/45 , H02M7/521
CPC分类号： H02M5/45 , H02M3/1563
摘要： A versatile current source inverter power supply for an ozonator in which a gating control circuit controls the gating of a thyristor bridge inverter power supply in a manner in which the output current to the ozonator is controlled and regulated. The current source inverter power supply circuit includes a DC/AC thyristor bridge inverter circuit coupled at its input terminals to a direct current power source and at its output terminals to an electrical network which includes the capacitative ozonator load. The thyristor bridge inverter includes a first pair of thyristors and diodes coupled to conduct current in a first direction through the electrical network, and a second pair of thyristors and diodes coupled to conduct current in a second, opposite direction through the electrical network. The electrical network includes a step up high voltage transformer, with its primary winding coupled to the thyristor bridge inverter and its secondary winding coupled to the ozonator load. First and second commutating capacitors are connected across the first and second pairs of thyristors for commutating off the thyristors. An adjustable current pulse amplitude conrol circuit is provided for controlling the amplitude of current pulses supplied through the thyristor bridge to the ozonator load.
摘要翻译：一种用于臭氧发生器的通用电流源逆变器电源，其中门控控制电路以控制和调节对臭氧发生器的输出电流的方式控制晶闸管桥式逆变器电源的选通。电流源逆变器电源电路包括DC / AC晶闸管桥式逆变器电路，其在其输入端耦合到直流电源，并在其输出端耦合到包括电容臭氧发生器负载的电网。晶闸管桥式逆变器包括第一对晶闸管和二极管，其耦合以通过电网在第一方向上传导电流，以及第二对晶闸管和二极管，其耦合以通过电网在第二相反方向传导电流。电网包括升压高压变压器，其初级绕组耦合到晶闸管桥式逆变器及其与臭氧发生器负载耦合的次级绕组。第一和第二换向电容器跨越第一和第二对晶闸管连接，用于使晶闸管换向。提供可调电流脉冲幅度控制电路，用于控制通过晶闸管桥供给到臭氧发生器负载的电流脉冲的幅度。

7. 发明授权

US4713479A Synthesis of high-purity dialkyl 2-vinylcyclopropane-1,1-dicarboxylate 失效
标题翻译：高纯度2-乙烯基环丙烷-1,1-二羧酸二烷基酯的合成
公开(公告)号：US4713479A
公开(公告)日：1987-12-15
申请号：US936004
申请日：1986-11-28
申请人： Clarence E. Clark, Jr. , Richard G. Fayter, Jr.
发明人： Clarence E. Clark, Jr. , Richard G. Fayter, Jr.
IPC分类号： C07C69/743
CPC分类号： C07C69/743
摘要： This invention relates to a two-step synthesis of high purity dialkyl 2-vinyl-cyclopropane-1,1-dicarboxylate in which a mixture of trans- and cis-1,4-dihalobutene-2 is first isomerized to essentially trans-1,4-dihalobutene-2 followed immediately by cyclocondensing the resultant trans-1,4-dihalobutene-2 with a malonic ester in the presence of an alcoholic solution of a metallic alkoxide.
摘要翻译：本发明涉及高纯度2-乙烯基 - 环丙烷-1,1-二羧酸二烷基酯的两步合成，其中反式 - 顺式-1,4-二卤丁烯-2的混合物首先被异构化为基本上反式-1，然后在金属醇盐的醇溶液存在下，立即将所得的反式1,4-二卤丁烷-2与丙二酸酯环化缩合。

8. 发明授权

US4709058A Process for the production of macrocyclic esters by the depolymerization of polyesters 失效
标题翻译：通过聚酯解聚制备大环酯的方法
公开(公告)号：US4709058A
公开(公告)日：1987-11-24
申请号：US909760
申请日：1986-09-19
申请人： Joseph Cahill, Jr. , Herbert G. Rodenberg
发明人： Joseph Cahill, Jr. , Herbert G. Rodenberg
IPC分类号： C07D321/00 , A61K8/00 , A61K8/37 , A61K8/49 , A61K8/85 , A61Q5/00 , A61Q11/00 , A61Q13/00 , B01J31/22 , C07B61/00 , C07D313/00 , C07D323/00 , C07D325/00 , C07D327/00 , C08G63/88 , C11B9/00 , C07D327/02
CPC分类号： C07D327/00 , C07D313/00 , C07D323/00 , C08G63/88 , C11B9/0084
摘要： The catalytic thermal depolymerization of polyesters to produce macrocyclic esters suitable for fragrance applications is carried out using an olefin polymer. High yields of the corresponding macrocyclic ester are produced at high rates while substantially eliminating reactor fouling and the formation of undesirable by-products. The depolymerization is most advantageously conducted using polyethylene.
摘要翻译：使用烯烃聚合物进行聚酯催化热解聚以产生适用于香料应用的大环酯。相应的大环酯的高产率以高速率生产，同时基本上消除了反应器结垢和形成不合需要的副产物。解聚最有利地使用聚乙烯进行。

9. 发明授权

US4698383A Liquid copolyester plasticizers derived from 1,4-butanediol and a dicarboxylic acid mixture 失效
标题翻译：衍生自1,4-丁二醇和二羧酸混合物的液体共聚酯增塑剂
公开(公告)号：US4698383A
公开(公告)日：1987-10-06
申请号：US23319
申请日：1987-03-09
申请人： William J. Mertz , William L. O'Brien
发明人： William J. Mertz , William L. O'Brien
IPC分类号： C07C69/42
CPC分类号： C07C69/42
摘要： Liquid copolyesters useful as plasticizers for vinyl resins are provided. The copolyesters are obtained by the esterification of specific aliphatic dicarboxylic acid ester mixtures with 1,4-butanediol and an aliphatic saturated monofunctional alcohol. The copolyesters have acceptably low solidification points; they are resistant to hydrocarbon extraction; and they impart good low-temperature flexibility to PVC compositions plasticized therewith.
摘要翻译：提供用作乙烯基树脂增塑剂的液体共聚酯。共聚酯通过特殊脂族二羧酸酯与1,4-丁二醇和脂族饱和单官能醇的酯化而得到。共聚酯具有可接受的低凝固点; 它们耐烃萃取; 并赋予其增塑的PVC组合物良好的低温柔韧性。

10. 发明授权

US4682947A Decorative candles 失效
标题翻译：装饰蜡烛
公开(公告)号：US4682947A
公开(公告)日：1987-07-28
申请号：US893423
申请日：1986-08-05
申请人： Clement H. Luken, Jr. , Donald V. Kinsman
发明人： Clement H. Luken, Jr. , Donald V. Kinsman
IPC分类号： C11C5/00 , F21S13/00 , F23D3/16
CPC分类号： C11C5/002 , F21S13/00
摘要： Pillar candles which upon burning develop a decorative, aesthetically pleasing, free-standing shell having a filigree or lace-like pattern are provided. The candles consist of a fatty acid fuel composition, predominantly stearic acid and palmitic acid, and a 27-45 ply flat cotton wick. To obtain the desired decorative effect, the ratio of wick size to candle diameter is maintained at 12 to 19 plies per inch.
摘要翻译：提供燃烧时的柱状蜡烛形成具有花丝状或花边状图案的装饰性，美学上令人满意的独立外壳。蜡烛由脂肪酸燃料组合物，主要是硬脂酸和棕榈酸组成，以及一个27-45层平坦棉芯。为了获得所需的装饰效果，芯尺寸与蜡烛直径的比值保持在每英寸12至19层。

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