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1. 发明授权

US08362126B2 Functionalized high cis-1,4-polybutadiene prepared using novel functionalizing agents 有权
标题翻译：使用新型官能化剂制备的官能化高顺式-1,4-聚丁二烯
公开(公告)号：US08362126B2
公开(公告)日：2013-01-29
申请号：US12644382
申请日：2009-12-22
申请人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
发明人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
IPC分类号： C08K5/13 , C08F36/00
CPC分类号： C08F136/14 , C08C19/00 , C08C19/22 , C08C19/44 , C08F36/04 , C08F136/06 , C08K3/04 , C08K3/045 , C08K3/36 , C08L21/00 , C08L91/00 , C08F4/545 , C08L15/00
摘要： A method for preparing a functionalized polymer comprising the steps of preparing a polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst, wherein the lanthanide-based catalyst comprises (a) a lanthanide compound, (b) an alkylating agent, and (c) a source of halogen, and reacting the pseudo-living polymer with at least one amide-containing functionalizing agent.
摘要翻译：一种制备官能化聚合物的方法，包括以下步骤：通过使镧系元素基催化剂聚合共轭二烯单体来制备聚合物，其中所述镧系元素基催化剂包含（a）镧系元素化合物，（b）烷基化剂和（c ）卤素源，并使假活性聚合物与至少一种含酰胺官能化试剂反应。

2. 发明授权

US07642322B2 Functionalized high cis-1,4-polybutadiene prepared using novel functionalizing agents 有权
标题翻译：使用新型官能化剂制备的官能化高顺式-1,4-聚丁二烯
公开(公告)号：US07642322B2
公开(公告)日：2010-01-05
申请号：US11216559
申请日：2005-08-31
申请人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
发明人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
IPC分类号： C08C19/34 , C08C19/22
CPC分类号： C08F136/14 , C08C19/00 , C08C19/22 , C08C19/44 , C08F36/04 , C08F136/06 , C08K3/04 , C08K3/045 , C08K3/36 , C08L21/00 , C08L91/00 , C08F4/545 , C08L15/00
摘要： A functionalized polymer prepared by a process comprising the steps of preparing a pseudo-living polymer by polymerizing conjugated monomer with a lanthanide-based catalyst, and reacting the pseudo-living polymer with a functionalizing agent defined by the formula (I) A-R1-Z (I) where R1 is a divalent bond or divalent organic group comprising from 0 to about 20 carbon atoms, A is a substituent that will undergo an addition reaction with a pseudo-living polymer, and Z is a substituent that will react or interact with silica or carbon black reinforcing fillers, with the proviso that A, R1, and Z are substituents that will not protonate a pseudo-living polymer.
摘要翻译：通过包括以下步骤制备的官能化聚合物的方法，所述方法包括通过使镧系元素类催化剂与共轭单体聚合制备假活性聚合物，并使假活性聚合物与式（I）A-R1- Z（I）其中R1是二价键或包含0至约20个碳原子的二价有机基团，A是将与假活性聚合物进行加成反应的取代基，Z是将反应或相互作用的取代基具有二氧化硅或炭黑增强填料，条件是A，R 1和Z是不会使假活性聚合物质子化的取代基。

3. 发明授权

US06992147B1 Modified polymers prepared with lanthanide-based catalysts 有权
标题翻译：用镧系元素催化剂制备的改性聚合物
公开(公告)号：US06992147B1
公开(公告)日：2006-01-31
申请号：US10296084
申请日：2000-11-10
申请人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Tatsuo Fujimaki , Takuo Sone , Iwakazu Hattori , Koichi Morita
发明人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Tatsuo Fujimaki , Takuo Sone , Iwakazu Hattori , Koichi Morita
IPC分类号： C08C19/00 , C08F8/00
CPC分类号： C08C19/44 , C08F136/04 , C08K3/36 , C08L7/00 , C08L9/06 , C08L19/006 , C08F4/545 , C08L2666/08
摘要： A method for preparing a functionalized polymer comprising the steps of preparing a pseudo-living polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst, and reacting the pseudo-living polymer with at least one functionalizing agent defined by the formula (I) where A is a substituent that will undergo an addition reaction with a pseudo-living polymer, R1 is a divalent organic group, R2 is a monovalent organic group, and each R4, which may be the same or different, is a monovalent organic group or a substituent defined by —OR5 where R5 is a monovalent organic group, with the proviso that A, R1, R2, R4, and R5 are substituents that will not protonate a pseudo-living polymer. Also, the functionalized polymer and a vulcanizable composition containing the polymer.
摘要翻译：一种制备官能化聚合物的方法，包括以下步骤：通过使共轭二烯单体与镧系元素基催化剂聚合制备假活性聚合物，并使假活性聚合物与至少一种由式（I）定义的官能化试剂反应，其中 A是将与假活性聚合物进行加成反应的取代基，R 1是二价有机基团，R 2是一价有机基团，并且每个R 可以相同或不同的一价有机基团或由-OR 5定义的取代基，其中R 5是一价有机基团，条件是A，R 1，R 2，R 4和R 5都是不会将假活性聚合物质子化的取代基。此外，官能化聚合物和含有聚合物的可硫化组合物。

4. 发明授权

US07750087B2 Modified polymers prepared with lanthanide-based catalysts 有权
标题翻译：用镧系元素催化剂制备的改性聚合物
公开(公告)号：US07750087B2
公开(公告)日：2010-07-06
申请号：US11244999
申请日：2005-10-06
申请人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Tatsuo Fujimaki , Takuo Sone , Iwakazu Hattori , Koichi Morita
发明人： Yoichi Ozawa , H. Jerrold Miller , Koji Masaki , Tatsuo Fujimaki , Takuo Sone , Iwakazu Hattori , Koichi Morita
IPC分类号： C08C19/00 , C08F8/00
CPC分类号： C08C19/44 , C08F136/04 , C08K3/36 , C08L7/00 , C08L9/06 , C08L19/006 , C08F4/545 , C08L2666/08
摘要： A method for preparing a functionalized polymer comprising the steps of preparing a pseudo-living polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst, and reacting the pseudo-living polymer with at least one functionalizing agent defined by the formula (I) where A is a substituent that will undergo an addition reaction with a pseudo-living polymer, R1 is a divalent organic group, R2 is a monovalent organic group, and each R4, which may be the same or different, is a monovalent organic group or a substituent defined by —OR5 where R5 is a monovalent organic group, with the proviso that A, R1, R2, R4, and R5 are substituents that will not protonate a pseudo-living polymer. Also, the functionalized polymer and a vulcanizable composition containing the polymer.
摘要翻译：一种制备官能化聚合物的方法，包括以下步骤：通过使共轭二烯单体与镧系元素基催化剂聚合制备假活性聚合物，并使假活性聚合物与式（I）定义的至少一种官能化试剂反应，其中 A是将与假活性聚合物进行加成反应的取代基，R 1是二价有机基团，R 2是一价有机基团，并且各个可以相同或不同的R 4是一价有机基团或由-OR5定义的取代基，其中R5是一价有机基团，条件是A，R1，R2，R4和R5是不会使假活性聚合物质子化的取代基。此外，官能化聚合物和含有聚合物的可硫化组合物。

5. 发明申请

US20100099826A1 FUNTIONALIZED HIGH CIS-1,4-POLYBUTADIENE PREPARED USING NOVEL FUNCTIONALIZING AGENTS 有权
标题翻译：使用新型功能化剂制备的功能性高的CIS-1,4-聚丁二烯
公开(公告)号：US20100099826A1
公开(公告)日：2010-04-22
申请号：US12644382
申请日：2009-12-22
申请人： Yoichi OZAWA , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
发明人： Yoichi OZAWA , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
IPC分类号： C08F136/06
CPC分类号： C08F136/14 , C08C19/00 , C08C19/22 , C08C19/44 , C08F36/04 , C08F136/06 , C08K3/04 , C08K3/045 , C08K3/36 , C08L21/00 , C08L91/00 , C08F4/545 , C08L15/00
摘要： A method for preparing a functionalized polymer comprising the steps of preparing a polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst, wherein the lanthanide-based catalyst comprises (a) a lanthanide compound, (b) an alkylating agent, and (c) a source of halogen, and reacting the pseudo-living polymer with at least one amide-containing functionalizing agent.
摘要翻译：一种制备官能化聚合物的方法，包括以下步骤：通过使镧系元素基催化剂聚合共轭二烯单体来制备聚合物，其中所述镧系元素基催化剂包含（a）镧系元素化合物，（b）烷基化剂和（c ）卤素源，并使假活性聚合物与至少一种含酰胺官能化试剂反应。

6. 发明授权

US08618199B2 Functionalized high cis-1,4-polybutadiene prepared using novel functionalizing agents 有权
公开(公告)号：US08618199B2
公开(公告)日：2013-12-31
申请号：US13711701
申请日：2012-12-12
申请人： Yoichi F. Ozawa , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
发明人： Yoichi F. Ozawa , H. Jerrold Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuya Omura , Takuo Sone , Iwakazu Hattori
IPC分类号： C08K5/13 , C08C19/22
CPC分类号： C08F136/14 , C08C19/00 , C08C19/22 , C08C19/44 , C08F36/04 , C08F136/06 , C08K3/04 , C08K3/045 , C08K3/36 , C08L21/00 , C08L91/00 , C08F4/545 , C08L15/00
摘要： A method for preparing a functionalized polymer comprising the steps of preparing a polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst, wherein the lanthanide-based catalyst comprises (a) a lanthanide compound, (b) an alkylating agent, and (c) a source of halogen, and reacting the pseudo-living polymer with at least one amide-containing functionalizing agent.

7. 发明申请

US20060030677A1 Modified polymers prepared with lanthanide-based catalysts 有权
公开(公告)号：US20060030677A1
公开(公告)日：2006-02-09
申请号：US11244999
申请日：2005-10-06
申请人： Yoichi Ozawa , H. Miller , Koji Masaki , Tatsuo Fujimaki , Takuo Sone , Iwakazu Hattori , Koichi Morita
发明人： Yoichi Ozawa , H. Miller , Koji Masaki , Tatsuo Fujimaki , Takuo Sone , Iwakazu Hattori , Koichi Morita
IPC分类号： C08F8/00
CPC分类号： C08C19/44 , C08F136/04 , C08K3/36 , C08L7/00 , C08L9/06 , C08L19/006 , C08F4/545 , C08L2666/08
摘要： A method for preparing a functionalized polymer comprising the steps of preparing a pseudo-living polymer by polymerizing conjugated diene monomer with a lanthanide-based catalyst, and reacting the pseudo-living polymer with at least one functionalizing agent defined by the formula (I) where A is a substituent that will undergo an addition reaction with a pseudo-living polymer, R1 is a divalent organic group, R2 is a monovalent organic group, and each R4, which may be the same or different, is a monovalent organic group or a substituent defined by —OR5 where R5 is a monovalent organic group, with the proviso that A, R1, R2, R4, and R5 are substituents that will not protonate a pseudo-living polymer. Also, the functionalized polymer and a vulcanizable composition containing the polymer.

8. 发明申请

US20060004131A1 Functionalized high cis-1,4-polybutadiene prepared using novel functionalizing agents 有权
标题翻译：使用新型官能化剂制备的官能化高顺式-1,4-聚丁二烯
公开(公告)号：US20060004131A1
公开(公告)日：2006-01-05
申请号：US11216559
申请日：2005-08-31
申请人： Yoichi Ozawa , H. Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuyo Ohumura , Takuo Sone , Iwakazu Hattori
发明人： Yoichi Ozawa , H. Miller , Koji Masaki , Koichi Morita , Tatsuo Fujimaki , Tetsuyo Ohumura , Takuo Sone , Iwakazu Hattori
IPC分类号： C08L1/00
CPC分类号： C08F136/14 , C08C19/00 , C08C19/22 , C08C19/44 , C08F36/04 , C08F136/06 , C08K3/04 , C08K3/045 , C08K3/36 , C08L21/00 , C08L91/00 , C08F4/545 , C08L15/00
摘要： A functionalized polymer prepared by a process comprising the steps of preparing a pseudo-living polymer by polymerizing conjugated monomer with a lanthanide-based catalyst, and reacting the pseudo-living polymer with a functionalizing agent defined by the formula (I) A-R1-Z (I) where R1 is a divalent bond or divalent organic group comprising from 0 to about 20 carbon atoms, A is a substituent that will undergo an addition reaction with a pseudo-living polymer, and Z is a substituent that will react or interact with silica or carbon black reinforcing fillers, with the proviso that A, R1, and Z are substituents that will not protonate a pseudo-living polymer.
摘要翻译：一种官能化聚合物，其通过以下步骤制备：包括以下步骤：通过使共轭单体与镧系元素基催化剂聚合制备假活性聚合物，并使假活性聚合物与由式（I）定义的官能化试剂反应， line-formula description =“In-line Formulas”end =“lead”？> AR ^{1 -Z（I）<？in-line-formula description =“In-line Formulas”end =“ 尾“→其中R 1是二价键或包含0至约20个碳原子的二价有机基团，A是将与假活性聚合物进行加成反应的取代基，Z 是将与二氧化硅或炭黑增强填料反应或相互作用的取代基，条件是A，R 1和Z是不会使假活性聚合物质子化的取代基。}

9. 发明授权

US06838526B1 Modified conjugated diene polymer and method of producing the same and rubber composition 有权
标题翻译：改性共轭二烯聚合物及其制备方法和橡胶组合物
公开(公告)号：US06838526B1
公开(公告)日：2005-01-04
申请号：US09709563
申请日：2000-11-13
申请人： Takuo Sone , Ryouji Tanaka , Kouichirou Tani , Iwakazu Hattori , Hiroshi Akema , Atsushi Nakayama
发明人： Takuo Sone , Ryouji Tanaka , Kouichirou Tani , Iwakazu Hattori , Hiroshi Akema , Atsushi Nakayama
IPC分类号： B60C1/00 , C08C19/00 , C08C19/44 , C08L19/00 , C08F8/34
CPC分类号： C08L19/006 , B60C1/0016 , B60C1/0025 , C08C19/00 , C08C19/44 , C08K3/04 , C08L7/00 , C08L9/00 , C08L9/02 , C08L9/06 , C08L11/00 , C08L23/0815 , C08L23/16 , C08L23/283 , C08L2666/08 , C08L2666/06
摘要： A novel modified conjugated diene polymer is obtained by polymerizing a conjugated diene compound with a specified catalyst consisting of components (a)-(c) and then reacting with at least one specified compound selected from the group consisting of components (d)-(l), and has a content of cis-1,4-bond of not less than 85% and a ratio of weight average molecular weight to number average molecular weight of not more than 4. And also, a rubber composition comprises the modified conjugated diene polymer a rubber ingredient.
摘要翻译：通过将共轭二烯化合物与由组分（a） - （c）组成的特定催化剂聚合，然后与至少一种选自组分（d） - （I））的特定化合物反应获得新的改性共轭二烯聚合物），并且具有不小于85％的顺式-1,4-键含量，重均分子量与数均分子量之比不大于4.另外，橡胶组合物包含改性共轭二烯聚合橡胶成分。

10. 发明授权

US6130299A Method for preparing conjugated diene polymer 失效
标题翻译：共轭二烯聚合物的制备方法
公开(公告)号：US6130299A
公开(公告)日：2000-10-10
申请号：US974922
申请日：1997-11-20
申请人： Takuo Sone , Akio Takashima , Katsutoshi Nonaka , Iwakazu Hattori
发明人： Takuo Sone , Akio Takashima , Katsutoshi Nonaka , Iwakazu Hattori
IPC分类号： C08F2/34 , C08F2/44 , C08F4/54 , C08F36/04 , C08F4/52
CPC分类号： C08F36/04
摘要： A method for preparing a conjugated diene polymer characterized by polymerizing a conjugated diene in vapor phase in the presence of an inorganic filler used as a rubber reinforcement agent and a catalyst which comprises (a) a compound containing a rare earth element of an atomic number of from 57 to 71 in the Periodic Table or a compound obtained by the reaction of this rare earth element-containing compound and a Lewis base, (b) an organic aluminum compound of the formula AlR.sup.1 R.sup.2 R.sup.3 or an almoxane, and (c) a halogen-containing compound. The vapor phase polymerization ensures easy control of the molecular weight of the polymer better dispersion of a rubber enforcement agent, and provides a rubber composition with improved rupture characteristics and abrasion resistance.
摘要翻译：一种制备共轭二烯聚合物的方法，其特征在于在用作橡胶增强剂的无机填料和催化剂存在下，气相中共轭二烯的聚合，所述催化剂包含（a）含有原子序数的稀土元素的化合物周期表中的57至71或通过该含稀土元素的化合物与路易斯碱的反应获得的化合物，（b）式AlR 1 R 2 R 3的有机铝化合物或阿莫氧烷，和（c）含有化合物。气相聚合确保了聚合物的分子量更容易控制橡胶强化剂的分散性，并提供了具有改进的断裂特性和耐磨性的橡胶组合物。

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