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1. 发明授权

US06498264B2 Silyl (meth)acrylates having bulky substituent group and preparation thereof 有权
标题翻译：具有庞大取代基的（甲基）丙烯酸甲硅烷酯及其制备方法
公开(公告)号：US06498264B2
公开(公告)日：2002-12-24
申请号：US10087822
申请日：2002-03-05
申请人： Yoichi Tonomura , Tohru Kubota , Yasufumi Kubota
发明人： Yoichi Tonomura , Tohru Kubota , Yasufumi Kubota
IPC分类号： C07F718
CPC分类号： C07F7/1896
摘要： Silyl (meth)acrylate compounds each having attached to a silicon atom one very bulky tertiary hydrocarbon group and two branched hydrocarbon groups each having a hydrocarbon group at &agr;- or &bgr;-position or two cyclic hydrocarbon groups are very stable to hydrolysis and are useful raw materials from which hydrolyzable, self-erodible polymers for ship bottom paints are prepared.
摘要翻译：各自具有连接到硅原子上的（甲基）丙烯酸甲硅烷酯化合物，一个非常大的叔烃基和两个在α或β-位或两个环烃基上具有烃基的支链烃基对于水解是非常稳定的，并且是有用的制备用于船底涂料的可水解的自溶性聚合物的材料。

2. 发明授权

US06518447B2 Thexylchlorosilanes and making process 有权
公开(公告)号：US06518447B2
公开(公告)日：2003-02-11
申请号：US09985528
申请日：2001-11-05
申请人： Yoichi Tonomura , Tohru Kubota , Yasufumi Kubota
发明人： Yoichi Tonomura , Tohru Kubota , Yasufumi Kubota
IPC分类号： C07F708
CPC分类号： C07F7/12 , C07F7/188
摘要： Chlorosilane compounds having a thexyl group which is a bulky substituent group are novel. The compounds are useful silylating agents because stable silylated products are obtained due to the bulky substituent group.

3. 发明授权

US07569691B2 Protected piperazino group-bearing organoxysilane compound and making method 有权
标题翻译：受保护的含哌嗪基的有机硅氧烷化合物及其制备方法
公开(公告)号：US07569691B2
公开(公告)日：2009-08-04
申请号：US11406239
申请日：2006-04-19
申请人： Yoichi Tonomura , Tohru Kubota
发明人： Yoichi Tonomura , Tohru Kubota
IPC分类号： C07D295/00 , C07D241/04
CPC分类号： C07F7/1804
摘要： A novel organoxysilane compound bearing a protected piperazino group is provided. It can impart rigidity, high mechanical strength, and transparency in the UV region when used in paints, adhesives and the like.
摘要翻译：提供一种带有受保护的哌嗪基的新型有机氧基硅烷化合物。当用于油漆，粘合剂等时，它可以赋予UV区域的刚性，高机械强度和透明度。

4. 发明申请

US20060241294A1 Protected piperazino group-bearing organoxysilane compound and making method 有权
公开(公告)号：US20060241294A1
公开(公告)日：2006-10-26
申请号：US11406239
申请日：2006-04-19
申请人： Yoichi Tonomura , Tohru Kubota
发明人： Yoichi Tonomura , Tohru Kubota
IPC分类号： C07F7/02
CPC分类号： C07F7/1804
摘要： A novel organoxysilane compound bearing a protected piperazino group is provided. It can impart rigidity, high mechanical strength, and transparency in the UV region when used in paints, adhesives and the like.

5. 发明授权

US08436166B2 Amino-containing vinylsilane compounds and making method 有权
标题翻译：含氨基乙烯基硅烷化合物及其制备方法
公开(公告)号：US08436166B2
公开(公告)日：2013-05-07
申请号：US12797721
申请日：2010-06-10
申请人： Yoichi Tonomura , Tohru Kubota
发明人： Yoichi Tonomura , Tohru Kubota
IPC分类号： C07F7/10
CPC分类号： C08K5/544 , C07F7/081
摘要： Vinylsilane compounds having a specific amino group, typically diethylaminopropyldimethylvinylsilane, N-methylpiperazinylpropyldimethylvinylsilane, and bistrimethylsilylaminopropyldimethylvinylsilane are novel and useful as a modifier for polymers.
摘要翻译：具有特定氨基的乙烯基硅烷化合物通常是二乙基氨基丙基二甲基乙烯基硅烷，N-甲基哌嗪基丙基二甲基乙烯基硅烷和双三甲基甲硅烷基氨基丙基二甲基乙烯基硅烷作为聚合物的改性剂。

6. 发明申请

US20100105938A1 SILYL (METH)ACRYLATE COMPOUND CONTAINING A SILOXY GROUP HAVING A BULKY SUBSTITUENT AND ITS PRODUCTION METHOD 有权
标题翻译：含甲基取代基的硅氧烷（甲基）丙烯酸酯化合物及其生产方法
公开(公告)号：US20100105938A1
公开(公告)日：2010-04-29
申请号：US12606520
申请日：2009-10-27
申请人： Yoichi Tonomura , Tohru Kubota
发明人： Yoichi Tonomura , Tohru Kubota
IPC分类号： C08F230/08
CPC分类号： C07F7/0838
摘要： A silyl (meth)acrylate compound containing a siloxy group having a bulky substituent is provided. The compound is represented by the following general formula (1): wherein R1 and R2 are independently a C3-10 monovalent branched hydrocarbon group having a hydrocarbon group at α or β position or a monovalent C3-10 cyclic hydrocarbon group; R3, R4, and R5 are independently an unsubstituted or substituted C1-20 hydrocarbon group or a siloxy group represented by the following general formula (2): —OSiR7R8R9 (2) wherein R7, R8, and R9 are independently an unsubstituted or substituted C1-20 hydrocarbon group; and R6 is hydrogen atom or methyl group. This compound is hydrolyzed at a reduced speed, and use of a polymer obtained by copolymerization with an alkyl methacrylate is capable of suppressing attachment of marine organisms to the ship with no or reduced biocide, and this polymer is useful for a hydrolytic self-polishing paint.
摘要翻译：提供含有大体积取代基的甲硅烷氧基的甲基（甲基）丙烯酸酯化合物。该化合物由以下通式（1）表示：其中R 1和R 2独立地为在α或bgr具有烃基的C 3-10单价支链烃基; 位置或一价C 3-10环烃基; R3，R4和R5独立地为未取代或取代的C 1-20烃基或由以下通式（2）表示的甲硅烷氧基：-OSiR7R8R9（2）其中R7，R8和R9独立地为未取代或取代的C1 -20烃基; R6是氢原子或甲基。该化合物以降低的速度水解，并且使用通过与甲基丙烯酸烷基酯共聚得到的聚合物能够抑制海洋生物与没有或减少的杀生物剂的船舶的附着，并且该聚合物可用于水解自抛光涂料。

7. 发明授权

US07202375B2 Bissilylamino group-bearing chlorosilane compound and preparation method, and method of preparing bissilylamino group-bearing organooxysilane compound 有权
标题翻译：含二甲硅烷基氨基的氯硅烷化合物及其制备方法，以及制备含二甲氨基氨基的有机氧基硅烷化合物的方法
公开(公告)号：US07202375B2
公开(公告)日：2007-04-10
申请号：US10854180
申请日：2004-05-27
申请人： Yoichi Tonomura , Tohru Kubota
发明人： Yoichi Tonomura , Tohru Kubota
IPC分类号： C07F7/10
CPC分类号： C07F7/12
摘要： Bissilylamino group-bearing chlorosilane compounds of formula (1): [(CH3)3Si]2NCH2CH2CH2Si(CH3)nCl3−n (1) wherein n is 0 or 1 are novel. They are useful as silane coupling agents and surface treating agents. They can be readily converted, through reaction with alcohols, to bissilyl group-bearing alkoxysilane compounds which are useful as intermediates for the synthesis of aminopropyl-modified silicone oil. The invention also provides an industrially advantageous method capable of preparing the bissilylamino group-bearing chlorosilane compounds.
摘要翻译：含二甲苯基氨基的氯硅烷化合物

8. 发明授权

US06426427B1 Preparation of bissilylnorbornane compounds 失效
标题翻译：二磺酰基降冰片烷化合物的制备
公开(公告)号：US06426427B1
公开(公告)日：2002-07-30
申请号：US09935659
申请日：2001-08-24
申请人： Yoichi Tonomura , Tohru Kubota , Mikio Endo
发明人： Yoichi Tonomura , Tohru Kubota , Mikio Endo
IPC分类号： C07F708
CPC分类号： C07F7/14
摘要： A bissilylnorbornane compound is prepared by reacting 2,5-norbornadiene with a hydrogenchlorosilane in the presence of a mixture of a palladium compound and a phosphite or a palladium complex having a phosphate ligand as a catalyst. The bissilylnorbornane compound can be produced in high yields while suppressing formation of by-product nortricyclene.
摘要翻译：通过在钯化合物和亚磷酸盐或具有磷酸盐配体作为催化剂的钯络合物的混合物存在下使2,5-降冰片二烯与氢氯硅烷反应来制备二苯基降冰片烷化合物。双降冰片烷基化合物可以以高产率生产，同时抑制副产物诺里克林的形成。

9. 发明授权

US06359161B2 Preparation of halopropyldimethylchlorosilanes 有权
标题翻译：制备卤代丙基二甲基氯硅烷
公开(公告)号：US06359161B2
公开(公告)日：2002-03-19
申请号：US09852638
申请日：2001-05-11
申请人： Yoichi Tonomura , Tohru Kubota , Mikio Endo
发明人： Yoichi Tonomura , Tohru Kubota , Mikio Endo
IPC分类号： C07F708
CPC分类号： C07F7/14
摘要： A halopropyldimethylchlorosilane is prepared by reacting dimethylchlorosilane with an allyl halide in the presence of an iridium catalyst. The reaction is effected in the presence of an internal olefin compound, typically 1,5-cyclooctadiene. The internal olefin compound suppresses deactivation of the iridium catalyst during reaction. Using a smaller amount of the iridium catalyst, the process produces the halopropyldimethylchlorosilane in high yields.
摘要翻译：卤代丙基二甲基氯硅烷通过使二氯甲硅烷与烯丙基卤化物在铱催化剂存在下反应来制备。反应在内部烯烃化合物（通常为1,5-环辛二烯）的存在下进行。内部烯烃化合物抑制反应期间铱催化剂的失活。使用较少量的铱催化剂，该方法以高产率生产卤代丙基二甲基氯硅烷。

10. 发明授权

US06245925B1 Hydrosilylation of 4-vinyl-1-cyclohexene 有权
标题翻译： 4-乙烯基-1-环己烯的氢化硅烷化
公开(公告)号：US06245925B1
公开(公告)日：2001-06-12
申请号：US09627074
申请日：2000-07-27
申请人： Yoichi Tonomura , Tohru Kubota , Mikio Endo
发明人： Yoichi Tonomura , Tohru Kubota , Mikio Endo
IPC分类号： C07F708
CPC分类号： C07F7/14
摘要： By reacting 4-vinyl-1-cyclohexene with a hydrogenchlorosilane compound in the presence of a platinum catalyst to give a reaction solution containing a monosilyl compound, removing the residual 4-vinyl-1-cyclohexene and isomers thereof from the reaction solution, and reacting the monosilyl compound again with the hydrogenchlorosilane compound, an organic silicon compound in which the two double bonds in 4-vinyl-1-cyclohexene have been hydrosilylated is produced in high yields.
摘要翻译：通过在铂催化剂存在下使4-乙烯基-1-环己烯与氢氯硅烷化合物反应，得到含有单甲硅烷基化合物的反应溶液，从反应溶液中除去残留的4-乙烯基-1-环己烯及其异构体，再次与高氯代硅烷化合物（其中4-乙烯基-1-环己烯中的两个双键已经被氢化硅烷化）的有机硅化合物再次产生单甲硅烷基化合物。

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