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1. 发明授权

US08246933B2 Aerosol method for nano silver-silica composite anti-microbial agent 有权
标题翻译：纳米银二氧化硅复合抗菌剂气溶胶法
公开(公告)号：US08246933B2
公开(公告)日：2012-08-21
申请号：US12324318
申请日：2008-11-26
申请人： Xingmao Jiang , C. Jeffrey Brinker , Yong Lin , Yung-Sung Cheng
发明人： Xingmao Jiang , C. Jeffrey Brinker , Yong Lin , Yung-Sung Cheng
IPC分类号： A61K9/14 , A01N59/16
CPC分类号： A61K33/38 , A01N59/16 , A61K9/5115 , A61K9/5192 , A01N25/06 , A01N25/34 , A01N2300/00
摘要： A method of forming and resulting nano-structured composite includes atomizing a mixture of an amount of each of aminopropyltriethoxysilane, AgNO3, DI water, and ethanol in a carrier gas; heating the atomized droplets at a selected temperature for a time sufficient to reduce the Ag to its elemental form in a silica matrix; and outputting the nano structured composite particles. A predetermined heating time is from about 0.01 to about 40 seconds and a selected heating temperature is from about 200 to about 800° C. The nano structured composite includes a plurality of nano particles at a contact surface of the composite, dispersed throughout and at a contact surface of the composite, or dispersed throughout the composite.
摘要翻译：形成和得到的纳米结构复合材料的方法包括在载气中雾化一定量的氨基丙基三乙氧基硅烷，AgNO 3，去离子水和乙醇的混合物; 在所选择的温度下加热雾化的液滴足以将Ag还原成二氧化硅基质中其元素的时间; 并输出纳米结构复合颗粒。预定的加热时间为约0.01至约40秒，选定的加热温度为约200至约800℃。纳米结构复合材料包括在复合材料的接触表面处的多个纳米颗粒，分散在整个和复合材料的接触表面，或分散在整个复合材料中。

2. 发明授权

US08318127B1 Methods for preparing high crystallinity and surface area porous metal oxides 有权
标题翻译：制备高结晶度和表面积多孔金属氧化物的方法
公开(公告)号：US08318127B1
公开(公告)日：2012-11-27
申请号：US13033232
申请日：2011-02-23
申请人： Xingmao Jiang , C. Jeffrey Brinker
发明人： Xingmao Jiang , C. Jeffrey Brinker
IPC分类号： C01F7/00
CPC分类号： C01F17/0043 , C01F7/30 , C01G23/0536 , C01P2002/72 , C01P2006/12 , C01P2006/16
摘要： Exemplary embodiments provide materials and methods of forming a metal oxide composite and a porous metal oxide, which can be used for applications including catalysis, sensors, energy storage, solar cells, heavy metal removal and separations, etc. In one embodiment, a one-step solvothermal process can be used to form the metal oxide phase with high crystallinity and high surface area.
摘要翻译：示例性实施例提供形成金属氧化物复合材料和多孔金属氧化物的材料和方法，其可用于包括催化，传感器，储能，太阳能电池，重金属去除和分离等的应用。在一个实施方案中，可以使用步骤溶剂热法形成具有高结晶度和高表面积的金属氧化物相。

3. 发明授权

US08992984B1 Protocells and their use for targeted delivery of multicomponent cargos to cancer cells 有权
标题翻译：原核细胞及其用于将多组分货物靶向递送至癌细胞的用途
公开(公告)号：US08992984B1
公开(公告)日：2015-03-31
申请号：US12909572
申请日：2010-10-21
申请人： C. Jeffrey Brinker , Carlee Erin Ashley , Xingmao Jiang , Juewen Liu , David S. Peabody , Walker Richard Wharton , Eric Carnes , Bryce Chackerian , Cheryl L. Willman
发明人： C. Jeffrey Brinker , Carlee Erin Ashley , Xingmao Jiang , Juewen Liu , David S. Peabody , Walker Richard Wharton , Eric Carnes , Bryce Chackerian , Cheryl L. Willman
IPC分类号： A61K9/14 , A61K9/51
CPC分类号： A61K9/127 , A61K9/1277 , A61K9/5115 , A61K9/5123 , A61K31/513 , A61K31/575 , A61K31/704 , A61K33/24 , A61K49/005
摘要： Various embodiments provide materials and methods for synthesizing protocells for use in targeted delivery of cargo components to cancer cells. In one embodiment, the lipid bilayer can be fused to the porous particle core to form a protocell. The lipid bilayer can be modified with targeting ligands or other ligands to achieve targeted delivery of cargo components that are loaded within the protocell to a target cell, e.g., a type of cancer. Shielding materials can be conjugated to the surface of the lipid bilayer to reduce undesired non-specific binding.
摘要翻译：各种实施方案提供用于合成原细胞以用于向癌细胞靶向递送货物组分的材料和方法。在一个实施方案中，脂质双层可以与多孔颗粒核心融合以形成原细胞。脂质双层可以用靶向配体或其他配体进行修饰，以实现载体在原细胞内的货物组分的靶向递送到靶细胞，例如一种类型的癌症。屏蔽材料可以结合到脂质双层的表面以减少不期望的非特异性结合。

4. 发明授权

US08501057B1 Freezing assisted fabrication of nano and micro hollow cubic metal oxides 有权
标题翻译：冷冻辅助制造纳米和微型中空立方体氧化物
公开(公告)号：US08501057B1
公开(公告)日：2013-08-06
申请号：US13010121
申请日：2011-01-20
申请人： Xingmao Jiang , C. Jeffrey Brinker
发明人： Xingmao Jiang , C. Jeffrey Brinker
IPC分类号： B29C35/02
CPC分类号： C01B33/163 , B82Y30/00 , C01B13/328 , C01P2004/38 , C01P2004/62 , C01P2004/64
摘要： Various embodiments provide materials and methods of forming hollow cubes. The hollow cubes can be formed to include a metal oxide shell layer encasing a cubic hollow space. In one embodiment, the hollow cubes can be formed from an emulsion having aqueous droplets with an interfacial layer encasing an aqueous core. By an exemplary freezing treatment, the aqueous droplets having a spherical shape can be transformed into ice components having a cubic shape. Metal oxide precursors can then be added to react with the encased cube-shaped ice core at the interface with the interfacial layer to form a sol-gel metal oxide shell layer. Hollow cubes can be formed by removing the cube-shaped ice core from the sol-gel metal oxide shell layer.
摘要翻译：各种实施例提供了形成中空立方体的材料和方法。中空立方体可以形成为包括包围立方中空空间的金属氧化物壳层。在一个实施例中，中空立方体可以由具有包含水性芯的界面层的水性液滴的乳液形成。通过示例性的冷冻处理，具有球形形状的水滴可以转变成具有立方体形状的冰组分。然后可以加入金属氧化物前体以与包封的立方体冰芯在与界面层的界面处反应以形成溶胶 - 凝胶金属氧化物壳层。可以通过从溶胶 - 凝胶金属氧化物壳层去除立方体状的冰芯来形成空心立方体。

5. 发明授权

US08864045B1 Aerosol fabrication methods for monodisperse nanoparticles 有权
标题翻译：单分散纳米粒子的气溶胶制备方法
公开(公告)号：US08864045B1
公开(公告)日：2014-10-21
申请号：US13300069
申请日：2011-11-18
申请人： Xingmao Jiang , C. Jeffrey Brinker
发明人： Xingmao Jiang , C. Jeffrey Brinker
IPC分类号： B05B1/24
CPC分类号： B05B1/24 , B22F1/0018 , B22F1/02 , B22F9/06 , B22F2001/0092 , C01B13/34 , C01B21/06 , C01P2004/32 , C01P2004/34 , C01P2004/64 , C22C2202/02 , C23C18/08 , C23C18/1204 , C23C18/1241 , C23C18/1245 , C23C18/127 , C23C18/1295
摘要： Exemplary embodiments provide materials and methods for forming monodisperse particles. In one embodiment, the monodisperse particles can be formed by first spraying a nanoparticle-containing dispersion into aerosol droplets and then heating the aerosol droplets in the presence of a shell precursor to form core-shell particles. By removing either the shell layer or the nanoparticle core of the core-shell particles, monodisperse nanoparticles can be formed.
摘要翻译：示例性实施方案提供了用于形成单分散颗粒的材料和方法。在一个实施方案中，单分散颗粒可以通过首先将含纳米颗粒的分散体喷雾到气溶胶液滴中，然后在壳前体的存在下加热气溶胶液滴形成核 - 壳颗粒来形成。通过去除核 - 壳颗粒的壳层或纳米颗粒芯，可以形成单分散纳米颗粒。

6. 发明授权

US07744673B2 Hollow sphere metal oxides 有权
标题翻译：中空球体金属氧化物
公开(公告)号：US07744673B2
公开(公告)日：2010-06-29
申请号：US11876338
申请日：2007-10-22
申请人： Xingmao Jiang , Charles Jeffrey Brinker
发明人： Xingmao Jiang , Charles Jeffrey Brinker
IPC分类号： B22F9/24
CPC分类号： B01J13/0095 , B01J13/02 , B22F3/1112 , B22F2001/0029 , B22F2998/00 , B22F2999/00 , B22F1/0018 , B22F9/22 , B22F2201/013
摘要： In accordance with invention, there are methods for fabricating hollow spheres and nanofoams. The method for making hollow spheres can include providing a homogeneous precursor solution including a first solvent and one or more anhydrous precursor species and forming aerosol droplets having a first size distribution using the homogeneous precursor solution in an anhydrous carrier gas. The method can also include transporting the aerosol droplets through an aerosol reactor including a reactant to form a plurality of hollow spheres, wherein each of the plurality of hollow spheres can be formed by one or more chemical reactions occurring at a surface of the aerosol droplet. The method can further include controlling size and thickness of the hollow spheres by one or more of the precursor solution concentration, aerosol droplet size, temperature, residence time of the aerosol droplets in the aerosol reactor, and the reactant distribution in the aerosol reactor.
摘要翻译：根据本发明，存在制造中空球体和纳米烟雾的方法。制备中空球体的方法可以包括提供包含第一溶剂和一种或多种无水前体物质的均匀前体溶液，并使用均匀的前体溶液在无水载气中形成具有第一尺寸分布的气雾剂液滴。该方法还可以包括通过包括反应物的气溶胶反应器运送气溶胶液滴以形成多个中空球体，其中多个中空球体中的每一个可以通过在气溶胶液滴的表面处发生的一个或多个化学反应形成。该方法还可以包括通过前体溶液浓度，气溶胶液滴尺寸，温度，气溶胶微滴在气溶胶反应器中的停留时间以及气溶胶反应器中的反应物分布中的一种或多种来控制中空球的尺寸和厚度。

7. 发明申请

US20080210053A1 HOLLOW SPHERE METAL OXIDES 有权
标题翻译：中空球状金属氧化物
公开(公告)号：US20080210053A1
公开(公告)日：2008-09-04
申请号：US11876338
申请日：2007-10-22
申请人： Xingmao Jiang , Charles Jeffrey Brinker
发明人： Xingmao Jiang , Charles Jeffrey Brinker
IPC分类号： B22F9/16 , B01J2/04
CPC分类号： B01J13/0095 , B01J13/02 , B22F3/1112 , B22F2001/0029 , B22F2998/00 , B22F2999/00 , B22F1/0018 , B22F9/22 , B22F2201/013
摘要： In accordance with invention, there are methods for fabricating hollow spheres and nanofoams. The method for making hollow spheres can include providing a homogeneous precursor solution including a first solvent and one or more anhydrous precursor species and forming aerosol droplets having a first size distribution using the homogeneous precursor solution in an anhydrous carrier gas. The method can also include transporting the aerosol droplets through an aerosol reactor including a reactant to form a plurality of hollow spheres, wherein each of the plurality of hollow spheres can be formed by one or more chemical reactions occurring at a surface of the aerosol droplet. The method can further include controlling size and thickness of the hollow spheres by one or more of the precursor solution concentration, aerosol droplet size, temperature, residence time of the aerosol droplets in the aerosol reactor, and the reactant distribution in the aerosol reactor.
摘要翻译：根据本发明，存在制造中空球体和纳米烟雾的方法。制备中空球体的方法可以包括提供包含第一溶剂和一种或多种无水前体物质的均匀前体溶液，并使用均匀的前体溶液在无水载气中形成具有第一尺寸分布的气雾剂液滴。该方法还可以包括通过包括反应物的气溶胶反应器运送气雾剂液滴以形成多个中空球体，其中多个中空球体中的每一个可以通过在气溶胶液滴的表面处发生的一个或多个化学反应形成。该方法还可以包括通过前体溶液浓度，气溶胶液滴尺寸，温度，气溶胶微滴在气溶胶反应器中的停留时间以及气溶胶反应器中的反应物分布中的一种或多种来控制中空球的尺寸和厚度。

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