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1. 发明授权

US4770691A 2-(4',6'-di-substituted pyrimidine-2'-yl)oxy- or thio-benzoic acid 失效
标题翻译： 2-（4'，6'-二取代的嘧啶-2'-基）氧基或硫代苯甲酸
公开(公告)号：US4770691A
公开(公告)日：1988-09-13
申请号：US918925
申请日：1986-10-15
申请人： Yukio Nezu , Kazuhiko Sugiyama , Shoji Kusano , Yasufumi Toyokawa , Takeshige Miyazawa , Ikuo Kajiwara
发明人： Yukio Nezu , Kazuhiko Sugiyama , Shoji Kusano , Yasufumi Toyokawa , Takeshige Miyazawa , Ikuo Kajiwara
IPC分类号： A01N43/54 , C07D239/34 , C07D239/38 , C07D239/52 , C07D239/56 , C07D239/60 , C07D403/12 , C07D405/12 , C07D239/28
CPC分类号： C07D239/34 , A01N43/54 , C07D239/52 , C07D239/56 , C07D239/60 , C07D403/12 , C07D405/12
摘要： As new compounds are provided 2-(4',6'-di-substituted pyrimidine-2'-yl)oxy- or thio-benzoic acid derivatives of the formula ##STR1## wherein R is hydrogen, hydroxy, alkoxy, alkenyloxy, alkylthio or other substituents, R.sup.1 and R.sup.2 are each a halo, alkyl, alkoxy or other substituents; and X is oxygen or sulfur atom. These new compounds are useful as herbicidal agent effective to inhibit the growth of annual weeds and also perennial weeds predominant in irrigated fields of aquatic rice plants and in plowed fields.
摘要翻译：当新化合物提供式（IMAGE）的2-（4'，6'-二取代嘧啶-2'-基）氧基或硫代苯甲酸衍生物时，其中R是氢，羟基，烷氧基，烯氧基，烷硫基或其它取代基，R 1和R 2各自为卤素，烷基，烷氧基或其它取代基; X为氧或硫原子。这些新化合物可用作抑制一年生杂草生长的除草剂，以及主要在水稻和灌溉田中灌溉的多年生杂草。

2. 发明授权

US4871751A 1,2,6-Triphenyl-4(1H)-pyridinone derivatives, and their use as fungicides 失效
标题翻译： 1,2,6-三苯基-4（1H） - 吡啶酮衍生物及其作为杀真菌剂的用途
公开(公告)号：US4871751A
公开(公告)日：1989-10-03
申请号：US178421
申请日：1988-04-06
申请人： Norihisa Yonekura , Takashi Yumita , Yukio Nezu , Yoshiyuki Kojima , Shin-ichiro Maeno , Shigeharu Yaguchi
发明人： Norihisa Yonekura , Takashi Yumita , Yukio Nezu , Yoshiyuki Kojima , Shin-ichiro Maeno , Shigeharu Yaguchi
IPC分类号： C07D213/69 , A01N43/40 , C07D213/68 , C07D213/70 , C07D213/80 , C07D213/85 , C07D405/04
CPC分类号： C07D213/70 , A01N43/40 , C07D213/68 , C07D405/04
摘要： New substituted derivatives of 1,2,6-triphenyl-4(1H)-pyridone are now provided, which are useful as fungicidal agent having practically valuable and improved fungicidal activities against a variety of phyto-pathogenic microorganisms, especially fungi and which show low toxicity to animals, including humans. These new compounds may be produced by different processes.

3. 发明授权

US5512551A Benzohydroxymoylazole derivatives and insecticide including the same 失效
标题翻译：苯并羟基肟基衍生物和杀虫剂包括相同
公开(公告)号：US5512551A
公开(公告)日：1996-04-30
申请号：US281039
申请日：1994-07-27
申请人： Keiji Toriyabe , Takayoshi Takehi , Yukio Nezu , Yuki Nakano , Tomonori Shimazu
发明人： Keiji Toriyabe , Takayoshi Takehi , Yukio Nezu , Yuki Nakano , Tomonori Shimazu
IPC分类号： A01N43/50 , A01N43/653 , C07D233/61 , C07D249/08 , C07D521/00 , C07F7/08 , C07F7/18 , C07F7/10
CPC分类号： C07D231/12 , A01N43/50 , A01N43/653 , C07D233/56 , C07D249/08 , C07F7/0812 , C07F7/1856
摘要： The present invention provides benzohydroximoylazole derivatives represented by the following novel formula: ##STR1## wherein R is a branched alkyl group having not fewer than 3 carbon atoms, a fluorine-substituted alkyl group having not fewer than 2 carbon atoms, a branched alkoxy group having not fewer than 3 carbon atoms, a halogen-substituted alkoxy group having not fewer than 3 carbon atoms, a cycloalkyl group, a cycloalkylmethyl group which may be substituted with one or two alkyl groups, a substituted silylalkyl group, a substituted silylalkyloxy group, a cycloalkyloxy group which may be substituted with one or two alkyl groups, an alkylthio group, a halogen-substituted alkyloxyalkyl group, an alkynyl group, or a halogen-substituted alkenyloxy group;X is a hydrogen atom, a chlorine atom, or a fluorine atom;Y is an alkyl group; and Z is a nitrogen atom or a methyne group,and methods for producing the same, insecticides including the benzohydroximoylazole derivatives as an active ingredient.
摘要翻译：本发明提供由以下新颖化学式表示的苯并羟肟基衍生物：其中R为不少于3个碳原子的支链烷基，具有不少于2个碳原子的氟取代烷基，支链烷氧基具有不少于3个碳原子，具有不少于3个碳原子的卤素取代的烷氧基，环烷基，可被一个或两个烷基取代的环烷基甲基，取代的甲硅烷基烷基，取代的甲硅烷基烷氧基，可以被一个或两个烷基取代的环烷氧基，烷硫基，卤素取代的烷氧基烷基，炔基或卤素取代的烯氧基; X是氢原子，氯原子或氟原子; Y为烷基; Z为氮原子或甲炔基，其制造方法为含有苯并羟基肟基衍生物的杀虫剂作为有效成分。

4. 发明授权

US4070377A Process for producing L-ascorbic acid-2-sulfate 失效
标题翻译：生产L-抗坏血酸-2-硫酸盐的方法
公开(公告)号：US4070377A
公开(公告)日：1978-01-24
申请号：US711409
申请日：1976-08-03
申请人： Eiichi Hayashi , Kiyoshi Takita , Hironari Sugiyama , Yukio Nezu
发明人： Eiichi Hayashi , Kiyoshi Takita , Hironari Sugiyama , Yukio Nezu
IPC分类号： C07D307/62 , C07D307/32
CPC分类号： C07D307/62
摘要： A process for producing a mono- or di-alkali metal salt or alkaline earth metal salt of L-ascorbic acid-2-sulfate which comprises reacting L-ascorbic acid in which the 5 and 6 positions are protected by a ketone or aldehyde, with dimethyl formamide-sulfur trioxide complex, and neutralizing the product with an alkali metal hydroxide or an alkaline earth metal hydroxide, and removing said protecting aldehyde or ketone at 5-and 6-positions.
摘要翻译：一种制备L-抗坏血酸-2-硫酸盐的单碱金属盐或二碱金属盐或碱土金属盐的方法，其包括将其中5和6位被酮或醛保护的L-抗坏血酸与二甲基甲酰胺 - 三氧化硫复合物，并用碱金属氢氧化物或碱土金属氢氧化物中和产物，并在5-和6-位除去所述保护醛或酮。

5. 发明授权

US5366988A Benzohydroximoylazole derivatives and insecticide including the same 失效
标题翻译：苯并羟基肟基衍生物和杀虫剂包括相同
公开(公告)号：US5366988A
公开(公告)日：1994-11-22
申请号：US915817
申请日：1992-07-28
申请人： Keiji Toriyabe , Takayoshi Takehi , Yukio Nezu , Yuki Nakano , Tomonori Shimazu
发明人： Keiji Toriyabe , Takayoshi Takehi , Yukio Nezu , Yuki Nakano , Tomonori Shimazu
IPC分类号： A01N43/50 , A01N43/653 , C07D233/61 , C07D249/08 , C07D521/00 , C07F7/08 , C07F7/18
CPC分类号： C07D231/12 , A01N43/50 , A01N43/653 , C07D233/56 , C07D249/08 , C07F7/0812 , C07F7/1856
摘要： The present invention provides benzohydroximoylazole derivatives represented by the following novel formula: ##STR1## wherein R is a branched alkyl group having not fewer than 5 carbon atoms, a fluorine-substituted alkyl group having not fewer than 2 carbon atoms, a branched alkoxy group having not fewer than 3 carbon atoms, a halogen-substituted alkoxy group having not fewer than 3 carbon atoms, a cycloalkyl group, a cycloalkylmethyl group which may be substituted with one or two alkyl groups, a substituted silylalkyl group, a substituted silylalkyloxy group, a cycloalkyloxy group which may be substituted with one or two alkyl groups, an alkylthio group, a halogen-substituted alkyloxyalkyl group, an alkynyl group, or a halogen-substituted alkenyloxy group;X is a hydrogen atom, a chlorine atom, or a fluorine atom;Y is an alkyl group; and Z is a nitrogen atom or a methyne group,and methods for producing the same, insecticides including the benzohydroximoylazole derivatives as an active ingredient.
摘要翻译： PCT No.PCT / JP91 / 01614 Sec。 371日期：1992年7月28日 102（e）日期1992年7月28日PCT 1991年11月25日PCT PCT。第WO92 / 09581号公报日本公开日1992年6月11日。本发明提供由以下新颖化学式表示的苯并氢吗啉衍生物：其中R为不少于5个碳原子的支链烷基，具有不少于2个碳的氟取代烷基原子，碳原子数3以上的支链烷氧基，碳原子数3以上的卤素取代烷氧基，环烷基，可被1或2个烷基取代的环烷基甲基，取代甲硅烷基烷基取代的甲硅烷基烷氧基，可被一个或两个烷基取代的环烷氧基，烷硫基，卤素取代的烷氧基烷基，炔基或卤素取代的烯氧基; X是氢原子，氯原子或氟原子; Y为烷基; Z为氮原子或甲炔基，其制造方法为含有苯并羟基肟基衍生物的杀虫剂作为有效成分。

6. 发明授权

US4757081A 1,2,6-triphenyl-4(1H)-pyridinone derivatives, and uses as fungicidal agents 失效
标题翻译： 1,2,6-三苯基-4（1H） - 吡啶酮衍生物，并用作杀真菌剂
公开(公告)号：US4757081A
公开(公告)日：1988-07-12
申请号：US29944
申请日：1987-03-26
申请人： Norihisa Yonekura , Takashi Yumita , Yukio Nezu , Yoshiyuki Kojima , Shin-ichiro Maeno , Shigeharu Yaguchi
发明人： Norihisa Yonekura , Takashi Yumita , Yukio Nezu , Yoshiyuki Kojima , Shin-ichiro Maeno , Shigeharu Yaguchi
IPC分类号： C07D213/69 , A01N43/40 , C07D213/68 , C07D213/70 , C07D213/80 , C07D213/85 , C07D405/04 , A61K31/44 , C07D213/62 , C07D213/63 , C07D401/04
CPC分类号： C07D213/70 , A01N43/40 , C07D213/68 , C07D405/04
摘要： New substituted derivatives of 1,2,6-triphenyl-4(1H)-pyridinone are now provided, which are useful as fungicidal agent having practically valuable and improved fungicidal activities against a variety of phyto-pathogenic microorganisms, especially fungi and which show low toxicity to animals, including humans. These new compounds may be produced by different processes.
摘要翻译：现在提供了1,2,6-三苯基-4（1H） - 吡啶酮的新取代的衍生物，它们可用作杀真菌剂，其对各种植物病原微生物，特别是真菌具有实际有价值和改善的杀真菌活性，并且显示低对动物，包括人类的毒性。这些新化合物可以通过不同的方法生产。

7. 发明授权

US4071534A Process for producing l-ascorbic acid-2-sulfate 失效
标题翻译：生产1-抗坏血酸-2-硫酸盐的方法
公开(公告)号：US4071534A
公开(公告)日：1978-01-31
申请号：US711410
申请日：1976-08-03
申请人： Eiichi Hayashi , Kiyoshi Takita , Hironari Sugiyama , Yukio Nezu
发明人： Eiichi Hayashi , Kiyoshi Takita , Hironari Sugiyama , Yukio Nezu
IPC分类号： C07D307/62
CPC分类号： C07D307/62
摘要： A process for producing a mono- or di-alkali metal salt or alkaline earth metal salt of L-ascorbic acid-2-sulfate which comprises reacting L-ascorbic acid in which the 5 and 6 positions are protected by a ketone or aldehyde, with dimethyl formamide-sulfur trioxide complex, which is produced by a reaction of dimethyl formamide with chlorosulfonic acid and a dehydrohalogenating agent such as pyridine, triethylamine, dimethyl aniline, which is a tertiary amine so as to produce a sulfate, and neutralizing the product with an alkali metal hydroxide or an alkaline earth metal hydroxide, and removing said protecting aldehyde or ketone at 5- and 6-positions.
摘要翻译：一种制备L-抗坏血酸-2-硫酸盐的单碱金属盐或二碱金属盐或碱土金属盐的方法，其包括将其中5和6位被酮或醛保护的L-抗坏血酸与二甲基甲酰胺 - 三氧化硫络合物，其通过二甲基甲酰胺与氯磺酸的反应和脱卤化氢剂如吡啶，三乙胺，二甲基苯胺（其是叔胺）反应生成硫酸盐，并用碱金属氢氧化物或碱土金属氢氧化物，并在5-和6-位除去所述保护醛或酮。

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