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1. 发明授权

US4920202A Method for production of hydrophilic polymer from hydrated gel polymer 失效
标题翻译：从水合凝胶聚合物制备亲水聚合物的方法
公开(公告)号：US4920202A
公开(公告)日：1990-04-24
申请号：US187866
申请日：1988-04-29
申请人： Yoshio Irie , Kaoru Iwasaki , Takumi Hatsuda , Kazumasa Kimura , Nobuyuki Harada , Kunihiko Ishizaki , Tadao Shimomura , Teruaki Fujiwara
发明人： Yoshio Irie , Kaoru Iwasaki , Takumi Hatsuda , Kazumasa Kimura , Nobuyuki Harada , Kunihiko Ishizaki , Tadao Shimomura , Teruaki Fujiwara
IPC分类号： C08F6/00
CPC分类号： C08F6/001
摘要： A method for the production of a hydrophilic polymer having a small residual monomer content from a hydrated gel polymer, which method comprises drying said hydrated gel polymer by contact thereof with a gas containing at least steam and having a dew point in the range of 50.degree. to 100.degree. C. at a temperature in the range of 80.degree. C. to 250.degree. C., and a hydrophilic polymer obtained therefrom.

2. 发明授权

US4985514A Method for production of water absorbent resin 失效
标题翻译：吸水树脂的生产方法
公开(公告)号：US4985514A
公开(公告)日：1991-01-15
申请号：US229988
申请日：1988-08-09
申请人： Kazumasa Kimura , Takumi Hatsuda , Yoshio Irie , Tadao Shimomura
发明人： Kazumasa Kimura , Takumi Hatsuda , Yoshio Irie , Tadao Shimomura
IPC分类号： C08F220/06 , B01J20/26 , C08F2/10 , C08F8/12 , C08F20/04
CPC分类号： B01J20/26 , C08F20/04 , Y10S526/93
摘要： The present invention is a method for the production of a water absorbent resin, which comprises preparing a monomer component possessing an ability to form a cross-linked structure and convert itself into a hydrated gel polymer during the course of aqueous solution polymerization, possessing an acid group-containing monomer content of at least 50 mol %, and having 10 to 50 mol % of said acid group-containing monomer neutralized and subjecting said monomer component to aqueous solution polymerization within a reaction vessel having a plurality of rotary shafts each fitted with stirring blades.

3. 发明授权

US4734478A Water absorbing agent 失效
标题翻译：吸水剂
公开(公告)号：US4734478A
公开(公告)日：1988-03-29
申请号：US748820
申请日：1985-06-26
申请人： Tsuneo Tsubakimoto , Tadao Shimomura , Yoshio Irie , Yoshihiko Masuda , Kazumasa Kimura , Takumi Hatsuda
发明人： Tsuneo Tsubakimoto , Tadao Shimomura , Yoshio Irie , Yoshihiko Masuda , Kazumasa Kimura , Takumi Hatsuda
IPC分类号： A61L15/18 , A61L15/60 , B01J20/26 , C08F8/14 , C08J3/12 , C08J3/24 , D21H17/28 , D21H17/43
CPC分类号： C08J3/12 , A61L15/18 , A61L15/60 , B01J20/26 , C08F8/14 , D21H17/28 , D21H17/43 , C08F2810/20 , C08J2300/14
摘要： The invention provides [I] a water-absorbing agent composed of a water-absorbing resin powder having the molecular chains near its surface being crosslinked, said powder being obtained by mixing 100 parts by weight of a powder of a carboxyl-containing water-absorbing resin selected from the group consisting of a hydrolyzate of a starch-acrylonitrile graft polymer, a partially neutralized product of a starch-acrylic acid graft polymer, a saponification product of a vinyl acetate-acrylic ester copolymer, a hydrolyzate of an acrylonitrile copolymer, a crosslinked product of a hydrolyzate of an acrylonitrile copolymer, a hydrolyzate of an acrylamide copolymer, a crosslinked product of a hydrolyzate of an acrylamide copolymer, a partially neutralized product of polyacrylic acid, and a crosslinked product of partially neutralized polyacrylic acid with 0.001 to 10 parts by weight of a polyhydric alcohol, 0.01 to 8 parts by weight of a hydrophilic organic solvent and 0 to 8 parts by weight of water, and heating the mixture at a temperature of at least 90.degree. C. to react the water-absorbing resin powder with the polyhydric alcohol; [II] a water-absorbing agent composed of a mixture of the water-absorbing agent [I] with finely divided silica; [III] a water-absorbing agent obtained by pulverizing and granulating a mixture of the water-absorbing agent [I] with an aqueous liquid; and [IV] a water-absorbing agent composed of a mixture of the water-absorbing agent [III] with finely divided silica.
摘要翻译：本发明提供[I]一种由其表面附近的分子链交联的吸水性树脂粉末组成的吸水剂，所述粉末是通过将100重量份的含羧基的吸水性粉末选自淀粉 - 丙烯腈接枝聚合物的水解产物，淀粉 - 丙烯酸接枝聚合物的部分中和产物，乙酸乙烯酯 - 丙烯酸酯共聚物的皂化产物，丙烯腈共聚物的水解产物，丙烯腈共聚物的水解产物，丙烯酰胺共聚物的水解产物，丙烯酰胺共聚物的水解产物的交联产物，聚丙烯酸的部分中和产物和部分中和的聚丙烯酸的交联产物与0.001至10份的交联产物的多元醇，0.01〜8重量份的亲水性有机溶剂和0〜8重量份的水，并在至少90℃的温度下加热混合物以使吸水性树脂粉末与多元醇反应; [II]由吸水剂[I]与细碎二氧化硅的混合物组成的吸水剂; [III]通过将吸水剂[I]与水性液体的混合物粉碎和造粒得到的吸水剂; 和[IV]由吸水剂[III]与细碎二氧化硅的混合物组成的吸水剂。

4. 发明授权

US5250640A Method for production of particulate hydrogel polymer and absorbent resin 失效
标题翻译：颗粒状水凝胶聚合物和吸水树脂的生产方法
公开(公告)号：US5250640A
公开(公告)日：1993-10-05
申请号：US865865
申请日：1992-04-09
申请人： Yoshio Irie , Takumi Hatsuda , Koichi Yonemura , Kazumasa Kimura
发明人： Yoshio Irie , Takumi Hatsuda , Koichi Yonemura , Kazumasa Kimura
IPC分类号： B01J19/20 , B01J20/26 , B29B7/18 , C08F2/10 , C08J3/12
CPC分类号： C08J3/12 , B01J19/20 , B01J20/26 , B29B7/183 , C08J2300/14
摘要： A method for the production of a particulate hydrogel polymer by the exposure of a hydrogel polymer possessing a cross-linked structure to shear force in a vessel thereby finely dividing said hydrogel polymer, which method comprises exerting shear force repeatedly on said hydrogel polymer while keeping said hydrogel polymer at a temperature in the range of from 40.degree. to 110.degree. C. under a mechanical pressure in the range of from 0.01 to 1.5 kg/cm.sup.2, and method for the production of an absorbent resin comprising drying the resultant particulate hydrogel polymer.

5. 发明授权

US5599763A Absorbent material, absorbent body, and method for production thereof 失效
标题翻译：吸收材料，吸收体及其制造方法
公开(公告)号：US5599763A
公开(公告)日：1997-02-04
申请号：US283181
申请日：1994-08-03
申请人： Nobuyuki Harada , Kazumasa Kimura , Tadao Shimomura
发明人： Nobuyuki Harada , Kazumasa Kimura , Tadao Shimomura
IPC分类号： A61F13/15 , A61L15/60 , B01J20/22
CPC分类号： A61F13/53 , A61F13/531 , A61L15/60 , A61F2013/15422 , A61F2013/530299 , A61F2013/53035 , A61F2013/53043 , A61F2013/530496 , A61F2013/530583 , A61F2013/5307 , A61F2013/530708 , Y10T428/24994 , Y10T428/2991 , Y10T428/2998
摘要： An absorbent material produced by mixing 100 parts by weight of an absorbent polymer with 1 to 80 parts by weight of synthetic pulp in the presence of 1 to 40 parts by weight of water, an absorbent body produced by mixing 100 parts by weight of an absorbent polymer with 1 to 80 parts by weight of synthetic pulp in the presence of 1 to 40 parts by weight of water, dry mixing the resultant mixture with 10 to 1,000 parts by weight hydrophilic fibers based on 100 parts by weight of said absorbent polymer, pneumatically molding the resultant mixture in the form of web, and thermally compressing the resultant web to a density in the range of from 0.1 to 1.0 g/cm.sup.3, and a method for production thereof.
摘要翻译：在100重量份的吸收性聚合物与1〜80重量份的合成纸浆中，在1〜40重量份的水的存在下，将100重量份的吸收体与100重量份的吸收剂聚合物，在1〜40重量份的水的存在下，使用1〜80重量份的合成纸浆，将得到的混合物与100重量份所述吸收性聚合物的10〜1000重量份亲水性纤维干混，气动地将所得到的混合物成型为网状，将所得纤维网热压至0.1〜1.0g / cm 3的密度及其制造方法。

6. 发明授权

US5098775A Body fluid-absorbing article 失效
标题翻译：身体吸收物品
公开(公告)号：US5098775A
公开(公告)日：1992-03-24
申请号：US498846
申请日：1990-03-26
申请人： Nobuyuki Harada , Yoshihiro Motono , Kazumasa Kimura , Tadao Shimomura
发明人： Nobuyuki Harada , Yoshihiro Motono , Kazumasa Kimura , Tadao Shimomura
IPC分类号： A61F13/15 , A61L15/50 , A61L15/60
CPC分类号： A61F13/534 , A61L15/50 , A61L15/60 , Y10T442/365 , Y10T442/3756 , Y10T442/3886 , Y10T442/40 , Y10T442/673 , Y10T442/678
摘要： In a body fluid-absorbing article composed of a liquid-permeable front-surface member, a liquid-impermeable rear-surface member, and a fibrous absorbent member nipped therebetween and adapted to be used with the front-surface member held in contact with the human body, by the improvement having disposed in half of the thickness of the absorbent member on the front-surface member side an absorbent composite (A) obtained by applying an ethylenically unsaturated monomer capable of forming an absorbent polymer by polymerization or an aqueous solution of the monomer to a fibrous web and thereafter polymerizing the monomer.

7. 发明授权

US5079034A Method for manufacturing a water absorbent composite by applying an aqueous polymerizable solution to a substrate and polymerizing the coating against polymerization inner surfaces 失效
标题翻译：通过将水性聚合物溶液应用于基材并聚合内聚合内嵌表面的方法制造吸水复合材料的方法
公开(公告)号：US5079034A
公开(公告)日：1992-01-07
申请号：US437714
申请日：1989-11-17
申请人： Koji Miyake , Nobuyuki Harada , Kazumasa Kimura , Tadao Shimomura
发明人： Koji Miyake , Nobuyuki Harada , Kazumasa Kimura , Tadao Shimomura
IPC分类号： D06M14/08
CPC分类号： D06M14/08
摘要： A method of preparation of an absorbent composite in which an aqueous solution containing a water-soluble radical polymerization initiator and a water-soluble ethylenically unsaturated monomer which can be converted into an absorbent polymer by polymerization is applied to a substrate, and the monomer is polymerized while the substrate to which the aqueous solution is applied is, on both the sides, held in contact with polymerization-inert surfaces facing each other. A continuous manufacturing method includes the sequential steps of continuously passing a substrate through (1) a region applying to the substrate an aqueous solution containing a water-soluble radical polymerization initiator and a water-soluble ethylenically unsaturated monomer which can be converted into an absorbent polymer by polymerization, and (2) a region of polymerizing the monomer while maintaining the substrate, on both the sides, in contact with polymerization-inert surfaces facing each other.

8. 发明授权

US5368918A Absorbent material comprising absorbent polymeric particulate material coated with synthetic pulp 失效
标题翻译：包含用合成纸浆涂覆的吸收性聚合物颗粒材料的吸收材料
公开(公告)号：US5368918A
公开(公告)日：1994-11-29
申请号：US752054
申请日：1991-08-29
申请人： Nobuyuki Harada , Kazumasa Kimura , Tadao Shimomura
发明人： Nobuyuki Harada , Kazumasa Kimura , Tadao Shimomura
IPC分类号： A61F13/15 , A61L15/60 , A61F13/20 , B32B5/16
CPC分类号： A61F13/53 , A61F13/531 , A61L15/60 , A61F2013/15422 , A61F2013/530299 , A61F2013/53035 , A61F2013/53043 , A61F2013/530496 , A61F2013/530583 , A61F2013/5307 , A61F2013/530708 , Y10T428/24994 , Y10T428/2991 , Y10T428/2998
摘要： An absorbent material produced by mixing 100 parts by weight of an absorbent polymer with 1 to 80 parts by weight of synthetic pulp in the presence of 1 to 40 parts by weight of water, an absorbent body produced by mixing 100 parts by weight of an absorbent polymer with 1 to 80 parts by weight of synthetic pulp in the presence of 1 to 40 parts by weight of water, dry mixing the resultant mixture with 10 to 1,000 parts by weight hydrophilic fibers based on 100 parts by weight of the absorbent polymer, pneumatically molding the resultant mixture in the form of web, and thermally compressing the resultant web to a density in the range of from 0.1 to 1.0 g/cm.sup.3, and a method for production thereof.
摘要翻译：在100重量份的吸收性聚合物与1〜80重量份的合成纸浆中，在1〜40重量份的水的存在下，将100重量份的吸收体与100重量份的吸收剂聚合物，在1〜40重量份水的存在下，合成纸浆重量为1〜80重量份，基于100重量份吸收性聚合物将所得混合物与10〜1000重量份亲水性纤维干混，气动地将所得到的混合物成型为网状，将所得纤维网热压至0.1〜1.0g / cm 3的密度及其制造方法。

9. 发明授权

US5195999A Absorbent body and absorbent article 失效
标题翻译：吸收体和吸收物品
公开(公告)号：US5195999A
公开(公告)日：1993-03-23
申请号：US751988
申请日：1991-08-29
申请人： Nobuyuki Harada , Kazumasa Kimura , Tadao Shimomura
发明人： Nobuyuki Harada , Kazumasa Kimura , Tadao Shimomura
IPC分类号： A61F13/15 , A61L15/42 , A61L15/60
CPC分类号： A61F13/53 , A61L15/42 , A61L15/60 , A61F2013/15422 , A61F2013/530299 , A61F2013/53035 , A61F2013/53043 , A61F2013/530496 , A61F2013/530583 , A61F2013/5307 , A61F2013/530708 , Y10S428/913 , Y10T442/676 , Y10T442/678
摘要： An absorbent body having an absorbent polymer and hydrophilic fibers as main components thereof, characterized by the fact that the density of said absorbent body is in the range of from 0.1 to 0.5 g/cm.sup.3 or a ratio of wet swelling is not less than 200%, a capacity of said absorbent body for absorption of physiological saline solution under pressure is in the range of from 11 to 25 g/g, and the ratio of exfoliation of said absorbent polymer is not more than 45%, and an absorbent article comprising a liquid-pervious surface material, a liquid-impervious lining material, and the absorbent body layer interposed therebetween.

10. 发明授权

US5140076A Method of treating the surface of an absorbent resin 失效
标题翻译：处理吸收树脂表面的方法
公开(公告)号：US5140076A
公开(公告)日：1992-08-18
申请号：US502738
申请日：1990-04-02
申请人： Takumi Hatsuda , Kazumasa Kimura , Kinya Nagasuna , Akito Yano
发明人： Takumi Hatsuda , Kazumasa Kimura , Kinya Nagasuna , Akito Yano
IPC分类号： B01J20/26 , A61L15/60 , C08F2/16 , C08F8/14 , C08F8/30 , C08F8/32 , C08J3/00 , C08J3/12 , C08J3/24 , C08L101/00
CPC分类号： C08J3/12 , A61L15/60 , C08F8/14 , C08F8/30 , C08F8/32 , C08F2810/20 , C08J2300/14
摘要： A method of treating the surface of an absorbent resin, which comprises mixing (A) 100 parts by weight of an absorbent resin powder possessing a carboxyl group (B) 0.01 to 30 parts by weight of a cross-linking agent, (C) 0 to 50 parts by weight of water, and (D) 0 to 60 parts by weight of a hydrophilic organic solvent in a high-speed stirring type mixer provided with an inner surface formed substantially of a substrate (I) possessing a contact angle of not less than about 60.degree. with respect to water and a heat distortion point of not lower than about 70.degree. C. and completing reaction of said absorbent resin powder (A) with said cross-linking agent (B).

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