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1. 发明授权

US08703294B2 Bioactive graded zirconia-based structures 有权
标题翻译：生物活性分级氧化锆基结构
公开(公告)号：US08703294B2
公开(公告)日：2014-04-22
申请号：US12284620
申请日：2008-09-22
申请人： Yu Zhang , Racquel Legeros , Jae-Won Kim
发明人： Yu Zhang , Racquel Legeros , Jae-Won Kim
IPC分类号： B32B17/06 , B32B15/00 , B32B9/00 , B32B19/00 , B05D1/36 , B05D3/00 , B05D3/02 , B05D1/18
CPC分类号： C04B41/5022 , A61L27/10 , A61L27/427 , C04B41/009 , C04B41/86 , C04B2111/00405 , C04B2111/00836 , C04B41/4539 , C04B41/4535 , C04B41/455 , C04B35/10 , C04B35/119 , C04B35/48 , C04B35/488
摘要： The present invention provides a functionally graded bioactive glass/ceramic composite structure or bioactive glass/ceramic/bioactive glass sandwich structure for use in such applications as damage resistant, ceramic dental implants, immediate tooth replacement, endodontic posts, orthopedic prostheses, orthopedic stems, bone substitutes, bone screws, plates, and anchors, nonunion defects repair, alveolar ridge augmentation, missing small bone parts (e.g. fingers, toes, etc), maxilla facial reconstruction, spinal fusion, and scaffolds for bone regeneration, comprising a residual bioactive glass or glass-ceramic layer at all accessible surfaces, followed by an underlying graded glass-ceramic layer, and then an dense interior ceramic. Further, the invention provides methods for making the same structure.
摘要翻译：本发明提供功能梯度的生物活性玻璃/陶瓷复合结构或生物活性玻璃/陶瓷/生物活性玻璃夹层结构，用于诸如耐损伤陶瓷牙科植入物，立即牙齿置换，牙髓根管，矫形假体，矫形骨，骨骼替代物，骨螺钉，板和锚，不连接缺陷修复，牙槽嵴隆起，缺少小骨部分（例如手指，脚趾等），上颌面部重建，脊柱融合和用于骨再生的支架，包括残留的生物活性玻璃或玻璃陶瓷层，随后是下层玻璃陶瓷层，然后是密集的内部陶瓷。此外，本发明提供了制造相同结构的方法。

2. 发明授权

US08951597B2 Graded glass/ceramic/glass structures for damage resistant ceramic dental and orthopedic prostheses 有权
标题翻译：分级玻璃/陶瓷/玻璃结构，用于耐磨陶瓷牙科和矫形假体
公开(公告)号：US08951597B2
公开(公告)日：2015-02-10
申请号：US12927137
申请日：2010-11-08
申请人： Yu Zhang , Jae-Won Kim , Van P. Thompson
发明人： Yu Zhang , Jae-Won Kim , Van P. Thompson
IPC分类号： A61L33/00 , A61C13/083 , C03C14/00
CPC分类号： A61C13/083 , C03C14/00
摘要： The present invention provides a functionally graded glass/ceramic/glass sandwich system especially useful in damage resistant, ceramic dental and orthopedic prosthesis. The functionally graded glass/substrate/glass composite structure comprises an outer (aesthetic) residual glass layer, a graded glass-ceramic layer, and a dense interior ceramic. The functionally graded glass/substrate/glass composite structure may further comprise a veneer on an exterior surface. The present invention also provides a method for preparing a functionally graded glass/ceramic/glass sandwich system. A powdered glass-ceramic composition or a glass tape is applied to the accessible surfaces of a dense alumina substrate to thereby substantially cover the substrate surfaces. The glass of the composition has a CTE similar to that of the substrate material. The glass-ceramic composition is infiltrated into the dense substrate by heating the assembly to temperatures 50-700° C. below the sintering temperature of the substrate.
摘要翻译：本发明提供了一种功能梯度的玻璃/陶瓷/玻璃夹层系统，特别适用于耐损伤陶瓷牙科和矫形假体。功能梯度的玻璃/基底/玻璃复合结构包括外部（美观的）残余玻璃层，梯度玻璃陶瓷层和致密的内部陶瓷。功能梯度的玻璃/基底/玻璃复合结构还可以在外表面上包括单板。本发明还提供了制备功能梯度玻璃/陶瓷/玻璃夹心系统的方法。将粉末状玻璃陶瓷组合物或玻璃带施加到致密氧化铝基板的可接近表面，从而基本上覆盖基板表面。组合物的玻璃具有与基材材料相似的CTE。通过将组件加热到低于衬底的烧结温度50-700℃的温度下，将玻璃 - 陶瓷组合物渗透到致密衬底中。

3. 发明申请

US20090118114A1 Bioactive graded zirconia-based structures 有权
标题翻译：生物活性分级氧化锆基结构
公开(公告)号：US20090118114A1
公开(公告)日：2009-05-07
申请号：US12284620
申请日：2008-09-22
申请人： Yu Zhang , Racquel Regeros , Jae-Won Kim
发明人： Yu Zhang , Racquel Regeros , Jae-Won Kim
IPC分类号： C04B35/053
CPC分类号： C04B41/5022 , A61L27/10 , A61L27/427 , C04B41/009 , C04B41/86 , C04B2111/00405 , C04B2111/00836 , C04B41/4539 , C04B41/4535 , C04B41/455 , C04B35/10 , C04B35/119 , C04B35/48 , C04B35/488
摘要： The present invention provides a functionally graded bioactive glass/ceramic composite structure or bioactive glass/ceramic/bioactive glass sandwich structure for use in such applications as damage resistant, ceramic dental implants, immediate tooth replacement, endodontic posts, orthopedic prostheses, orthopedic stems, bone substitutes, bone screws, plates, and anchors, nonunion fractures repair, alveolar ridge augmentation, missing small bone parts (e.g. fingers, toes, etc), maxilla facial reconstruction, spinal fusion, and scaffolds for bone regeneration, comprising a residual bioactive glass or glass-ceramic layer at all accessible surfaces, followed by an underlying graded glass-ceramic layer, and then an dense interior ceramic. The residual bioactive glass or glass-ceramic layer can be further transformed to a carbonate apatite (CHA) layer by immersing in calcifying solution or simulated body fluid (SBF) with electrolyte composition similar to that of serum. The interior ceramic preferably contains yttria-tetragonal zirconia polycrystal (Y-TZP) or ceria stabilized tetragonal zirconia polycrystal (Ce-TZP) or magnesia stabilized zirconia (Mg-PSZ) or calcia stabilized zirconia (Ca-PSZ) or alumina or zirconia-alumina composites. Further, the invention provides methods for making the same functionally graded bioactive glass/ceramic composite structure or graded bioactive glass/ceramic/bioactive glass sandwich structure.
摘要翻译：本发明提供功能梯度的生物活性玻璃/陶瓷复合结构或生物活性玻璃/陶瓷/生物活性玻璃夹层结构，用于诸如耐损伤陶瓷牙科植入物，立即牙齿置换，牙髓根管，矫形假体，矫形骨，骨骼替代物，骨螺钉，板和锚，不愈合骨折修复，牙槽嵴隆起，缺少小骨部分（例如手指，脚趾等），上颌面部重建，脊柱融合和用于骨再生的支架，包括残留生物活性玻璃或玻璃陶瓷层，随后是下层玻璃陶瓷层，然后是密集的内部陶瓷。残留的生物活性玻璃或玻璃陶瓷层可以通过浸入含钙血浆或模拟体液（SBF）的电解质组成与血清类似的碳酸钙磷灰石（CHA）层。内部陶瓷优选含有氧化钇 - 四方晶氧化锆多晶（Y-TZP）或二氧化铈稳定的四方晶氧化锆多晶（Ce-TZP）或氧化镁稳定的氧化锆（Mg-PSZ）或氧化钙稳定的氧化锆（Ca-PSZ）或氧化铝或氧化锆 - 氧化铝复合材料。此外，本发明提供了制造相同功能梯度生物活性玻璃/陶瓷复合结构或分级生物活性玻璃/陶瓷/生物活性玻璃夹心结构的方法。

4. 发明申请

US20110123956A1 Graded glass/ceramic/glass structures for damage resistant ceramic dental and orthopedic prostheses 有权
标题翻译：分级玻璃/陶瓷/玻璃结构，用于耐磨陶瓷牙科和矫形假体
公开(公告)号：US20110123956A1
公开(公告)日：2011-05-26
申请号：US12927137
申请日：2010-11-08
申请人： Yu Zhang , Jae-Won Kim , Van P. Thompson
发明人： Yu Zhang , Jae-Won Kim , Van P. Thompson
IPC分类号： A61C13/08 , B32B17/06 , A61L27/30
CPC分类号： A61C13/083 , C03C14/00
摘要： The present invention provides a functionally graded glass/ceramic/glass sandwich system especially useful in damage resistant, ceramic dental and orthopedic prosthesis. The functionally graded glass/substrate/glass composite structure comprises an outer (aesthetic) residual glass layer, a graded glass-ceramic layer, and a dense interior ceramic. The functionally graded glass/substrate/glass composite structure may further comprise a veneer on an exterior surface. The present invention also provides a method for preparing a functionally graded glass/ceramic/glass sandwich system. A powdered glass-ceramic composition or a glass tape is applied to the accessible surfaces of a dense alumina substrate to thereby substantially cover the substrate surfaces. The glass of the composition has a CTE similar to that of the substrate material. The glass-ceramic composition is infiltrated into the dense substrate by heating the assembly to temperatures 50-700° C. below the sintering temperature of the substrate.
摘要翻译：本发明提供了一种功能梯度的玻璃/陶瓷/玻璃夹层系统，特别适用于耐损伤陶瓷牙科和矫形假体。功能梯度的玻璃/基底/玻璃复合结构包括外部（美观的）残余玻璃层，梯度玻璃陶瓷层和致密的内部陶瓷。功能梯度的玻璃/基底/玻璃复合结构还可以在外表面上包括单板。本发明还提供了制备功能梯度玻璃/陶瓷/玻璃夹心系统的方法。将粉末状玻璃陶瓷组合物或玻璃带施加到致密氧化铝基板的可接近表面，从而基本上覆盖基板表面。组合物的玻璃具有与基材材料相似的CTE。通过将组件加热到低于衬底的烧结温度50-700℃的温度下，将玻璃 - 陶瓷组合物渗透到致密衬底中。

5. 发明授权

US07871706B2 Graded glass/zirconia/glass structures for damage resistant ceramic dental and orthopedic prostheses 有权
标题翻译：分级玻璃/氧化锆/玻璃结构，用于耐磨陶瓷牙科和矫形假体
公开(公告)号：US07871706B2
公开(公告)日：2011-01-18
申请号：US11983815
申请日：2007-11-09
申请人： Yu Zhang , Jae-Won Kim
发明人： Yu Zhang , Jae-Won Kim
IPC分类号： B32B17/06
CPC分类号： C04B35/486 , B82Y30/00 , C04B41/009 , C04B41/5023 , C04B41/86 , C04B2111/00405 , C04B2111/00836 , C04B2235/3217 , C04B2235/3225 , C04B2235/5409 , C04B2235/5454 , C04B41/4539 , C04B35/48
摘要： The present invention provides a functionally graded glass/ceramic/glass sandwich system for use in damage resistant, ceramic and orthopedic prosthesis. The functionally graded glass/substrate/glass composite structure comprises an outer residual glass layer, a graded glass-ceramic layer, and a dense interior ceramic. The functionally graded glass/substrate/glass composite structure may further comprise a veneer on an exterior surface.The present invention also provides a method for preparing a functionally graded glass/ceramic/glass sandwich system. A powdered glass-ceramic composition is applied to the accessible surfaces of a presintered zirconia substrate to thereby substantially cover the substrate surfaces. The glass of the composition has a CTE similar to that of the substrate material. The glass-ceramic composition is infiltrated into and densifies the substrate by heating the assembly to at least the sintering temperature of the substrate.
摘要翻译：本发明提供了一种功能梯度玻璃/陶瓷/玻璃夹层系统，用于耐损伤，陶瓷和矫形假体。功能梯度的玻璃/衬底/玻璃复合结构包括外残留玻璃层，梯度玻璃陶瓷层和致密内部陶瓷。功能梯度的玻璃/基底/玻璃复合结构还可以在外表面上包括单板。本发明还提供了制备功能梯度玻璃/陶瓷/玻璃夹心系统的方法。将粉末状的玻璃 - 陶瓷组合物施加到预烧结的氧化锆衬底的可接近表面上，从而基本上覆盖衬底表面。组合物的玻璃具有与基材材料相似的CTE。玻璃 - 陶瓷组合物通过将组件加热至少至基材的烧结温度而渗入并使其密实化。

6. 发明授权

US07858192B2 Graded glass/ceramic/glass structures for damage resistant ceramic dental and orthopedic prostheses 有权
标题翻译：分级玻璃/陶瓷/玻璃结构，用于耐磨陶瓷牙科和矫形假体
公开(公告)号：US07858192B2
公开(公告)日：2010-12-28
申请号：US11986290
申请日：2007-11-20
申请人： Yu Zhang , Jae-Won Kim , Van P. Thompson
发明人： Yu Zhang , Jae-Won Kim , Van P. Thompson
IPC分类号： B32B17/06
CPC分类号： A61C13/083 , C03C14/00
摘要： The present invention provides a functionally graded glass/ceramic/glass sandwich system especially useful in damage resistant, ceramic dental and orthopedic prosthesis. The functionally graded glass/substrate/glass composite structure comprises an outer (aesthetic) residual glass layer, a graded glass-ceramic layer, and a dense interior ceramic. The functionally graded glass/substrate/glass composite structure may further comprise a veneer on an exterior surface. The present invention also provides a method for preparing a functionally graded glass/ceramic/glass sandwich system. A powdered glass-ceramic composition or a glass tape is applied to the accessible surfaces of a dense alumina substrate to thereby substantially cover the substrate surfaces. The glass of the composition has a CTE similar to that of the substrate material. The glass-ceramic composition is infiltrated into the dense substrate by heating the assembly to temperatures 50-700° C. below the sintering temperature of the substrate.
摘要翻译：本发明提供了一种功能梯度的玻璃/陶瓷/玻璃夹层系统，特别适用于耐损伤陶瓷牙科和矫形假体。功能梯度的玻璃/基底/玻璃复合结构包括外部（美观的）残余玻璃层，梯度玻璃陶瓷层和致密的内部陶瓷。功能梯度的玻璃/基底/玻璃复合结构还可以在外表面上包括单板。本发明还提供了制备功能梯度玻璃/陶瓷/玻璃夹心系统的方法。将粉末状玻璃陶瓷组合物或玻璃带施加到致密氧化铝基板的可接近表面，从而基本上覆盖基板表面。组合物的玻璃具有与基材材料相似的CTE。通过将组件加热到低于衬底的烧结温度50-700℃的温度下，将玻璃 - 陶瓷组合物渗透到致密衬底中。

7. 发明申请

US20080213727A1 Graded glass/ceramic/glass structures for damage resistant ceramic dental and orthopedic prostheses 有权
标题翻译：分级玻璃/陶瓷/玻璃结构，用于耐磨陶瓷牙科和矫形假体
公开(公告)号：US20080213727A1
公开(公告)日：2008-09-04
申请号：US11986290
申请日：2007-11-20
申请人： Yu Zhang , Jae-Won Kim , Van P. Thompson
发明人： Yu Zhang , Jae-Won Kim , Van P. Thompson
IPC分类号： A61C13/08 , C03C14/00
CPC分类号： A61C13/083 , C03C14/00
摘要： The present invention provides a functionally graded glass/ceramic/glass sandwich system especially useful in damage resistant, ceramic dental and orthopedic prosthesis. The functionally graded glass/substrate/glass composite structure comprises an outer (aesthetic) residual glass layer, a graded glass-ceramic layer, and a dense interior ceramic. The functionally graded glass/substrate/glass composite structure may further comprise a veneer on an exterior surface. The present invention also provides a method for preparing a functionally graded glass/ceramic/glass sandwich system. A powdered glass-ceramic composition or a glass tape is applied to the accessible surfaces of a dense alumina substrate to thereby substantially cover the substrate surfaces. The glass of the composition has a CTE similar to that of the substrate material. The glass-ceramic composition is infiltrated into the dense substrate by heating the assembly to temperatures 50-700° C. below the sintering temperature of the substrate.
摘要翻译：本发明提供了一种功能梯度的玻璃/陶瓷/玻璃夹层系统，特别适用于耐损伤陶瓷牙科和矫形假体。功能梯度的玻璃/基底/玻璃复合结构包括外部（美观的）残余玻璃层，梯度玻璃陶瓷层和致密的内部陶瓷。功能梯度的玻璃/基底/玻璃复合结构还可以在外表面上包括单板。本发明还提供了制备功能梯度玻璃/陶瓷/玻璃夹心系统的方法。将粉末状玻璃陶瓷组合物或玻璃带施加到致密氧化铝基板的可接近表面，从而基本上覆盖基板表面。组合物的玻璃具有与基材材料相似的CTE。通过将组件加热到低于衬底的烧结温度50-700℃的温度下，将玻璃 - 陶瓷组合物渗透到致密衬底中。

8. 发明授权

US08815327B2 Graded glass/zirconia/glass structures for damage resistant ceramic dental and orthopedic prostheses 有权
标题翻译：分级玻璃/氧化锆/玻璃结构，用于耐磨陶瓷牙科和矫形假体
公开(公告)号：US08815327B2
公开(公告)日：2014-08-26
申请号：US12927586
申请日：2010-11-18
申请人： Yu Zhang , Jae-Won Kim
发明人： Yu Zhang , Jae-Won Kim
IPC分类号： A61L33/00
CPC分类号： C04B35/486 , B82Y30/00 , C04B41/009 , C04B41/5023 , C04B41/86 , C04B2111/00405 , C04B2111/00836 , C04B2235/3217 , C04B2235/3225 , C04B2235/5409 , C04B2235/5454 , C04B41/4539 , C04B35/48
摘要： The present invention provides a functionally graded glass/ceramic/glass sandwich system for use in damage resistant, ceramic and orthopedic prosthesis. The functionally graded glass/substrate/glass composite structure comprises an outer residual glass layer, a graded glass-ceramic layer, and a dense interior ceramic. The functionally graded glass/substrate/glass composite structure may further comprise a veneer on an exterior surface. The present invention also provides a method for preparing a functionally graded glass/ceramic/glass sandwich system. A powdered glass-ceramic composition is applied to the accessible surfaces of a presintered zirconia substrate to thereby substantially cover the substrate surfaces. The glass of the composition has a CTE similar to that of the substrate material. The glass-ceramic composition is infiltrated into and densifies the substrate by heating the assembly to at least the sintering temperature of the substrate.
摘要翻译：本发明提供了一种功能梯度玻璃/陶瓷/玻璃夹层系统，用于耐损伤，陶瓷和矫形假体。功能梯度的玻璃/衬底/玻璃复合结构包括外残留玻璃层，梯度玻璃陶瓷层和致密内部陶瓷。功能梯度的玻璃/基底/玻璃复合结构还可以在外表面上包括单板。本发明还提供了制备功能梯度玻璃/陶瓷/玻璃夹心系统的方法。将粉末状的玻璃 - 陶瓷组合物施加到预烧结的氧化锆衬底的可接近表面上，从而基本上覆盖衬底表面。组合物的玻璃具有与基材材料相似的CTE。玻璃 - 陶瓷组合物通过将组件加热至少至基材的烧结温度而渗入并使其密实化。

9. 发明申请

US20080241551A1 Graded glass/zirconia/glass structures for damage resistant ceramic dental and orthopedic prostheses 有权
标题翻译：分级玻璃/氧化锆/玻璃结构，用于耐磨陶瓷牙科和矫形假体
公开(公告)号：US20080241551A1
公开(公告)日：2008-10-02
申请号：US11983815
申请日：2007-11-09
申请人： Yu Zhang , Jae-Won Kim
发明人： Yu Zhang , Jae-Won Kim
IPC分类号： B05D3/00 , B32B17/06
CPC分类号： C04B35/486 , B82Y30/00 , C04B41/009 , C04B41/5023 , C04B41/86 , C04B2111/00405 , C04B2111/00836 , C04B2235/3217 , C04B2235/3225 , C04B2235/5409 , C04B2235/5454 , C04B41/4539 , C04B35/48
摘要： The present invention provides a functionally graded glass/ceramic/glass sandwich system for use in damage resistant, ceramic and orthopedic prosthesis. The functionally graded glass/substrate/glass composite structure comprises an outer residual glass layer, a graded glass-ceramic layer, and a dense interior ceramic. The functionally graded glass/substrate/glass composite structure may further comprise a veneer on an exterior surface. The present invention also provides a method for preparing a functionally graded glass/ceramic/glass sandwich system. A powdered glass-ceramic composition is applied to the accessible surfaces of a presintered zirconia substrate to thereby substantially cover the substrate surfaces. The glass of the composition has a CTE similar to that of the substrate material. The glass-ceramic composition is infiltrated into and densifies the substrate by heating the assembly to at least the sintering temperature of the substrate.
摘要翻译：本发明提供了一种功能梯度玻璃/陶瓷/玻璃夹层系统，用于耐损伤，陶瓷和矫形假体。功能梯度的玻璃/衬底/玻璃复合结构包括外残留玻璃层，梯度玻璃陶瓷层和致密内部陶瓷。功能梯度的玻璃/基底/玻璃复合结构还可以在外表面上包括单板。本发明还提供了制备功能梯度玻璃/陶瓷/玻璃夹心系统的方法。将粉末状的玻璃 - 陶瓷组合物施加到预烧结的氧化锆衬底的可接近表面上，从而基本上覆盖衬底表面。组合物的玻璃具有与基材材料相似的CTE。玻璃 - 陶瓷组合物通过将组件加热至少至基材的烧结温度而渗入并使其密实化。

10. 发明申请

US20110070452A1 Graded glass/zirconia/glass structures for damage resistant ceramic dental and orthopedic prostheses 有权
公开(公告)号：US20110070452A1
公开(公告)日：2011-03-24
申请号：US12927586
申请日：2010-11-18
申请人： Yu Zhang , Jae-Won Kim
发明人： Yu Zhang , Jae-Won Kim
IPC分类号： B32B17/06 , B05D3/02 , B05D3/06
CPC分类号： C04B35/486 , B82Y30/00 , C04B41/009 , C04B41/5023 , C04B41/86 , C04B2111/00405 , C04B2111/00836 , C04B2235/3217 , C04B2235/3225 , C04B2235/5409 , C04B2235/5454 , C04B41/4539 , C04B35/48
摘要： The present invention provides a functionally graded glass/ceramic/glass sandwich system for use in damage resistant, ceramic and orthopedic prosthesis. The functionally graded glass/substrate/glass composite structure comprises an outer residual glass layer, a graded glass-ceramic layer, and a dense interior ceramic. The functionally graded glass/substrate/glass composite structure may further comprise a veneer on an exterior surface. The present invention also provides a method for preparing a functionally graded glass/ceramic/glass sandwich system. A powdered glass-ceramic composition is applied to the accessible surfaces of a presintered zirconia substrate to thereby substantially cover the substrate surfaces. The glass of the composition has a CTE similar to that of the substrate material. The glass-ceramic composition is infiltrated into and densifies the substrate by heating the assembly to at least the sintering temperature of the substrate.

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