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    • 1. 发明授权
    • Technological method for preparing sponge titanium from sodium fluotitanate raw material
    • 从氟酸钠原料制备海绵钛的技术方法
    • US08871002B2
    • 2014-10-28
    • US13585783
    • 2012-08-14
    • Xuemin ChenJun YangZhi Zhou
    • Xuemin ChenJun YangZhi Zhou
    • C22B34/12
    • C22B34/1277C22B34/1272
    • The invention provides a technological method for preparing sponge titanium from sodium fluotitanate raw material, comprising the following steps: step A: placing aluminum in an airtight resistance furnace, evacuating, introducing inert gas into the resistance furnace, and heating the aluminum to obtain molten aluminum; step B: opening a reactor cover, adding a proper amount of sodium fluotitanate into the reactor, closing the reactor cover, detecting leakage, slowly heating the reactor to 150° C., evacuating and continuously heating the reactor to 250° C.; step C: introducing inert gas into the reactor, continuously heating the reactor to 900° C., and stirring uniformly; step D: opening a valve, adjusting the stirring speed, dripping the molten aluminum, and controlling the temperature of reaction in a range from 900 to 1000° C.; and step E: opening the reactor cover, removing a stirring device out of the reactor, and eliminating NaAlF4 at upper layer to obtain sponge titanium.
    • 本发明提供了一种由氟钛酸钠原料制备海绵钛的技术方法,包括以下步骤:步骤A:将铝放置在密封电阻炉中,抽真空,将惰性气体引入电阻炉,并加热铝以获得熔融铝 ; 步骤B:打开反应器盖,向反应器中加入适量的氟钛酸钠,关闭反应器盖,检测泄漏,将反应器缓慢加热至150℃,抽空并连续加热反应器至250℃。 步骤C:将惰性气体引入反应器,将反应器连续加热至900℃,均匀搅拌; 步骤D:打开阀门,调节搅拌速度,滴入熔融铝,并将反应温度控制在900至1000℃的范围内。 步骤E:打开反应器盖,从反应器中取出搅拌装置,除去上层的NaAlF4,得到海绵钛。
    • 2. 发明授权
    • Process for producing sponge titanium
    • 海绵钛生产工艺
    • US08876938B2
    • 2014-11-04
    • US13585717
    • 2012-08-14
    • Xuemin ChenJun YangZhi Zhou
    • Xuemin ChenJun YangZhi Zhou
    • C22B34/12
    • C22B34/1277C22B34/1272
    • The present invention provides a process for producing sponge titanium, which includes the following steps: Step A: placing aluminum into a resistance furnace, vacuum pumping, introducing inert gas, heating to molten aluminum; Step B: opening a reactor cover, adding a proper amount of potassium fluotitanate to a reactor, leakage detecting after closing the reactor cover, slowly raising the temperature to 150° C., vacuum pumping, and continuously heating to 250° C.; Step C: introducing inert gas into the reactor, continuously raising the temperature to 750° C., stirring uniformly; Step D: opening a valve to adjust the stirring speed, adding molten aluminum drops, and controlling the reaction temperature to 750° C. to 850° C.; Step E: opening the reactor cover, removing a stirring device, eliminating the upper layer of KAlF4 to obtain sponge titanium. The present invention has the beneficial effects of short process flow, low cost, environmental protection and harmlessness.
    • 本发明提供一种生产海绵钛的方法,其包括以下步骤:步骤A:将铝放入电阻炉中,真空泵送,引入惰性气体,加热至熔融铝; 步骤B:打开反应器盖,向反应器中加入适量的氟钛酸钾,关闭反应器盖后进行泄漏检测,缓慢升温至150℃,真空泵送,并连续加热至250℃。 步骤C:将惰性气体引入反应器,将温度持续升至750℃,均匀搅拌; 步骤D:打开阀门以调节搅拌速度,加入熔融的铝滴,并将反应温度控制在750℃至850℃; 步骤E:打开反应器盖,取出搅拌装置,取出上层的KAlF4,得到海绵钛。 本发明具有工艺流程短,成本低,环保和无害化的有益效果。
    • 6. 发明授权
    • Method for preparing sponge titanium from potassium fluotitanate by aluminothermic reduction
    • 通过铝热还原从氟酸钾制备海绵钛的方法
    • US08864873B2
    • 2014-10-21
    • US13585721
    • 2012-08-14
    • Xuemin ChenJun YangZhi Zhou
    • Xuemin ChenJun YangZhi Zhou
    • C22B34/00C22B34/12
    • C22B34/1277
    • The invention provides a method for preparing sponge titanium from potassium fluotitanate by aluminothermic reduction, comprising the following steps: a reaction step: aluminum and zinc are mixed under a vacuum state, and the mixture is then reacted with potassium fluotitanate; a distillation step: KF, AlF3 and Zn generated by reaction are distilled out under a vacuum state; and a cooling step: sponge titanium is obtained subsequent to banking cooling. The invention further provides another method for preparing sponge titanium from potassium fluotitanate by aluminothermic reduction, comprising the following steps: a reaction step: aluminum and magnesium are mixed under a vacuum argon introduction condition, and the mixture is then reacted with potassium fluotitanate; a distillation step: KF, AlF3, MgF2 and Mg generated by reaction are distilled out under a vacuum state; and a cooling step: sponge titanium is obtained subsequent to banking cooling.
    • 本发明提供了一种通过铝热还原从氟酸钾制备海绵钛的方法,包括以下步骤:反应步骤:将铝和锌在真空状态下混合,然后使该混合物与氟钛酸钾反应; 蒸馏步骤:在真空状态下蒸馏出由反应产生的KF,AlF 3和Zn; 和冷却步骤:在银行冷却之后获得海绵钛。 本发明还提供另一种通过铝热还原由氟钛酸钾制备海绵钛的方法,包括以下步骤:反应步骤:在真空氩气引入条件下将铝和镁混合,然后使该混合物与氟钛酸钾反应; 蒸馏步骤:在真空状态下蒸馏出由反应产生的KF,AlF 3,MgF 2和Mg; 和冷却步骤:在银行冷却之后获得海绵钛。
    • 10. 发明授权
    • Method and system for improved fault tolerance in distributed customization controls using non-volatile memory
    • 使用非易失性存储器的分布式定制控制中改进容错的方法和系统
    • US09497022B2
    • 2016-11-15
    • US11558360
    • 2006-11-09
    • Iue-Shuenn ChenXuemin Chen
    • Iue-Shuenn ChenXuemin Chen
    • H04L29/06H04L9/00
    • H04L9/004H04L2209/12
    • Certain aspects of a method and system for improved fault tolerance in distributed customization controls using non-volatile memory are disclosed. Aspects of one method may include mapping an input control signal to a plurality of input logic circuits within a security processor. A plurality of independent processing paths may be defined between each of the plurality of input logic circuits and an output logic circuit. Each of the plurality of independent processing paths may comprise one or more logic circuits. The input control signal may be routed via at least a portion of the plurality of independent processing paths. The portion of the plurality of independent processing paths may be combined in the output logic circuit to generate the input control signal.
    • 公开了使用非易失性存储器的分布式定制控制中用于改进容错的方法和系统的某些方面。 一种方法的方面可以包括将输入控制信号映射到安全处理器内的多个输入逻辑电路。 可以在多个输入逻辑电路中的每一个和输出逻辑电路之间定义多个独立的处理路径。 多个独立处理路径中的每一个可以包括一个或多个逻辑电路。 输入控制信号可以经由多个独立处理路径的至少一部分路由。 多个独立处理路径的部分可以组合在输出逻辑电路中以产生输入控制信号。