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    • 3. 发明授权
    • Method of producing R-Fe-B permanent magnet, and lubricant agent and release agent for use in shaping the same
    • 生产R-Fe-B永磁体的方法,以及用于成型R-Fe-B永磁体的润滑剂和脱模剂
    • US06361738B1
    • 2002-03-26
    • US09446334
    • 2000-03-28
    • Yuji KanekoJunichiro BabaKazuo TanakaShizuo Mori
    • Yuji KanekoJunichiro BabaKazuo TanakaShizuo Mori
    • B22F312
    • B22F1/0059H01F1/0577
    • The method of producing an R—Fe—B magnet of the present invention is characterized in that R—Fe—B alloy fine powder is molded in a magnetic field and sintered using a lubricant for molding magnets containing specific components, individually or as a mixture, of specific amounts of methyl caproate and/or methyl caprylate, which provide high crystal orientation, and lubricant comprising depolymerized polymer for improving molded article strength, or a lubricant for molding magnets wherein Ti coupling agent that improves crystal orientation is added to this lubricant for molding magnets. Each particle of the fine powder has a high degree of crystal orientation in the direction of the magnetic field, and molded article strength is markedly improved, leading to improved mass-productivity and yield. Moreover, the above-mentioned lubricants do not react with this magnet powder during sintering and are emitted as a gas. Therefore, binder removal performance is excellent and as a result, an increase in the amount of C remaining in the sintered compact is inhibited, to obtain an R—Fe—B permanent magnet with high Br and iHc properties.
    • 本发明的R-Fe-B磁体的制造方法的特征在于,R-Fe-B合金细粉末在磁场中成型,并使用用于成型含有特定成分的磁体的润滑剂单独或作为混合物 的特定量的提供高结晶取向的己酸甲酯和/或辛酸甲酯,以及包含用于提高成型体强度的解聚聚合物的润滑剂或用于成型磁体的润滑剂,其中将用于改善结晶取向的Ti偶联剂加入到该润滑剂中 成型磁铁。 细粉末的每个颗粒在磁场方向上具有高度的晶体取向,并且模制品强度显着提高,从而提高了批量生产率和产率。 此外,上述润滑剂在烧结期间不与该磁粉反应,作为气体排出。 因此,除去粘合剂的性能优异,因此抑制烧结体中剩余C量的增加,得到Br和iHc特性高的R-Fe-B永磁体。
    • 4. 发明授权
    • Rare-earth sintered magnet and method of producing the same
    • 稀土烧结磁体及其制造方法
    • US07048808B2
    • 2006-05-23
    • US09966743
    • 2001-10-01
    • Yuji KanekoKatsuya TaniguchiTakao Sekino
    • Yuji KanekoKatsuya TaniguchiTakao Sekino
    • H01F1/057
    • H01F1/058H01F1/0577
    • The present invention provides a rare-earth sintered magnet exhibiting desirable magnetic properties in which the amount of Nd and/or Pr forming a non-magnetic phase in a grain boundary phase is reduced. Specifically, the present invention provides a rare-earth sintered magnet having a composition of (R1x+R2y)T100-x-y-zQz where R1 is at least one element selected from the group consisting of all rare-earth elements excluding La (lanthanum), Y (yttrium) and Sc (scandium); R2 is at least one element selected from the group consisting of La, Y and Sc; T is at least one element selected from the group consisting of all transition elements; Q is at least one element selected from the group consisting of B and C, and including, as a main phase, a crystal grain of an Nd2Fe14B crystalline structure, wherein: molar fractions x, y and z satisfy 8≦x≦18 at %, 0.1≦y≦3.5 at % and 3≦z≦20 at %, respectively; and a concentration of R2 is higher in at least a part of a grain boundary phase than in the main phase crystal grains.
    • 本发明提供一种稀土烧结磁体,其具有期望的磁特性,其中在晶界相中形成非磁性相的Nd和/或Pr的量减少。 具体地说,本发明提供了一种稀土烧结磁体,其具有(R1→X2 + R2→Y)T100-xyZ < 其中R1是选自除La(镧),Y(钇)和Sc(钪)之外的所有稀土元素中的至少一种元素; R2是选自La,Y和Sc中的至少一种元素; T是选自由所有过渡元素组成的组中的至少一种元素; Q是选自B和C中的至少一种元素,并且包括作为主相的Nd 2 Fe 14 B晶体结构的晶粒 ,其中:摩尔分数x,y和z分别满足8≤x≤18at%,0.1≤y≤3.5at%和3≤z≤20at% 并且在晶界相的至少一部分中R2的浓度高于主相晶粒中的浓度。
    • 5. 发明授权
    • Rare earth magnet material and method for producing the same
    • 稀土磁铁材料及其制造方法
    • US09242296B2
    • 2016-01-26
    • US13384901
    • 2010-09-10
    • Yuji KanekoYukio Takada
    • Yuji KanekoYukio Takada
    • B22F3/12H01F1/057B22F1/00B22F3/24C22C33/02H01F41/02
    • B22F1/0088B22F3/24C22C33/0278H01F1/0577H01F41/0246H01F41/0293
    • A method for producing a rare earth magnet material which allows efficient Dy or the like diffusion into an inside thereof. This method includes a preparation step of preparing a powder mixture of magnet powder including one or more rare earth elements including neodymium, boron, and the remainder being iron; and neodymium fluoride powder; a heating step of heating a compact of the powder mixture and causing oxygen around magnet powder particles to react with the fluoride powder, thereby obtaining a lump rare earth magnet material in which neodymium oxyfluoride is wholly distributed. The fluoride powder traps oxygen enclosed in the powder mixture and fixes the oxygen as stable NdOF. When Dy is diffused into this rare earth magnet material, Dy smoothly enters into its inside without being oxidized at grain boundaries. Consequently, coercivity of the entire rare earth magnet material can be efficiently increased without wasting scarce Dy.
    • 一种稀土类磁铁材料的制造方法,其特征在于,能够有效地将Dy等扩散到内部。 该方法包括制备包括一种或多种稀土元素的磁粉的粉末混合物的制备步骤,所述稀土元素包括钕,硼,其余为铁; 和氟化钕粉末; 加热粉末混合物的粉末并使磁体粉末颗粒周围的氧与氟化物粉末反应的加热步骤,从而获得其中全氟分布有氟化钕的块状稀土磁体材料。 氟化物粉末将氧气封闭在粉末混合物中并固定氧气作为稳定的NdOF。 当Dy扩散到这种稀土磁体材料中时,Dy平滑地进入其内部而不在晶界处被氧化。 因此,可以有效地提高整个稀土磁体材料的矫顽力,而不会浪费稀少的Dy。
    • 8. 发明申请
    • Replication system having the capability to accept commands at a standby-system site before completion of updating thereof
    • 复制系统具有在完成更新之前在备用系统站点接受命令的能力
    • US20050289197A1
    • 2005-12-29
    • US11148411
    • 2005-06-09
    • Masaki KanJun-ichi YamatoYuji Kaneko
    • Masaki KanJun-ichi YamatoYuji Kaneko
    • G06F12/00
    • G06F11/2097G06F11/2023G06F11/2038G06F11/2048
    • A replication system rapidly switches from a normal-system site to a standby-system site in the event of a problem and reliably maintains functions, and moreover, reduces drops in performance. A first site provides system functions that accompany writing and reading of data. A relay transfer device receives update information from the first site, causes completion of processes for replication in the first site, and continuously executes processes for successively transferring the update information to a second site. The second site receives the update information of the first site and applies this update information to itself to retain a replica of the data of the first site. If, when executing a write request command or a read request command to provide at least a portion of the system functions, the second site has not yet retained the most recent data that are the target of the command, the second site acquires the necessary update information and then executes the command.
    • 在发生问题的情况下,复制系统可以从普通系统站点快速切换到备用系统站点,并可靠地维护功能,此外,降低性能下降。 第一个站点提供与数据的写入和读取相关的系统功能。 中继传送装置从第一站点接收更新信息,导致在第一站点进行复制处理,并连续执行将更新信息连续传送到第二站点的处理。 第二站点接收第一站点的更新信息,并将此更新信息应用于其自身以保留第一站点的数据的副本。 如果当执行写入请求命令或读取请求命令以提供系统功能的至少一部分时,第二站点尚未保留作为命令目标的最新数据,则第二站点获取必要的更新 信息,然后执行命令。
    • 9. 发明授权
    • Magnetic alloy powder for permanent magnet and method for producing the same
    • 用于永磁体的磁性合金粉末及其制造方法
    • US06818041B2
    • 2004-11-16
    • US09952056
    • 2001-09-14
    • Hiroyuki TomizawaYuji Kaneko
    • Hiroyuki TomizawaYuji Kaneko
    • B22F100
    • H01F1/0574H01F1/058
    • Magnetic alloy powder for a permanent magnet contains: R of about 20 mass percent to about 40 mass percent (R is Y, or at least one type of rare earth element); T of about 60 mass percent to about 79 mass percent (T is a transition metal including Fe as a primary component); and Q of about 0.5 mass percent to about 2.0 mass percent (Q is an element including B (boron) and C (carbon)). The magnetic alloy powder is formed by an atomize method, and the shape of particles of the powder is substantially spherical. The magnetic alloy powder includes a compound phase having Nd2Fe14B tetragonal structure as a primary composition phase. A ratio of a content of C to a total content of B and C is about 0.05 to about 0.90.
    • 用于永磁体的磁性合金粉末包含:R为约20质量%至约40质量%(R为Y或至少一种稀土元素); T为约60质量%至约79质量%(T为包含Fe为主要成分的过渡金属); 和Q为约0.5质量%至约2.0质量%(Q为包含B(硼)和C(碳)的元素)。 磁性合金粉末通过雾化法形成,粉末的形状基本上是球形的。 磁性合金粉末包括具有Nd 2 Fe 14 B四方晶系的化合物相作为主要组成相。 C与B和C的总含量之比为约0.05至约0.90。