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1. 发明申请

US20120136177A1 Process for Preparation of Hexafluoroacetone Monohydrate 审中-公开
标题翻译：六氟丙酮一水合物的制备方法
公开(公告)号：US20120136177A1
公开(公告)日：2012-05-31
申请号：US13384736
申请日：2010-07-30
申请人： Yutaka Katsuhara , Tatsuya Hayasaka , Mineo Watanabe , Takashi Kume
发明人： Yutaka Katsuhara , Tatsuya Hayasaka , Mineo Watanabe , Takashi Kume
IPC分类号： C07C29/82
CPC分类号： C07C29/82 , C07C31/42
摘要： Disclosed is a method for producing hexafluoroacetone monohydrate by (1) allowing, in an organic solvent, hexafluoroacetone to be absorbed into water or a hexafluoroacetone hydrate (water addition method) or by (2) an easy method in which a hexafluoroacetone hydrate is mixed with an organic solvent and then distillation is conducted, thereby removing a mixture of water and the organic solvent as a low-boiling-point composition and obtaining a mixture of hexafluoroacetone monohydrate and the organic solvent as a high-boiling-point composition (dehydration method).
摘要翻译：公开了通过（1）在有机溶剂中将六氟丙酮吸收到水中或六氟丙酮水合物（水添加方法）中或通过（2）将六氟丙酮水合物与然后进行蒸馏，除去作为低沸点组合物的水和有机溶剂的混合物，得到作为高沸点组合物的六氟丙酮一水合物和有机溶剂的混合物（脱水法）。

2. 发明授权

US08822588B2 Fluorine-containing polymer and anti-static agent wherein same is used 有权
标题翻译：含氟聚合物和防静电剂，其中使用相同的
公开(公告)号：US08822588B2
公开(公告)日：2014-09-02
申请号：US12992035
申请日：2009-06-10
申请人： Yoshiharu Terui , Haruhiko Komoriya , Susumu Inoue , Takashi Kume
发明人： Yoshiharu Terui , Haruhiko Komoriya , Susumu Inoue , Takashi Kume
IPC分类号： C08F20/28
CPC分类号： C09K3/16 , C08F20/24 , C08F20/38 , C08F212/14 , C08F220/38 , C08L33/16 , Y10T428/3154 , Y10T428/31649
摘要： A fluorine-containing polymer has a repeating unit of the general formula (2) and is produced by homopolymerization or copolymerization with another polymerizable double bond-containing monomer. In general formula (2), W represents a linking group; R1 each independently represents a perfluoroalkyl group; Q represents a unit structure formed by cleavage of a double bond of a polymerizable double bond-containing group; and M+ represents a hydrogen cation, a metal ion or a quaternary ammonium ion.
摘要翻译：含氟聚合物具有通式（2）的重复单元，并且通过与另一种可聚合双键的单体均聚或共聚制备。在通式（2）中，W表示连接基团; R1各自独立地表示全氟烷基; Q表示通过裂解含可聚合双键的双键的双键形成的单元结构; M +表示氢阳离子，金属离子或季铵离子。

3. 发明申请

US20110065857A1 Fluorine-Containing Polymer and Anti-Static Agent Wherein Same is Used 有权
标题翻译：含氟聚合物和防静电剂，其中使用相同的
公开(公告)号：US20110065857A1
公开(公告)日：2011-03-17
申请号：US12992035
申请日：2009-06-10
申请人： Yoshiharu Terui , Haruhiko Komoriya , Susumu Inoue , Takashi Kume
发明人： Yoshiharu Terui , Haruhiko Komoriya , Susumu Inoue , Takashi Kume
IPC分类号： C08L27/12 , C08F14/18
CPC分类号： C09K3/16 , C08F20/24 , C08F20/38 , C08F212/14 , C08F220/38 , C08L33/16 , Y10T428/3154 , Y10T428/31649
摘要： There is provided a fluorine-containing polymer having a repeating unit of the general formula (2) and produced by homopolymerization or copolymerization with an other polymerizable double bond-containing monomer. In the formula, W represents a linking group; R1 each independently represents a perfluoroalkyl group; Q represents a unit structure formed by cleavage of a double bond of a polymerizable double bond-containing group; and M+ represents a hydrogen cation, a metal ion or a quaternary ammonium ion.There is also provided an antistatic agent using the above fluorine-containing polymer such that the antistatic agent can impart antistatic performance to an article stably over a long time and show excellent transparency.
摘要翻译：提供具有通式（2）的重复单元并通过与其它可聚合双键的单体均聚或共聚制备的含氟聚合物。在该式中，W表示连接基团; R1各自独立地表示全氟烷基; Q表示通过裂解含可聚合双键的双键的双键形成的单元结构; M +表示氢阳离子，金属离子或季铵离子。还提供了使用上述含氟聚合物的抗静电剂，使得抗静电剂能够长时间稳定地赋予制品抗静电性能并且显示出优异的透明性。

4. 发明申请

US20100022803A1 Method for Producing Tris(Perfluoroalkanesulfonyl)Methide Acid Salt 有权
标题翻译：生产三（全氟烷基磺酰基）甲酸盐的方法
公开(公告)号：US20100022803A1
公开(公告)日：2010-01-28
申请号：US12520178
申请日：2007-12-18
申请人： Tsutomu Nanmyo , Shintaro Sasaki , Takashi Kume
发明人： Tsutomu Nanmyo , Shintaro Sasaki , Takashi Kume
IPC分类号： C07C315/00
CPC分类号： C07C315/00 , C07C315/04 , C07F3/02 , C07C317/04
摘要： There is provided a method for producing a tris(perfluoroalkanesulfonyl)methide acid salt represented by formula [1], including the steps of (a) reacting a methylmagnesium halide represented by formula [2] with a perfluoroalkanesulfonyl fluoride represented by formula [3], thereby obtaining a reaction mixture; and (b) directly reacting the obtained reaction mixture with at least one selected from the group consisting of alkali metal halides, quaternary ammonium salts, and quaternary phosphonium salts. By this method, it is possible to easily produce the target methide acid salt with high yield.
摘要翻译：提供了一种由式[1]表示的三（全氟烷基磺酰基）甲基化物酸盐的制备方法，其包括以下步骤：（a）使式[2]表示的甲基卤化镁与式[3]表示的全氟烷基磺酰氟反应，从而得到反应混合物; 和（b）使所得反应混合物与选自碱金属卤化物，季铵盐和季鏻盐中的至少一种直接反应。通过该方法，可以容易地以高产率制备目标甲基化酸盐。

5. 发明授权

US5801122A N-phenyltetrahydrophthalamic acid derivatives, methods of producing same, and herbicides containing same as effective components 失效
标题翻译： N-苯基四氢酞酸衍生物，其制造方法，以及含有与有效成分相同的除草剂
公开(公告)号：US5801122A
公开(公告)日：1998-09-01
申请号：US676148
申请日：1996-07-15
申请人： Tetsuo Takematsu , Takeo Komata , Takashi Kume , Yumiko Kohda , Kiyoshi Suzuki , Matsue Kawamura , Yukio Ikeda , Kaoru Mori
发明人： Tetsuo Takematsu , Takeo Komata , Takashi Kume , Yumiko Kohda , Kiyoshi Suzuki , Matsue Kawamura , Yukio Ikeda , Kaoru Mori
IPC分类号： A01N37/26 , A01N39/00 , A01N43/10 , A01N43/40 , C07C323/52 , C07D213/82 , C07D333/38 , A01N43/36 , C07C321/00 , C07D333/22
CPC分类号： C07D213/82 , A01N37/26 , A01N39/00 , A01N43/10 , A01N43/40 , C07C323/52 , C07D333/38 , C07C2101/16
摘要： The invention provides N-phenyltetrahydrophthalamic acid derivatives represented by the general formula �I!, methods of producing the same, herbicides containing the same as the effective components, imidoylchloride derivatives as the intermediate products and methods of producing the same, ##STR1## wherein X and Y each individually represent hydrogen atoms or halogen atoms, R.sup.1 represents a lower alkoxycarbonylalkylthio group, R.sup.2 represents a lower alkyl group, a halogenated lower alkyl group or a substituted or unsubstituted phenyl group, and R.sup.3 represents a lower alkoxy group, a lower alkenyloxy group, a lower alkynyloxy group, or a lower alkoxyalkoxy group. The herbicides of the present invention, which are very useful, can be widely applied to upland, paddy field, orchard, turf, forest, non-crop land, etc., and are not harmful to crops.
摘要翻译： PCT No.PCT / JP95 / 00044 Sec。 371日期：1996年7月15日 102（e）日期1996年7月15日PCT提交1995年1月19日PCT公布。第WO95 / 19962号公报日期1995年7月27日本发明提供由通式[I]表示的N-苯基四氢酞酸衍生物，其制备方法，含有与有效成分相同的除草剂，作为中间产物的亚氨基氯衍生物及其制备方法，表示氢原子或卤素原子，R1表示低级烷氧基羰基烷硫基，R2表示低级烷基，卤代低级烷基或取代或未取代的苯基，R3表示低级烷氧基，低级链烯氧基，低级炔氧基基团或低级烷氧基烷氧基。本发明的除草剂非常有用，可广泛应用于旱地，水田，果园，草坪，森林，非作物地等，对作物无害。

6. 发明申请

US20090200719A1 Fluid-filled cylindrical vibration-damping device 有权
标题翻译：流体填充圆柱形减振装置
公开(公告)号：US20090200719A1
公开(公告)日：2009-08-13
申请号：US12320925
申请日：2009-02-09
申请人： Kazuhiko Kato , Takashi Kume
发明人： Kazuhiko Kato , Takashi Kume
IPC分类号： F16F13/00
CPC分类号： F16F13/1427
摘要： A fluid filled cylindrical vibration damping device having a main rubber elastic body elastically connecting an inner shaft member and an intermediate cylindrical member, wherein base wall portions of either of a pair of pocket portions are constituted by the main rubber elastic body to actively rise opposing positive/negative pressure fluctuations in a pair of fluid chambers at times of vibration input across the inner shaft member and the outer cylindrical member; a low-frequency orifice passage and a high-frequency orifice passage are provided; and the high-frequency orifice passage is provided in an aperture section thereof leading to at least one of the pair of fluid chambers with a moveable film adapted to limit fluid flow through the high-frequency orifice passage on the basis of displacement and/or deformation thereof.
摘要翻译：一种流体填充的圆柱形减振装置，其具有弹性地连接内轴构件和中间圆筒构件的主橡胶弹性体，其中一对凹部中的任一个的基壁部分由主橡胶弹性体构成，以主动地增加相对的正在穿过内轴构件和外圆柱形构件的振动输入时一对流体室中的负压波动; 提供低频孔通道和高频孔通道; 并且高频孔通道设置在其开口部分中，其通过可移动膜导向至少一个流体室，该可移动膜适于基于位移和/或变形来限制流过高频孔通道的流体其中。

7. 发明授权

US06943271B2 Process for producing fluorine-containing, polymerizable styrene monomer and intermediates used in same 有权
标题翻译：制备含氟聚合性苯乙烯单体的方法及其中使用的中间体
公开(公告)号：US06943271B2
公开(公告)日：2005-09-13
申请号：US10600510
申请日：2003-06-23
申请人： Shinichi Sumida , Takashi Kume , Sunao Koga , Haruhiko Komoriya
发明人： Shinichi Sumida , Takashi Kume , Sunao Koga , Haruhiko Komoriya
IPC分类号： C07C29/58 , C07B61/00 , C07C29/00 , C07C29/17 , C07C33/30 , C07F7/08 , C07C41/08 , C07F7/02
CPC分类号： C07C29/00 , C07C29/17 , C07F7/081 , C07C33/483
摘要： A fluorine-containing styrene monomer of the formula (2) is produced by a first, second or third process. The first process includes (a) reacting a compound of the formula (1) with a compound of the formula (3), in the presence of a metal catalyst; (b) reacting the product of the step (a) with a base; and (c) reacting the product of the step (b) with hydrogen, in the presence of a metal catalyst and a phosphine or amine, thereby producing the target styrene monomer. The second process includes reacting a compound of the formula (1) with a compound of the formula (12), in the presence of a metal catalyst, thereby producing the target styrene monomer. The third process includes reacting a compound of the formula (13) with a compound of the formula (14) or (15), in the presence of a base, thereby producing the target styrene monomer.
摘要翻译：通过第一，第二或第三工艺制备式（2）的含氟苯乙烯单体。第一种方法包括（a）在金属催化剂存在下使式（1）化合物与式（3）化合物反应; （b）使步骤（a）的产物与碱反应; 和（c）在金属催化剂和膦或胺的存在下，使步骤（b）的产物与氢反应，由此制备目标苯乙烯单体。第二种方法包括在金属催化剂的存在下使式（1）的化合物与式（12）的化合物反应，由此制备目标苯乙烯单体。第三种方法包括在碱的存在下使式（13）的化合物与式（14）或（15）的化合物反应，由此制备目标苯乙烯单体。

8. 发明授权

US06362372B1 Process for producing trifluoromethylbenzylamines 有权
公开(公告)号：US06362372B1
公开(公告)日：2002-03-26
申请号：US09833210
申请日：2001-04-12
申请人： Satoru Narizuka , Takashi Kume
发明人： Satoru Narizuka , Takashi Kume
IPC分类号： C07C20900
摘要： The invention relates to a process for producing a trifluoromethylbenzylamine represented by the following general formula (1), where each R independently represents a halogen selected from the group consisting of fluorine, chlorine, bromine and iodine, an alkyl group having a carbon atom number of 1-4, an alkoxy group having a carbon atom number of 1-4, an amino group, a hydroxyl group or a trifluoromethyl group, and n represents an integer from 0 to 4. The process includes hydrogenating a trifluoromethylbenzonitrile by hydrogen in an organic solvent in the presence of ammonia and a catalyst containing a platinum group element. This trifluoromethylbenzonitrile is represented by the following general formula (2), where R and n are defined as above. With this process, it is possible to obtain the trifluoromethylbenzylamine at an extremely high yield.

9. 发明授权

US5510317A N-acyl-N-phenylmaleamic acid derivatives, methods of producing same, and herbicides containing same as effective components 失效
标题翻译： N-酰基-N-苯基马来酰胺酸衍生物，其制备方法，以及含有与有效成分相同的除草剂
公开(公告)号：US5510317A
公开(公告)日：1996-04-23
申请号：US256683
申请日：1994-07-20
申请人： Tetsuo Takematsu , Takashi Kume , Takeo Komata , Kiyoshi Suzuki , Yukio Ikeda , Matsue Kawamura , Kaoru Mori
发明人： Tetsuo Takematsu , Takashi Kume , Takeo Komata , Kiyoshi Suzuki , Yukio Ikeda , Matsue Kawamura , Kaoru Mori
IPC分类号： A01N37/30 , C07C231/08 , C07C231/10 , C07C231/12 , C07C233/91 , C07C233/92 , C07C235/88 , A01N27/00 , A01N29/04 , A01N29/10 , C07C229/36
CPC分类号： C07C233/92 , A01N37/30 , C07C233/91
摘要： The invention provides N-acyl-N-phenylmaleamic acid derivatives represented by the general formula I!, a method of producing the same, and a herbicide containing the same as the effective components, ##STR1## wherein X and Y each individually represent hydrogen atoms or halogen atoms, R.sup.1 represents a hydrogen atom, a halogen atom, a lower alkyl group, a lower alkenyl group, a lower alkynyl group, a lower alkoxyalkyl group or a lower alkoxycarbonylalkyl group, R.sup.2 represents a lower alkyl group, a halogenated lower alkyl group or a substituted or unsubstituted phenyl group, R.sup.3 represents a hydrogen atom or a lower alkyl group, and R.sup.4 represents a hydroxyl, a lower alkoxy group, a lower alkenyloxy group, a lower alkynyloxy group, a lower alkoxyalkoxy group, a benzyloxy group or a lower alkoxycarbonylalkoxy group. This herbicide which is very useful can be widely applied to upland, paddy field, orchard, turf, forest, non-crop land, etc., and is not harmful to crops.
摘要翻译： PCT No.PCT / JP93 / 01755 Sec。 371日期：1994年7月20日 102（e）日期1994年7月20日PCT 1993年12月2日PCT公布。 WO94 / 12468 PCT出版物日期：1994年6月9日本发明提供由通式[I]表示的N-酰基-N-苯基马来酰胺酸衍生物，其制备方法和含有与有效成分相同的除草剂， I]其中X和Y各自独立地表示氢原子或卤原子，R1表示氢原子，卤素原子，低级烷基，低级烯基，低级炔基，低级烷氧基烷基或低级烷氧基羰基烷基， R2表示低级烷基，卤代低级烷基或取代或未取代的苯基，R3表示氢原子或低级烷基，R4表示羟基，低级烷氧基，低级链烯氧基，低级炔氧基低级烷氧基烷氧基，苄氧基或低级烷氧羰基烷氧基。这种非常有用的除草剂可广泛应用于旱地，水田，果园，草坪，森林，非作物地等，对作物无害。

10. 发明授权

US08304580B2 Method for producing tris(perfluoroalkanesulfonyl)methide acid salt 有权
标题翻译：三（全氟烷基磺酰基）甲基化物酸盐的制备方法
公开(公告)号：US08304580B2
公开(公告)日：2012-11-06
申请号：US12520178
申请日：2007-12-18
申请人： Tsutomu Nanmyo , Shintaro Sasaki , Takashi Kume
发明人： Tsutomu Nanmyo , Shintaro Sasaki , Takashi Kume
IPC分类号： C07C315/00
CPC分类号： C07C315/00 , C07C315/04 , C07F3/02 , C07C317/04
摘要： There is provided a method for producing a tris(perfluoroalkanesulfonyl)methide acid salt represented by formula [1], including the steps of (a) reacting a methylmagnesium halide represented by formula [2] with a perfluoroalkanesulfonyl fluoride represented by formula [3], thereby obtaining a reaction mixture; and (b) directly reacting the obtained reaction mixture with at least one selected from the group consisting of alkali metal halides, quaternary ammonium salts, and quaternary phosphonium salts. By this method, it is possible to easily produce the target methide acid salt with high yield.
摘要翻译：提供了一种由式[1]表示的三（全氟烷基磺酰基）甲基化物酸盐的制备方法，其包括以下步骤：（a）使式[2]表示的甲基卤化镁与式[3]表示的全氟烷基磺酰氟反应，从而得到反应混合物; 和（b）使所得反应混合物与选自碱金属卤化物，季铵盐和季鏻盐中的至少一种直接反应。通过该方法，可以容易地以高产率制备目标甲基化酸盐。

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