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1. 发明授权

US06780832B1 Water-soluble polymer and its use 失效
标题翻译：水溶性聚合物及其用途
公开(公告)号：US06780832B1
公开(公告)日：2004-08-24
申请号：US09703959
申请日：2000-11-01
申请人： Yoshihiro Maeda , Akiko Hemmi , Shigeru Yamaguchi
发明人： Yoshihiro Maeda , Akiko Hemmi , Shigeru Yamaguchi
IPC分类号： C11D337
CPC分类号： C08F220/06 , C11D3/3757
摘要： The present invention provides: a specific water-soluble polymer exhibiting a high calcium-ion-scavenging function and further exhibiting a high clay-dispersing function even in high-hardness water; a detergent composition comprising the water-soluble polymer; and uses, other than the detergent composition, by making the best use of the characteristics of the water-soluble polymer. The specific water-soluble polymer, according to the present invention, has a calcium ion scavengeability of not less than 0.40 and further has a clay dispersibility of not less than 0.50 in high-hardness water and, preferably, includes polymers A and B as essential components wherein the polymer A has a calcium ion scavengeability of not less than 0.45 and wherein the polymer B has a clay dispersibility of not less than 0.65 in high-hardness water. The detergent composition comprising this water-soluble polymer has a good detergency even in high-hardness water.
摘要翻译：本发明提供：具有高钙离子清除功能的特定的水溶性聚合物，即使在高硬度水中也具有高的粘土分散功能; 包含所述水溶性聚合物的洗涤剂组合物; 并且除了洗涤剂组合物之外，通过充分利用水溶性聚合物的特性来使用。根据本发明的具体的水溶性聚合物的钙离子清除能力不低于0.40，并且在高硬度水中还具有不小于0.50的粘土分散性，并且优选地包括聚合物A和B作为必需的其中聚合物A的钙离子清除能力不低于0.45，其中聚合物B在高硬度水中的粘土分散性不低于0.65。包含该水溶性聚合物的洗涤剂组合物即使在高硬度水中也具有良好的去污力。

2. 发明授权

US06777385B2 Low-Molecular (meth)acrylicacid(salt)-based polymer and its production process and uses 失效
标题翻译：低分子（甲基）丙烯酸（盐）基聚合物及其制备方法和用途
公开(公告)号：US06777385B2
公开(公告)日：2004-08-17
申请号：US09887345
申请日：2001-06-25
申请人： Akiko Hemmi , Yoshihiro Maeda , Shigeru Yamaguchi , Yoshikazu Fujii
发明人： Akiko Hemmi , Yoshihiro Maeda , Shigeru Yamaguchi , Yoshikazu Fujii
IPC分类号： C11D337
CPC分类号： C08F20/04 , C08F2/10 , C08F220/06
摘要： A low-molecular (meth)acrylic acid (salt)-based polymer having a good color tone is obtained by polymerizing an aqueous solution of at least one monomer component of a high concentration in the presence of an alkaline substance, wherein: 100 to 95 mol % of the at least one monomer component is a monoethylenically unsaturated monocarboxylic acid (salt) monomer (a) having 3 to 6 carbon atoms; and 0 to 5 mol % of the at least one monomer component is a monoethylenically unsaturated monomer (b) copolymerizable with the monomer (a) (wherein the total of (a) and (b) is 100 mol % ); and wherein: a persulfate salt and hydrogen peroxide are used together as polymerization catalysts; and the entirety of the alkaline substance as used is set not to be more than 99 mol % of the amount which is necessary for neutralizing all acid groups of the at least one monomer component; and wherein: the dropwise addition of the hydrogen peroxide is completed at the latest 10 minutes earlier than the completion time of the dropwise addition of the at least one monomer component; and/or the amount of the hydrogen peroxide as added till the initiation of the dropwise addition of the at least one monomer component is kept from exceeding 10% of the entirety of the hydrogen peroxide as added. The resultant polymer is useful for such as detergent compositions and water-treating agents.
摘要翻译：通过在碱性物质的存在下聚合至少一种高浓度单体组分的水溶液，得到具有良好色调的低分子（甲基）丙烯酸（盐）基聚合物，其中：100至95 所述至少一种单体成分的摩尔％为碳原子数为3〜6的单烯属不饱和一元羧酸（盐）单体（a） 0〜5摩尔％的单体成分为与单体（a）共聚的单烯属不饱和单体（b）（式中，（a）和（b）的合计为100摩尔％）。并且其中：过硫酸盐和过氧化氢一起用作聚合催化剂; 并且所使用的碱性物质的总量不得大于中和所述至少一种单体成分的所有酸基所必需的量的99摩尔％并且其中：过氧化氢的滴加最早比滴加至少一种单体组分的完成时间早10分钟完成; 和/或直到滴加至少一种单体组分开始时加入的过氧化氢的量保持超过加入的全部过氧化氢的10％。所得聚合物可用于洗涤剂组合物和水处理剂。

3. 发明申请

US20050215463A1 Detergent and fabric care additive containing carboxylic acid polymer 审中-公开
标题翻译：含有羧酸聚合物的洗涤剂和织物保养添加剂
公开(公告)号：US20050215463A1
公开(公告)日：2005-09-29
申请号：US11090211
申请日：2005-03-28
申请人： Akihiko Kanzaki , Yoshikazu Fujii , Akiko Hemmi , Satoshi Yamada , Shuichi Toriya , Shigeru Yamaguchi
发明人： Akihiko Kanzaki , Yoshikazu Fujii , Akiko Hemmi , Satoshi Yamada , Shuichi Toriya , Shigeru Yamaguchi
IPC分类号： C11D3/37 , C08F283/04
CPC分类号： C08F283/04 , C11D3/3757 , C11D3/378
摘要： The present invention provides a detergent and fabric care additive containing a high molecular weight carboxylic acid polymer excellent in solubility in the use of a fabric treatment product such as a detergent and fabric care additive. A detergent and fabric care additive containing a carboxylic acid polymer powder, wherein the carboxylic acid polymer powder satisfies the following conditions (a) and (b) [(a) at least one of conditions that a 0.2% by weight aqueous solution has a viscosity of 10 mPa·s or higher and that a 1% by weight aqueous solution has pH lower than 6 and a 10% by weight aqueous solution has a viscosity of 300 mPa·s or higher and (b) at least one of conditions that 50% by weight or more of the carboxylic acid polymer powder passes through 20 mesh of a sieve according to JIS (Z8801) and that the average particle diameter is 600 μm or smaller]. A detergent and fabric care additive containing a carboxylic acid polymer powder, wherein the carboxylic acid polymer powder satisfies the following conditions (c) and (d) [(c) a 0.2% by weight aqueous solution of the carboxylic acid polymer powder has a viscosity of 10 mPa·s or higher and (d) the carboxylic acid polymer powder contains a carboxyl group and a sulfonic acid group and the ratio of the sulfonic acid group-containing monomer relative to 100% by mole of all monomers comprising the polymer is not less than 0.5% by mole and not more than 90% by mole].
摘要翻译：本发明提供了一种洗涤剂和织物护理添加剂，其含有在使用织物处理产品如洗涤剂和织物护理添加剂时溶解性优异的高分子量羧酸聚合物。一种含有羧酸聚合物粉末的洗涤剂和织物保养添加剂，其中羧酸聚合物粉末满足以下条件（a）和（b）[（a）0.2重量％水溶液具有粘度 10mPa.s或更高，并且1重量％的水溶液的pH低于6，10重量％的水溶液的粘度为300mPa.s或更高，（b）至少一个条件为50 羧酸聚合物粉末的重量％以上根据JIS（Z8801）通过20目筛，平均粒径为600μm以下]。含有羧酸聚合物粉末的洗涤剂和织物保养添加剂，其中羧酸聚合物粉末满足以下条件（c）和（d）[（c）0.2重量％羧酸聚合物粉末水溶液的粘度（d）羧酸聚合物粉末含有羧基和磺酸基，并且含有磺酸基的单体相对于包含聚合物的所有单体相对于100摩尔％的比例不是小于0.5摩尔％且不超过90摩尔％]。

4. 发明授权

US07390776B2 Liquid detergent builder and liquid detergent containing the same 有权
标题翻译：液体洗涤剂助洗剂和含有它的液体洗涤剂
公开(公告)号：US07390776B2
公开(公告)日：2008-06-24
申请号：US10493108
申请日：2003-09-11
申请人： Takahiro Tsumori , Atsuro Yoneda , Akiko Hemmi , Shigeru Yamaguchi
发明人： Takahiro Tsumori , Atsuro Yoneda , Akiko Hemmi , Shigeru Yamaguchi
IPC分类号： C11D1/00 , C11D3/37
CPC分类号： C11D3/3765
摘要： A liquid detergent builder which is highly compatible with a surfactant and gives transparent liquid detergents having extremely excellent detergency, a liquid detergent containing the builder, and a liquid detergent containing an acrylic acid-based polymer (salt) having excellent clay dispersibility and good compatibility with a surfactant. The liquid detergent builder comprises an acrylic acid/maleic acid-based copolymer (salt), wherein the acrylic acid/maleic acid-based copolymer (salt) contains maleic acid (salt) in an amount of 5-90 mol % per mole of the sum of acrylic acid (salt) and maleic acid (salt), and a product (MA×Mw) of a weight average molecular weight (Mw) of the copolymer (salt) and a proportion (MA (mol %)) of the maleic acid (salt) in the copolymer (salt) is 450,000 or less.
摘要翻译：一种液体洗涤剂助洗剂，其与表面活性剂高度相容，并提供具有极好洗涤力的透明液体洗涤剂，含有助洗剂的液体洗涤剂和含有具有优异粘土分散性的丙烯酸类聚合物（盐）和与表面活性剂。液体洗涤剂助洗剂包括丙烯酸/马来酸基共聚物（盐），其中丙烯酸/马来酸基共聚物（盐）含有马来酸（盐）的量为每摩尔5-90摩尔％丙烯酸（盐）和马来酸（盐）的总和和共聚物（盐）的重均分子量（Mw）和马来酸的比例（MA（mol％））的产物（MAxMw）盐）为45万以下。

5. 发明申请

US20050176897A1 Polyalkylenimine-derived polymer and its production process and uses 审中-公开
标题翻译：聚亚烷基亚胺衍生的聚合物及其制备方法和用途
公开(公告)号：US20050176897A1
公开(公告)日：2005-08-11
申请号：US11033951
申请日：2005-01-12
申请人： Akihiko Kanzaki , Yoshikazu Fujii , Shigeru Yamaguchi , Takahiro Miwa , Akiko Hemmi
发明人： Akihiko Kanzaki , Yoshikazu Fujii , Shigeru Yamaguchi , Takahiro Miwa , Akiko Hemmi
IPC分类号： B01F17/16 , B01F17/52 , C02F5/12 , C08G73/02 , C08G73/04 , C11D3/37 , C08L79/00
CPC分类号： C08G73/0213 , C02F5/12 , C02F2103/002 , C11D3/3723
摘要： An object of the present invention is to provide a polyalkylenimine-derived polymer and its production process and uses, wherein the polyalkylenimine-derived polymer can efficiently disperse such as liquid (particularly, water-soluble) dirt and dyes and can exercise excellent performances in uses for such as detergents and water-treating agents. As a means of achieving this object, a polyalkylenimine-derived polymer according to the present invention is an addition product of a carboxyalkyl group to a polyalkylenimine chain and is in the range of 30,000 to 5,000,000 in weight-average molecular weight. In addition, a process according to the present invention for production of a polyalkylenimine-derived polymer comprises a step of causing a polyalkylenimine of 20,000 to 1,000,000 in weight-average molecular weight and an unsaturated carboxylic acid to react together wherein the reaction is carried out under conditions where its reaction concentration is in the range of from 5 weight % up to an X value (weight %) determined by the following equation: X value (weight %)=34−(ratio (mol %) of unsaturated carboxylic acid (mols) to be caused to react relative to all amino groups (mols) of polyalkylenimine chain)/5.
摘要翻译：本发明的目的是提供一种聚亚烷基亚胺衍生的聚合物及其制备方法和用途，其中聚亚烷基亚胺衍生的聚合物可以有效地分散如液体（特别是水溶性）污垢和染料，并且可以在使用中起到优异的性能例如洗涤剂和水处理剂。作为实现该目的的手段，根据本发明的聚亚烷基亚胺衍生的聚合物是羧基烷基与聚亚烷基亚胺链的加成产物，其重均分子量在30,000至5,000,000的范围内。此外，根据本发明的用于制备聚亚烷基亚胺衍生的聚合物的方法包括使重均分子量为20,000至1,000,000的聚亚烷基亚胺和不饱和羧酸反应的步骤，其中反应在其反应浓度在5重量％至X值（重量％）范围内的条件，其由下式确定：<？in-line-formula description =“In-line formula”end =“lead”？ >相对于聚亚烷基亚胺链的所有氨基（摩尔），X值（重量％）= 34-（不饱和羧酸（摩尔）的比例（摩尔％））与5反应。 <？in-line-formula description =“In-line Formulas”end =“tail”？>

6. 发明申请

US20070043178A1 Water-soluble polymer and its production process and uses 审中-公开
标题翻译：水溶性聚合物及其生产工艺及用途
公开(公告)号：US20070043178A1
公开(公告)日：2007-02-22
申请号：US10557828
申请日：2004-06-10
申请人： Akihiko Kanzaki , Akiko Hemmi , Yoshikazu Fujii , Shigeru Yamaguchi
发明人： Akihiko Kanzaki , Akiko Hemmi , Yoshikazu Fujii , Shigeru Yamaguchi
IPC分类号： C08G61/02 , C08F2/00
CPC分类号： C11D3/3757 , C02F1/56 , C02F5/10 , C02F5/105 , C08F220/04 , C08F222/02
摘要： An object of the present invention is to provide: a water-soluble polymer which can exercise a high calcium-ion-binding ability and a high clay dispersibility even under circumstances where high-hardness water is used; and a process for producing such a water-soluble polymer with ease and good productivity. As a means of achieving this object, the water-soluble polymer according to the present invention has: (1) a calcium-ion-binding ability of not less than 470 mgCaCO3/g and further a clay dispersibility of not less than 0.90 in a test liquid having a calcium concentration of 50 ppm in terms of calcium carbonate; or (2) a calcium-ion-binding ability of not less than 430 mgCaCO3/g and further a clay dispersibility of not less than 0.70 in a test liquid having a calcium concentration of 100 ppm in terms of calcium carbonate.
摘要翻译：本发明的目的是提供：即使在使用高硬度水的情况下也能够运用高钙离子结合能力和高粘土分散性的水溶性聚合物; 以及容易且生产率高的水溶性聚合物的制造方法。作为实现该目的的手段，本发明的水溶性聚合物具有：（1）不低于470mgCaCO 3 / g的钙离子结合能力，还有一种粘土在钙浓度为50ppm的试验液中，以碳酸钙计，分散度不小于0.90; 或者（2）在钙浓度为100ppm的试验液中，不低于430mgCaCO 3 / g的钙离子结合能力和不低于0.70的粘土分散性，的碳酸钙。

7. 发明申请

US20050003993A1 Liquid detergent builder and liquid detergent containing the same 有权
标题翻译：液体洗涤剂助洗剂和含有它的液体洗涤剂
公开(公告)号：US20050003993A1
公开(公告)日：2005-01-06
申请号：US10493108
申请日：2003-09-11
申请人： Takahiro Tsumori , Atsuro Yoneda , Akiko Hemmi , Shigeru Yamaguchi
发明人： Takahiro Tsumori , Atsuro Yoneda , Akiko Hemmi , Shigeru Yamaguchi
IPC分类号： C11D3/37
CPC分类号： C11D3/3765
摘要： A liquid detergent builder which is highly compatible with a surfactant and gives transparent liquid detergents having extremely excellent detergency, a liquid detergent containing the builder, and a liquid detergent containing an acrylic acid-based polymer (salt) having excellent clay dispersibility and good compatibility with a surfactant. The liquid detergent builder comprises an acrylic acid/maleic acid-based copolymer (salt), wherein the acrylic acid/maleic acid-based copolymer (salt) contains maleic acid (salt) in an amount of 5-90 mol % per mole of the sum of acrylic acid (salt) and maleic acid (salt), and a product (MA×Mw) of a weight average molecular weight (Mw) of the copolymer (salt) and a proportion (MA (mol %)) of the maleic acid (salt) in the copolymer (salt) is 450,000 or less.
摘要翻译：一种液体洗涤剂助洗剂，其与表面活性剂高度相容，并提供具有极好洗涤力的透明液体洗涤剂，含有助洗剂的液体洗涤剂和含有具有优异粘土分散性的丙烯酸类聚合物（盐）和与表面活性剂。液体洗涤剂助洗剂包括丙烯酸/马来酸基共聚物（盐），其中丙烯酸/马来酸基共聚物（盐）含有马来酸（盐）的量为每摩尔5-90摩尔％丙烯酸（盐）和马来酸（盐）的总和和共聚物（盐）的重均分子量（Mw）和马来酸的比例（MA（mol％））的产物（MAxMw）盐）为45万以下。

8. 发明申请

US20080227949A1 Hydrophilized Polyalkylene Glycol, Production Method Thereof, and Application Thereof 审中-公开
标题翻译：亲水聚亚烷基二醇，其制备方法及其应用
公开(公告)号：US20080227949A1
公开(公告)日：2008-09-18
申请号：US12088646
申请日：2006-09-26
申请人： Atsuro Yoneda , Akiko Hemmi
发明人： Atsuro Yoneda , Akiko Hemmi
IPC分类号： C08G65/02
CPC分类号： C07C305/10 , B01F17/0028 , C08G65/334 , C08G65/335 , C08L71/02 , C11D3/3707
摘要： To provide: a hydrophilized polyalkylene glycol which is preferably used in various applications, and sufficiently exhibits high performances such as detergency; a production method thereof; and an application thereof. A hydrophilized polyalkylene glycol represented by the following formula (1): in the formula, X1 and Y1 being different from each other, and each representing a hydrogen atom, —SO3M, —S—CH2—CH2—SO3M, —PO3M2, or —S—(CH2)t—COOM; R1 to R6 representing a hydrogen atom or an alkyl group; R7 representing a hydrogen atom, an alkyl group, an aryl group, a polyhydric alcohol group, Z1 or Z2 represented by the following formula (2-2) or (2-2); p, q, r, and s representing a valency; in the formula, X2 and Y2 being different from each other, and each representing a hydrogen atom, —SO3M, —S—CH2—CH2—SO3M, —PO3M2, or —S—(CH2)t—COOM; R8 and R9 representing a hydrogen atom or an alkyl group; and R10 representing an alkyl group or an aryl group.
摘要翻译：提供：亲水化的聚亚烷基二醇，其优选用于各种应用，并且充分显示出诸如去污力的高性能; 其制造方法; 及其应用。由下式（1）表示的亲水化聚亚烷基二醇：在式中，X 1和Y 1彼此不同，并且各自表示氢原子， SO 3 M，-S-CH 2 -CH 2 -SO 3 M，-PO 3 或者-S-（CH 2）2 -COOM;或者-S-（CH 2）2 -COOM; 表示氢原子或烷基的R 1至R 6; R 7表示由下列各项表示的氢原子，烷基，芳基，多元醇基，Z 1或Z 2，式（2-2）或（2-2）; p，q，r和s表示化合价; 在式中，X 2和Y 2彼此不同，并且各自表示氢原子，-SO 3 M，-S -CH 2 CH 2，-SO 3 M，-PO 3，M 2，...，N 2 >或-S-（CH 2）2 -COOM; R 8和R 9代表氢原子或烷基; 和R 10代表烷基或芳基。

9. 发明申请

US20080221293A1 Polyalkylene Glycol Monomer, Polyalkylene Glycol Polymer Containing the Same, and Application Thereof 有权
标题翻译：聚亚烷基二醇单体，含有该聚亚烷基二醇单体的聚亚烷基二醇聚合物及其应用
公开(公告)号：US20080221293A1
公开(公告)日：2008-09-11
申请号：US12088629
申请日：2006-09-26
申请人： Atsuro Yoneda , Akiko Hemmi
发明人： Atsuro Yoneda , Akiko Hemmi
IPC分类号： C08F20/00 , C07C33/025
CPC分类号： C08F283/065 , B01F17/0028 , C04B24/161 , C04B24/2605 , C04B24/32 , C08F290/06 , C08F290/062 , C08G65/2609 , C08L51/08 , C11D3/0036 , C11D3/3746 , C08L2666/02
摘要： To provide: a monomer having a polyalkylene glycol chain preferably used in various industrial applications such as detergent builder compositions for clothes and bodies, water-treatment agents, and pigment dispersants; and a polyalkylene glycol polymer using such a monomer as a raw material. A polyalkylene glycol monomer having a polymerizable double bond and a polyalkylene glycol chain, wherein the polyalkylene glycol monomer has a hydrophobic part in the polyalkylene glycol chain and/or at a terminal of the chain, and the polymerizable double bond is derived from allyl glycidyl ether, and a polyalkylene glycol monomer having a monomer unit derived from the above-mentioned polyalkylene glycol monomer, wherein the polyalkylene glycol polymer is a polyalkylene glycol polymer having a carboxylic acid group and/or a sulfonic acid group.
摘要翻译：提供：具有优选用于各种工业应用的聚亚烷基二醇链的单体，例如用于衣服和身体的洗涤剂助洗剂组合物，水处理剂和颜料分散剂; 和使用这种单体作为原料的聚亚烷基二醇聚合物。具有可聚合双键和聚亚烷基二醇链的聚亚烷基二醇单体，其中聚亚烷基二醇单体在聚亚烷基二醇链中和/或末端具有疏水部分，并且可聚合双键衍生自烯丙基缩水甘油醚和具有源自上述聚亚烷基二醇单体的单体单元的聚亚烷基二醇单体，其中聚亚烷基二醇聚合物是具有羧酸基和/或磺酸基的聚亚烷基二醇聚合物。

10. 发明申请

US20140066583A1 CARBOXYL GROUP-CONTAINING POLYMER COMPOSITION 有权
标题翻译：含羧基的聚合物组合物
公开(公告)号：US20140066583A1
公开(公告)日：2014-03-06
申请号：US13600312
申请日：2012-08-31
申请人： Atsuro Yoneda , Akiko Hemmi , Brian Joseph Loughnane
发明人： Atsuro Yoneda , Akiko Hemmi , Brian Joseph Loughnane
IPC分类号： C08F28/02
CPC分类号： C08F28/02 , C08F220/16 , C08F220/18
摘要： The present invention provides a carboxyl group-containing polymer composition that exhibits excellent anti-soil redeposition ability in fabric washing. The carboxyl group-containing polymer composition contains a carboxyl group-containing polymer, which includes specific ratios of a structure unit (a) derived from an acrylic acid-based monomer (A) and a structure unit (b) derived from a sulfonic acid group-containing monomer (B) and has a specific weight average molecular weight, and a specific amount of an adduct of a hydrogen sulfite to the acrylic acid-based monomer (A).
摘要翻译：本发明提供了一种在织物洗涤中表现出优异的抗污垢再沉积能力的含羧基聚合物组合物。含羧基的聚合物组合物含有含羧基的聚合物，其包含来源于丙烯酸类单体（A）的结构单元（a）和源自磺酸基团的结构单元（b）的比例（B），并且具有比重重均分子量和特定量的亚硫酸氢盐与丙烯酸类单体（A）的加合物。

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