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1. 发明授权

US07923572B2 Method for producing ketimine structure-containing alkoxysilane 有权
标题翻译：制备含有酮亚胺结构的烷氧基硅烷的方法
公开(公告)号：US07923572B2
公开(公告)日：2011-04-12
申请号：US12067746
申请日：2006-09-21
申请人： Yoshinori Taniguchi , Makoto Iwai , Keiji Wakita
发明人： Yoshinori Taniguchi , Makoto Iwai , Keiji Wakita
IPC分类号： C07F7/18 , C08K5/00 , C08K5/5465
CPC分类号： C08K5/5465 , C07F7/1892
摘要： A method for producing ketimine structure-containing alkoxysilane comprising reacting amino-functional alkoxysilane with a monocarbonyl compound by heating and azeotropically distilling off the produced water together with the monocarbonyl compound to yield ketimine structure-containing alkoxysilane, characterized by introducing additional monocarbonyl compound at the time of the azeotropic distillation of the produced water together with the monocarbonyl compound.
摘要翻译：一种含有酮亚胺结构的烷氧基硅烷的制造方法，其特征在于，通过与单羰基化合物一起加热共沸蒸馏生成的水，使氨基官能的烷氧基硅烷与单羰基化合物反应，得到含有酮亚胺结构的烷氧基硅烷，其特征在于，与单羰基化合物一起共沸蒸馏生产的水。

2. 发明申请

US20100130764A1 Method For Producing Ketimine Structure-Containing Alkoxysilane 有权
标题翻译：制备含有Ketimine结构的烷氧基硅烷的方法
公开(公告)号：US20100130764A1
公开(公告)日：2010-05-27
申请号：US12067746
申请日：2006-09-21
申请人： Yoshinori Taniguchi , Makoto Iwai , Keiji Wakita
发明人： Yoshinori Taniguchi , Makoto Iwai , Keiji Wakita
IPC分类号： C07F7/10
CPC分类号： C08K5/5465 , C07F7/1892
摘要： A method for producing ketimine structure-containing alkoxysilane comprising reacting amino-functional alkoxysilane with a monocarbonyl compound by heating and azeotropically distilling off the produced water together with the monocarbonyl compound to yield ketimine structure-containing alkoxysilane, characterized by introducing additional monocarbonyl compound at the time of the azeotropic distillation of the produced water together with the monocarbonyl compound.
摘要翻译：一种含有酮亚胺结构的烷氧基硅烷的制造方法，其特征在于，通过与单羰基化合物一起加热共沸蒸馏生成的水，使氨基官能的烷氧基硅烷与单羰基化合物反应，得到含有酮亚胺结构的烷氧基硅烷，其特征在于，与单羰基化合物一起共沸蒸馏生产的水。

3. 发明授权

US07446137B2 Thermosetting resin and thiocyanato-containing organohydrocarbonoxysilane 有权
标题翻译：热固性树脂和含硫氰酸酯的有机氢氧化硅烷
公开(公告)号：US07446137B2
公开(公告)日：2008-11-04
申请号：US10492622
申请日：2002-10-29
申请人： Makoto Iwai , Keiji Wakita , Akihiko Shirahata
发明人： Makoto Iwai , Keiji Wakita , Akihiko Shirahata
IPC分类号： B32B15/00 , B32B27/18 , B32B27/38 , B32B27/42 , C08K5/5419 , C08L61/10 , C08L63/00 , C08L63/04 , C08L79/08
CPC分类号： C09J175/04 , C08G18/4045 , C08G18/54 , C08G18/542 , C08G18/58 , C08G18/61 , C08G18/6438 , C08G18/6529 , C08G18/718 , C08G59/08 , C08G59/4215 , C08G59/621 , C08K5/54 , C08K5/5465 , C08K5/548 , C08L61/06 , C09J163/00 , Y10T428/31511 , Y10T428/31515 , Y10T428/31522 , Y10T428/31529 , Y10T428/31612 , Y10T428/31616 , Y10T428/31623 , Y10T428/31627 , Y10T428/31663 , Y10T428/31678 , Y10T428/31681 , Y10T428/31688 , Y10T428/31721 , Y10T428/31786 , Y10T428/31942
摘要： A curable organic resin composition comprising (A) 100 parts by weight of a curable organic resin and (B) 0.01 to 100 parts by weight of a thiocyanato-containing organohydrocarbonoxysilane or an isothiocyanato-containing organohydrocarbonoxysilane represented by the general formula: X—R1—Si(OR2)nR33-n, wherein X is NCS— or SCN—, R1 is an alkylene or alkyleneoxyalkylene group, R2 and R3 are monovalent hydrocarbon groups, and the subscript n is 1, 2, or 3. The curable organic resin composition possesses superior moldability and, when cured, exhibits superior adhesive properties on substrates such as metals.
摘要翻译：一种可固化有机树脂组合物，其包含（A）100重量份的可固化有机树脂和（B）0.01至100重量份的含硫氰酸酯的有机氢氧化硅烷或由以下通式表示的含异硫氰酸酯的有机氢氧化硅烷：XR < 其中X是NCS-或SCN-，R ^{3 > 1是亚烷基或亚烷氧基亚烷基，R 2和R 3是一价烃基，下标n是1,2或3。可固化有机树脂组合物具有优异的成型性，并且当固化时在诸如金属的基材上表现出优异的粘合性。}

4. 发明授权

US08624064B2 4-hydroxyphenylalkylamine derivative 有权
标题翻译： 4-羟基苯基烷基胺衍生物
公开(公告)号：US08624064B2
公开(公告)日：2014-01-07
申请号：US12808855
申请日：2008-12-16
申请人： Takeaki Saiki , Keiji Wakita , Yasushi Sugiura , Yoshinori Taniguchi
发明人： Takeaki Saiki , Keiji Wakita , Yasushi Sugiura , Yoshinori Taniguchi
IPC分类号： C07C211/09 , C07C211/17 , C07C211/18 , C07C211/22 , C07C211/50 , C07C211/53
CPC分类号： C08F2/40 , C07B63/04 , C07D295/08 , C07D295/096 , C07F7/1804 , C09K15/24
摘要： The present invention relates to a compound represented by the following general formula (I): wherein R1 and R2 independently represent a monovalent hydrocarbon group; R3 represents a hydrogen atom or an alkyl group having 1 to 4 carbon atoms; X represents a divalent hydrocarbon group; and R4, R5 and R6 independently represent a monovalent organic group or a group represented by the following general formula (II): in which R7 and R8 independently represent a monovalent hydrocarbon group; and R9 represents a hydrogen atom or an alkyl group having 1 to 4 carbon atoms, with the proviso that R5 and R6 may combine together to form a divalent hydrocarbon group. The aforementioned compounds are useful as a polymerization inhibitor and the like.
摘要翻译：本发明涉及由以下通式（I）表示的化合物：其中R1和R2独立地表示一价烃基; R3表示氢原子或碳原子数1〜4的烷基。 X表示二价烃基; 并且R 4，R 5和R 6独立地表示一价有机基团或由以下通式（II）表示的基团：其中R 7和R 8独立地表示一价烃基; 并且R 9表示氢原子或具有1至4个碳原子的烷基，条件是R 5和R 6可以结合在一起形成二价烃基。上述化合物可用作阻聚剂等。

5. 发明申请

US20100280188A1 4-HYDROXYPHENYLALKYLAMINE DERIVATIVE 有权
标题翻译： 4-羟基苯甲酰胺衍生物
公开(公告)号：US20100280188A1
公开(公告)日：2010-11-04
申请号：US12808855
申请日：2008-12-16
申请人： Takeaki Saiki , Keiji Wakita , Yasushi Sugiura , Yoshinori Taniguchi
发明人： Takeaki Saiki , Keiji Wakita , Yasushi Sugiura , Yoshinori Taniguchi
IPC分类号： C08L83/05 , C07C211/27 , C07D241/04 , C09K3/00 , C07F7/08
CPC分类号： C08F2/40 , C07B63/04 , C07D295/08 , C07D295/096 , C07F7/1804 , C09K15/24
摘要： The present invention relates to a compound represented by the following general formula (I): wherein R1 and R2 independently represent a monovalent hydrocarbon group; R3 represents a hydrogen atom or an alkyl group having 1 to 4 carbon atoms; X represents a divalent hydrocarbon group; and R4, R5 and R6 independently represent a monovalent organic group or a group represented by the following general formula (II): in which R7 and R8 independently represent a monovalent hydrocarbon group; and R9 represents a hydrogen atom or an alkyl group having 1 to 4 carbon atoms, with the proviso that R5 and R6 may combine together to form a divalent hydrocarbon group. The aforementioned compounds are useful as a polymerization inhibitor and the like.
摘要翻译：本发明涉及由以下通式（I）表示的化合物：其中R1和R2独立地表示一价烃基; R3表示氢原子或碳原子数1〜4的烷基。 X表示二价烃基; 并且R 4，R 5和R 6独立地表示一价有机基团或由以下通式（II）表示的基团：其中R 7和R 8独立地表示一价烃基; 并且R 9表示氢原子或具有1至4个碳原子的烷基，条件是R 5和R 6可以结合在一起形成二价烃基。上述化合物可用作阻聚剂等。

6. 发明授权

US07847116B2 Method of manufacturing an aminoaryl-containing organosilicon compound and method of manufacturing an intermediate product of the aforementioned compound 有权
标题翻译：制备含氨基芳基的有机硅化合物的方法和制备上述化合物的中间产物的方法
公开(公告)号：US07847116B2
公开(公告)日：2010-12-07
申请号：US11576571
申请日：2005-10-04
申请人： Keiji Wakita , Yasushi Sugiura
发明人： Keiji Wakita , Yasushi Sugiura
IPC分类号： C07F7/10
CPC分类号： C07F7/0816 , Y02P20/55
摘要： To provide an aminoaryl containing organosilicon compound with high efficiency, after protecting amino groups of a haloaniline compound with a specific compound, to form a Grignard reagent and to deprotect the aforementioned groups by reacting the Grignard reagent with a silicon compound.
摘要翻译：为了提供具有高效率的含氨基芳基的有机硅化合物，在用特定化合物保护卤代苯胺化合物的氨基后，形成格氏试剂，并通过使格利雅试剂与硅化合物反应来使上述组脱保护。

7. 发明授权

US07932412B2 Method of manufacturing an aminoaryl-containing organosilicon compound and method of manufacturing an intermediate product of the aforementioned compound 有权
标题翻译：制备含氨基芳基的有机硅化合物的方法和制备上述化合物的中间产物的方法
公开(公告)号：US07932412B2
公开(公告)日：2011-04-26
申请号：US12913705
申请日：2010-10-27
申请人： Keiji Wakita , Yasushi Sugiura
发明人： Keiji Wakita , Yasushi Sugiura
IPC分类号： C07F7/10
CPC分类号： C07F7/0816 , Y02P20/55
摘要： To provide an aminoaryl-containing organosilicon compound with high efficiency, after protecting amino groups of a haloaniline compound with a specific compound, to form a Grignard reagent and to deprotect the aforementioned groups by reacting the Grignard reagent with a silicon compound.
摘要翻译：为了提供具有高效氨基芳基的有机硅化合物，在用特定化合物保护卤代苯胺化合物的氨基后，形成格氏试剂，并通过使格利雅试剂与硅化合物反应来使上述基团脱保护。

8. 发明授权

US07915439B2 Method of producing silylalkoxymethyl halide 有权
标题翻译：产生甲硅烷基烷氧基甲基卤的方法
公开(公告)号：US07915439B2
公开(公告)日：2011-03-29
申请号：US11577047
申请日：2005-09-28
申请人： Keiji Wakita
发明人： Keiji Wakita
IPC分类号： C07F7/08 , C07F7/04
CPC分类号： C07F7/083
摘要： A method for making a silylalkoxymethyl halide at good yield represented by the formula: R1R2R3Si—R4—O—CH2X wherein R1, R2, and R3 are an alkyl, cycloalkyl, aryl group, or a halogen atom, R4 is a divalent hydrocarbyl group having 1 to 10 carbon atoms, and X is a halogen atom, by reacting: (a) a silyl alcohol compound with the formula R1R2R3Si—R4—OH wherein R1, R2, R3 and R4 are defined as above, with (b) formaldehyde or a polymer thereof, and (c) a halosilane.
摘要翻译：一种制备甲硅烷基烷氧基甲基卤化物的方法，其以良好的收率由式R1R2R3Si-R4-O-CH2X表示，其中R1，R2和R3是烷基，环烷基，芳基或卤素原子，R4是一个二价烃基，通过使（a）具有式R 1 R 2 R 3 Si-R 4 -OH的甲硅烷醇化合物，其中R 1，R 2，R 3和R 4如上所定义，与（b）甲醛或其聚合物，和（c）卤代硅烷。

9. 发明申请

US20090203932A1 Method of Producing Silylalkoxymethyl Halide 有权
标题翻译：硅烷基烷氧基卤化物的制备方法
公开(公告)号：US20090203932A1
公开(公告)日：2009-08-13
申请号：US11577047
申请日：2005-09-28
申请人： Keiji Wakita
发明人： Keiji Wakita
IPC分类号： C07F7/08
CPC分类号： C07F7/083
摘要： A method for making a silylalkoxymethyl halide at good yield represented by the formula: R1R2R3Si—R4—O—CH2X wherein R1, R2, and R3 are an alkyl, cycloalkyl, aryl group, or a halogen atom, R4 is a divalent hydrocarbyl group having 1 to 10 carbon atoms, and X is a halogen atom, by reacting: (a) a silyl alcohol compound with the formula R1R2R3Si—R4—OH wherein R1, R2, R3 and R4 are defined as above, with (b) formaldehyde or a polymer thereof, and (c) a halosilane.
摘要翻译：制备具有良好收率的甲硅烷基烷氧基甲基卤化物的方法由下式表示：<？in-line-formula description =“In-line Formulas”end =“lead”？> R1R2R3Si-R4-O-CH2X < 式中，R1，R2，R3为烷基，环烷基，芳基或卤原子，R4为碳原子数为1〜10的二价烃基，通过使（a）具有式R 1 R 2 R 3 Si-R 4 -OH的甲硅烷醇化合物，其中R 1，R 2，R 3和R 4如上定义，和（b）甲醛或其聚合物和（ c）卤代硅烷。

10. 发明申请

US20090306370A1 Method Of Manufacturing An Organic Silicon Compound That Contains A Methacryloxy Group Or An Acryloxy Group 有权
标题翻译：含有甲基丙烯酰氧基或丙烯酰氧基的有机硅化合物的制造方法
公开(公告)号：US20090306370A1
公开(公告)日：2009-12-10
申请号：US12064208
申请日：2006-08-09
申请人： Keiji Wakita
发明人： Keiji Wakita
IPC分类号： C07D279/18
CPC分类号： C07D279/20 , C07F7/0879 , C07F7/1876 , C08F2/40
摘要： A method of manufacturing an organic silicon compound that contains a methacryloxy group or an acryloxy group, the method being characterized by the fact that manufacturing or conducting purification by distillation is carried out in the presence of a phenothiazine derivative having a molecular weight equal to or higher than 240. And a stable composition comprising an organic silicon compound that contains a methacryloxy group or an acryloxy group and a phenothiazine derivative having a molecular weight equal to or higher than 240 and used in an amount sufficient to stabilize the aforementioned organic silicon compound.
摘要翻译：一种制造含有甲基丙烯酰氧基或丙烯酰氧基的有机硅化合物的方法，其特征在于，在分子量等于或高于其的分子量的吩噻嗪衍生物存在下，通过蒸馏进行制造或进行精制以及包含含有甲基丙烯酰氧基或丙烯酰氧基的有机硅化合物和分子量等于或高于240的吩噻嗪衍生物并以足以稳定上述有机硅化合物的量使用的稳定组合物。

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