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1. 发明授权

US07497900B2 Two-part borate, silicate and zinc compositions, and methods for treating wood products 失效
标题翻译：两部分硼酸盐，硅酸盐和锌组合物，以及木制品的处理方法
公开(公告)号：US07497900B2
公开(公告)日：2009-03-03
申请号：US11547377
申请日：2005-03-31
申请人： Yatao Hu , Jason D. Lenox , Neil T. Miller , David M. Schubert
发明人： Yatao Hu , Jason D. Lenox , Neil T. Miller , David M. Schubert
IPC分类号： A01N59/14 , A01N59/16
CPC分类号： C09D1/02 , A01N59/16 , B27K3/16 , B27N9/00 , C09D5/14 , C09D15/00 , Y10S424/11 , A01N59/14 , A01N59/00 , A01N25/22 , A01N25/02 , A01N2300/00
摘要： Systems and methods are provided for treating products containing wood fibers to provide protection against wood destroying organisms and fire, and resistance against leaching of the preservative from the wood by water in exposed environments such as exterior applications. The methods involve applying to a substrate a first aqueous composition containing a boron compound, a source of zinc, and ammonia, followed by application of a second aqueous composition containing an alkali metal silicate. The compositions may be applied by vacuum and/or pressure treatment or dip treatment under atmospheric pressure.
摘要翻译：提供了用于处理含有木纤维的产品的系统和方法，以提供防止木材破坏的生物和火灾的保护，以及在诸如外部应用的暴露的环境中防止来自木材的水的浸出。所述方法包括向基材施加含有硼化合物，锌源和氨的第一含水组合物，然后施加含有碱金属硅酸盐的第二含水组合物。组合物可以通过在大气压下进行真空和/或压力处理或浸渍处理来施加。

2. 发明申请

US20080124478A1 Two-Part Borate, Silicate and Zinc Compositions, and Methods for Treating Wood Products 失效
标题翻译：两部分硼酸盐，硅酸盐和锌组合物以及木制品处理方法
公开(公告)号：US20080124478A1
公开(公告)日：2008-05-29
申请号：US11547377
申请日：2005-03-31
申请人： Yatao Hu , Jason D. Lenox , Neil T. Miller , David M. Schubert
发明人： Yatao Hu , Jason D. Lenox , Neil T. Miller , David M. Schubert
IPC分类号： C09D5/00 , B05D1/18 , B05D5/00
CPC分类号： C09D1/02 , A01N59/16 , B27K3/16 , B27N9/00 , C09D5/14 , C09D15/00 , Y10S424/11 , A01N59/14 , A01N59/00 , A01N25/22 , A01N25/02 , A01N2300/00
摘要： Systems and methods are provided for treating products containing wood fibers to provide protection against wood destroying organisms and fire, and resistance against leaching of the preservative from the wood by water in exposed environments such as exterior applications. The methods involve applying to a substrate a first aqueous composition containing a boron compound, a source of zinc, and ammonia, followed by application of a second aqueous composition containing an alkali metal silicate. The compositions may be applied by vacuum and/or pressure treatment or dip treatment under atmospheric pressure.
摘要翻译：提供了用于处理含有木纤维的产品的系统和方法，以提供防止木材破坏的生物和火灾的保护，以及在诸如外部应用的暴露的环境中防止来自木材的水的浸出。所述方法包括向基材施加含有硼化合物，锌源和氨的第一含水组合物，然后施加含有碱金属硅酸盐的第二含水组合物。组合物可以通过在大气压下进行真空和/或压力处理或浸渍处理来施加。

3. 发明授权

US07547354B2 Ammoniacal borate and zinc compositions, and methods for treating wood products 失效
标题翻译：氨基硼酸锌和锌组合物，以及木制品的处理方法
公开(公告)号：US07547354B2
公开(公告)日：2009-06-16
申请号：US11547375
申请日：2005-03-31
申请人： Yatao Hu , Neil T. Miller , David M. Schubert
发明人： Yatao Hu , Neil T. Miller , David M. Schubert
IPC分类号： A01N59/14 , A01N59/16
CPC分类号： B27K3/20 , A01N59/16 , B27K3/163 , B27K3/22 , B27K3/32 , Y10S424/10 , Y10S424/11 , A01N59/14 , A01N59/00 , A01N25/22 , A01N25/02 , A01N2300/00
摘要： Compositions and methods are provided for treating wood products to provide leach-resistant protection against fungal decay, termites and other wood destroying organisms. The preservative compositions provided include ammonia-stabilized solutions of zinc and boron, preferably in a molar ratio of Zn:B of between about 0.4:1 and 5:1, and are essentially copper free. The preservative may be applied by vacuum and/or pressure treatment or dip treatment under atmospheric pressure.
摘要翻译：提供了组合物和方法，用于处理木制品以提供防止真菌腐烂，白蚁和其他破坏木材的生物的耐水浸保护。提供的防腐剂组合物包括锌稳定的锌和硼的溶液，优选的是Zn:B的摩尔比为约0.4:1至5:1，并且基本上不含铜。防腐剂可以通过在大气压下进行真空和/或压力处理或浸渍处理来施加。

4. 发明申请

US20080166481A1 Ammoniacal Borate And Zinc Compositions, And Methods For Treating Wood Products 失效
标题翻译：氨基硼酸锌和锌组合物，以及木制品的处理方法
公开(公告)号：US20080166481A1
公开(公告)日：2008-07-10
申请号：US11547375
申请日：2005-03-31
申请人： Yatao Hu , Neil T. Miller , David M. Schubert
发明人： Yatao Hu , Neil T. Miller , David M. Schubert
IPC分类号： C09D1/00 , B05D3/00 , B05D1/18
CPC分类号： B27K3/20 , A01N59/16 , B27K3/163 , B27K3/22 , B27K3/32 , Y10S424/10 , Y10S424/11 , A01N59/14 , A01N59/00 , A01N25/22 , A01N25/02 , A01N2300/00
摘要： Compositions and methods are provided for treating wood products to provide leachresistant protection against fungal decay, termites and other wood destroying organisms. The preservative compositions provided include ammonia-stabilized solutions of zinc and boron, preferably in a molar ratio of Zn:B of between about 0.4:1 and 5:1, and are essentially copper free. The preservative may be applied by vacuum and/or pressure treatment or dip treatment under atmospheric pressure.
摘要翻译：提供了组合物和方法，用于处理木制品以提供抗真菌保护，防止真菌腐烂，白蚁和其他破坏木材的生物体。提供的防腐剂组合物包括锌稳定的锌和硼的溶液，优选的是Zn:B的摩尔比为约0.4:1至5:1，并且基本上不含铜。防腐剂可以通过在大气压下进行真空和/或压力处理或浸渍处理来施加。

5. 发明申请

US20090156073A1 FIRE RESISTANT CELLULOSIC MATERIALS AND METHOD OF MAKING THE SAME 失效
标题翻译：耐火纤维材料及其制备方法
公开(公告)号：US20090156073A1
公开(公告)日：2009-06-18
申请号：US12337494
申请日：2008-12-17
申请人： David M. Schubert
发明人： David M. Schubert
IPC分类号： C09K21/02 , B32B29/00 , B32B5/02
CPC分类号： C09K21/06 , Y10T428/2916 , Y10T428/31971 , Y10T428/31993 , Y10T442/2631 , Y10T442/2664
摘要： The invention relates to a fire resistant composition and a method of making fire resistant cellulosic materials comprising the fire resistant composition. More specifically, the invention relates to liquid compositions, including liquid compositions comprising urea and a boron-containing compound for imparting fire resistance to cellulosic products. The boron-containing compound typically comprises boric acids; borates (i.e., boric acid salts); boric oxides (i.e., any compound containing boron and oxygen), and mixtures thereof.
摘要翻译：本发明涉及耐火组合物和制备包含耐火组合物的耐火纤维素材料的方法。更具体地，本发明涉及液体组合物，包括含有尿素和用于赋予纤维素产品耐火性的含硼化合物的液体组合物。含硼化合物通常包含硼酸; 硼酸盐（即硼酸盐）; 硼氧化物（即含有硼和氧的任何化合物）及其混合物。

6. 发明授权

US06919036B2 Nonaborate compositions and their preparation 失效
标题翻译：无硼组合物及其制备
公开(公告)号：US06919036B2
公开(公告)日：2005-07-19
申请号：US10181628
申请日：2001-01-18
申请人： David M. Schubert
发明人： David M. Schubert
IPC分类号： C07D233/02 , A01N47/44 , A01N59/14 , B27K3/16 , B27K3/36 , C01B35/10 , C01B35/12 , C04B35/583 , C04B35/622 , C07C279/02 , C07F5/02 , C07F5/05 , C08K5/19 , C09K21/02 , C09K21/10 , C23F11/14 , C01B35/18 , A01N55/08 , C09K21/00
CPC分类号： C07F5/022 , A01N47/44 , A01N59/14 , C01B35/10 , C01B35/12 , C04B35/583 , C04B2235/3409 , C04B2235/386 , C08K5/19 , C09K21/02 , C23F11/146 , C23F11/149 , C08L23/10
摘要： A family of borate compounds containing an isolated (finite) nonaborate anion with the structural formula [B9O12(OH)6]3−. Preferred amine nonaborate compounds have a resolved oxide formula of A2O.3B2O3.2H2O, where A is the monovalent cation of an amine salt, such as guanidinium and imidazolium. Also provided is a method for preparing these compounds by crystallization from an aqueous solution under mild conditions without the formation of significant amounts of by-products. These compounds have potential application as precursors for the production of advanced boron nitride ceramic materials, and as flame retardants, corrosion inhibitors, and biocides.
摘要翻译：一种硼酸盐化合物，其含有具有结构式[B 9] 12（OH）6]的分离（有限）非硼酸阴离子 > 3 - 。优选的胺非硼酸化合物具有分解的氧化物分子式为A 2 O 3 B 2 O 3 N 2 O 2 B 2 O 2 其中A是胺盐的一价阳离子，例如胍和咪唑鎓。还提供了一种通过在温和条件下从水溶液中结晶而制备这些化合物而不形成大量副产物的方法。这些化合物可用作生产先进的氮化硼陶瓷材料以及作为阻燃剂，腐蚀抑制剂和杀生物剂的前体。

7. 发明授权

US08308997B2 Fire resistant cellulosic materials and method of making the same 失效
标题翻译：耐火纤维素材料及其制造方法
公开(公告)号：US08308997B2
公开(公告)日：2012-11-13
申请号：US12337494
申请日：2008-12-17
申请人： David M. Schubert
发明人： David M. Schubert
IPC分类号： C09K21/00 , B32B5/02
CPC分类号： C09K21/06 , Y10T428/2916 , Y10T428/31971 , Y10T428/31993 , Y10T442/2631 , Y10T442/2664
摘要： The invention relates to a fire resistant composition and a method of making fire resistant cellulosic materials comprising the fire resistant composition. More specifically, the invention relates to liquid compositions, including liquid compositions comprising urea and a boron -containing compound for imparting fire resistance to cellulosic products. The boron-containing compound typically comprises boric acids; borates (i.e., boric acid salts); boric oxides (i.e., any compound containing boron and oxygen), and mixtures thereof.
摘要翻译：本发明涉及耐火组合物和制备包含耐火组合物的耐火纤维素材料的方法。更具体地，本发明涉及液体组合物，包括含有尿素和含硼化合物的液体组合物，用于赋予纤维素产品耐火性。含硼化合物通常包含硼酸; 硼酸盐（即硼酸盐）; 硼氧化物（即含有硼和氧的任何化合物）及其混合物。

8. 发明授权

US5785939A Method for producing calcium borate 失效
标题翻译：硼酸钙生产方法
公开(公告)号：US5785939A
公开(公告)日：1998-07-28
申请号：US844481
申请日：1997-04-18
申请人： David M. Schubert
发明人： David M. Schubert
IPC分类号： C01B35/12
CPC分类号： C01B35/126
摘要： An improved method is provided for producing crystalline calcium hexaborate tetrahydrate, synthetic nobleite, by the reaction of boric acid and lime in an aqueous slurry. Reaction conditions include boric acid to water molar ratios of greater than 0.25:1, lime to boric acid molar ratios in the range of 0.05-0.15:1 and temperatures in the range of 60.degree.-85.degree. C. A concentration of at least 25% by weight undissolved solids is in the aqueous product slurry.
摘要翻译：提供了一种通过硼酸和石灰在含水浆料中反应生产结晶六硼酸钙四水合物，合成贵金属的改进方法。反应条件包括硼酸与水的摩尔比大于0.25:1，石灰与硼酸的摩尔比在0.05-0.15:1范围内，温度在60-85℃范围内。浓度至少为25 未溶解固体的重量％在水性产品浆料中。

9. 发明授权

US5688481A Method for producing calcium borate 失效
标题翻译：硼酸钙生产方法
公开(公告)号：US5688481A
公开(公告)日：1997-11-18
申请号：US544518
申请日：1995-10-18
申请人： David M. Schubert
发明人： David M. Schubert
IPC分类号： C01B35/12
CPC分类号： C01B35/126
摘要： An improved method is provided for producing crystalline calcium hexaborate tetrahydrate, synthetic nobleite, by the reaction of boric acid and lime in an aqueous slurry. Reaction conditions include boric acid to water molar ratios of greater than 0.25:1, lime to boric acid molar ratios in the range of 0.05-0.15:1 and temperatures in the range of 85.degree.-105.degree. C. A novel crystalline product is produced having a unique crystal habit resulting in improved physical properties. Dehydration of this product produced a novel amorphous, anhydrous product having similar crystal habit and physical properties.
摘要翻译：提供了一种通过硼酸和石灰在含水浆料中反应生产结晶六硼酸钙四水合物，合成贵金属的改进方法。反应条件包括硼酸与水的摩尔比大于0.25:1，石灰与硼酸摩尔比在0.05-0.15:1范围内，温度在85-105℃范围内。产生新的结晶产物具有独特的晶体习性，从而改善物理性能。该产品的脱水产生了具有类似晶体习性和物理性质的新型无定形无水产品。

10. 发明授权

US5472644A Zinc borate 失效
标题翻译：硼酸锌
公开(公告)号：US5472644A
公开(公告)日：1995-12-05
申请号：US258163
申请日：1994-06-10
申请人： David M. Schubert
发明人： David M. Schubert
IPC分类号： C01B35/12 , C09C1/00 , C08K3/22 , C08K3/38 , C08L83/00 , C08L101/00 , C09D5/00 , C09D5/08 , C09D5/18 , C09K21/02 , C23F11/00
CPC分类号： C01B35/12 , C08K3/38 , C09D5/084
摘要： Zinc borate compositions having a ZnO:B.sub.2 O.sub.3 ratio of 4:1. The hydrated zinc borate 4ZnO.B.sub.2 O.sub.3.H.sub.2 O and anhydrous zinc borate 4ZnO.B.sub.2 O.sub.3 are especially useful as fire-retardants and smoke-suppressant additives for polymeric compositions.
摘要翻译：具有ZnO：B2O3比为4:1的硼酸锌组合物。水合硼酸锌4ZnO.B2O3.H2O和无水硼酸锌4ZnO.B2O3特别用作聚合物组合物的阻燃剂和防烟添加剂。

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