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1. 发明授权

US07531149B2 Synthetic control of metal oxide nanocrystal sizes and shapes 有权
标题翻译：金属氧化物纳米晶体尺寸和形状的合成控制
公开(公告)号：US07531149B2
公开(公告)日：2009-05-12
申请号：US11204766
申请日：2005-08-16
申请人： Xiaogang Peng , Yongfen Chen , Nikhil Jana , Arun Narayanaswamy
发明人： Xiaogang Peng , Yongfen Chen , Nikhil Jana , Arun Narayanaswamy
IPC分类号： B23B5/16 , C01G5/00 , C01G7/00 , C01G51/00 , C01G55/00
CPC分类号： C01B13/18 , B82Y25/00 , B82Y30/00 , C01G1/02 , C01G9/02 , C01G15/00 , C01G19/00 , C01G19/02 , C01G37/02 , C01G49/02 , C01G49/08 , C01G53/04 , C01P2002/72 , C01P2002/82 , C01P2002/84 , C01P2004/04 , C01P2004/52 , C01P2004/64 , H01F1/0054 , Y10S977/777 , Y10S977/811 , Y10T428/2982
摘要： A general, reproducible, and simple synthetic method that employs readily available chemicals permits control of the size, shape, and size distribution of metal oxide nanocrystals. The synthesis entails reacting a metal fatty acid salt, the corresponding fatty acid, and a hydrocarbon solvent, with the reaction product being pyrolyzed to the metal oxide. Nearly monodisperse oxide nanocrystals of Fe3O4, Cr2O3, MnO, Co3O4, NiO, ZnO, SnO2, and In2O3, in a large size range (3-50 nm), are described. Size and shape control of the nanocrystals is achieved by varying the reactivity and concentration of the precursors.
摘要翻译：使用容易获得的化学品的一般的，可重现的和简单的合成方法允许控制金属氧化物纳米晶体的尺寸，形状和尺寸分布。合成需要使金属脂肪酸盐，相应的脂肪酸和烃溶剂反应，反应产物被热解成金属氧化物。描述了大尺寸范围（3-50nm）中的Fe 3 O 4，Cr 2 O 3，MnO，Co 3 O 4，NiO，ZnO，SnO 2和In 2 O 3的近似单分散氧化物纳米晶体。通过改变前体的反应性和浓度来实现纳米晶体的尺寸和形状控制。

2. 发明申请

US20060211152A1 Synthetic control of metal oxide nanocrystal sizes and shapes 有权
标题翻译：金属氧化物纳米晶体尺寸和形状的合成控制
公开(公告)号：US20060211152A1
公开(公告)日：2006-09-21
申请号：US11204766
申请日：2005-08-16
申请人： Xiaogang Peng , Yongfen Chen , Nikhil Jana , Arun Narayanaswamy
发明人： Xiaogang Peng , Yongfen Chen , Nikhil Jana , Arun Narayanaswamy
IPC分类号： H01L21/00
CPC分类号： C01B13/18 , B82Y25/00 , B82Y30/00 , C01G1/02 , C01G9/02 , C01G15/00 , C01G19/00 , C01G19/02 , C01G37/02 , C01G49/02 , C01G49/08 , C01G53/04 , C01P2002/72 , C01P2002/82 , C01P2002/84 , C01P2004/04 , C01P2004/52 , C01P2004/64 , H01F1/0054 , Y10S977/777 , Y10S977/811 , Y10T428/2982
摘要： A general, reproducible, and simple synthetic method that employs readily available chemicals permits control of the size, shape, and size distribution of metal oxide nanocrystals. The synthesis entails reacting a metal fatty acid salt, the corresponding fatty acid, and a hydrocarbon solvent, with the reaction product being pyrolyzed to the metal oxide. Nearly monodisperse oxide nanocrystals of Fe3O4, Cr2O3, MnO, Co3O4, NiO, ZnO, SnO2, and In2O3, in a large size range (3-50 nm), are described. Size and shape control of the nanocrystals is achieved by varying the reactivity and concentration of the precursors.
摘要翻译：使用容易获得的化学品的一般的，可重现的和简单的合成方法允许控制金属氧化物纳米晶体的尺寸，形状和尺寸分布。合成需要使金属脂肪酸盐，相应的脂肪酸和烃溶剂反应，反应产物被热解成金属氧化物。 Fe 3 O 4，Cr 2 O 3 3，MnO 3，Co 3的几乎单分散的氧化物纳米晶体 O 4，N 4，NiO，ZnO，SnO 2，和In 2 O 3 3，在描述了大尺寸范围（3-50nm）。通过改变前体的反应性和浓度来实现纳米晶体的尺寸和形状控制。

3. 发明授权

US08679543B2 Stable indium-containing semiconductor nanocrystals 有权
标题翻译：稳定的含铟半导体纳米晶体
公开(公告)号：US08679543B2
公开(公告)日：2014-03-25
申请号：US13002035
申请日：2009-07-02
申请人： Joseph Bartel , Yongfen Chen , Eric Tulsky , Joseph Treadway
发明人： Joseph Bartel , Yongfen Chen , Eric Tulsky , Joseph Treadway
IPC分类号： A61K9/14
CPC分类号： G01N21/6486 , B82Y5/00 , B82Y15/00 , C01B25/082 , C09K11/02 , C09K11/565 , C09K11/70 , C30B7/00 , C30B29/40 , C30B29/48 , C30B29/60 , G01N33/588 , H01L21/02392 , H01L21/02557 , H01L21/02601 , H01L21/02628 , H01L33/06
摘要： Nanocrystals having an indium-based core and methods for making them and using them to construct core-shell nanocrystals are described. These core-shell nanocrystals are highly stable and provide higher quantum yields than known nanocrystals of similar composition, and they provide special advantages for certain applications because of their small size.
摘要翻译：描述了具有铟基核的纳米晶体及其制备方法和用于构建核壳纳米晶体的方法。这些核 - 壳纳米晶体是高度稳定的并且提供比已知具有类似组成的纳米晶体更高的量子产率，并且由于它们的小尺寸，它们为某些应用提供了特殊的优点。

4. 发明申请

US20110223110A1 STABLE INDIUM-CONTAINING SEMICONDUCTOR NANOCRYSTALS 有权
标题翻译：稳定的包含半导体纳米晶体的纳米晶体
公开(公告)号：US20110223110A1
公开(公告)日：2011-09-15
申请号：US13002035
申请日：2009-07-02
申请人： Joseph Bartel , Yongfen Chen , Eric Tulsky , Joseph Treadway
发明人： Joseph Bartel , Yongfen Chen , Eric Tulsky , Joseph Treadway
IPC分类号： A61K49/00 , H01L21/34 , H01L33/06 , H01L29/15 , G01N21/64 , C12Q1/02 , C40B30/00 , B82Y40/00 , B82Y99/00
CPC分类号： G01N21/6486 , B82Y5/00 , B82Y15/00 , C01B25/082 , C09K11/02 , C09K11/565 , C09K11/70 , C30B7/00 , C30B29/40 , C30B29/48 , C30B29/60 , G01N33/588 , H01L21/02392 , H01L21/02557 , H01L21/02601 , H01L21/02628 , H01L33/06
摘要： Nanocrystals having an indium-based core and methods for making them and using them to construct core-shell nanocrystals are described. These core-shell nanocrystals are highly stable and provide higher quantum yields than known nanocrystals of similar composition, and they provide special advantages for certain applications because of their small size.
摘要翻译：描述了具有铟基核的纳米晶体及其制备方法和用于构建核壳纳米晶体的方法。这些核 - 壳纳米晶体是高度稳定的并且提供比已知具有类似组成的纳米晶体更高的量子产率，并且由于它们的小尺寸，它们为某些应用提供了特殊的优点。

5. 发明授权

US09577037B2 Nanocrystals with high extinction coefficients and methods of making and using such nanocrystals 有权
标题翻译：具有高消光系数的纳米晶体和制备和使用这种纳米晶体的方法
公开(公告)号：US09577037B2
公开(公告)日：2017-02-21
申请号：US13997598
申请日：2011-12-23
申请人： Eric Welch , Joseph Bartel , Eric Tulsky , Joseph Treadway , Yongfen Chen
发明人： Eric Welch , Joseph Bartel , Eric Tulsky , Joseph Treadway , Yongfen Chen
IPC分类号： C09K11/08 , B82Y30/00 , H01L29/06 , C30B7/00 , C30B29/40 , C30B29/48 , C30B29/60 , G01N33/533 , H01L51/00 , H01L21/02 , C09K11/56 , C09K11/57 , C09K11/02 , B82Y15/00 , G01N33/58 , B82Y40/00 , B82Y20/00
CPC分类号： H01L29/0665 , B82Y20/00 , B82Y30/00 , B82Y40/00 , C30B7/00 , C30B29/40 , C30B29/48 , C30B29/60 , G01N33/533 , G01N33/588 , H01L21/02628 , H01L31/035209 , H01L33/04 , H01L51/0007
摘要： A population of bright and stable nanocrystals is provided. The nanocrystals include a semiconductor core and a thick semiconductor shell and can exhibit high extinction coefficients, high quantum yields, and limited or no detectable blinking.
摘要翻译：提供了一群明亮稳定的纳米晶体。纳米晶体包括半导体芯和厚半导体外壳，并且可以表现出高消光系数，高量子产率以及有限或无可检测的闪烁。

6. 发明申请

US20130295586A1 PREPARATION OF NANOCRYSTALS WITH MIXTURES OF ORGANIC LIGANDS 审中-公开
标题翻译：用有机配体混合物制备纳米晶体
公开(公告)号：US20130295586A1
公开(公告)日：2013-11-07
申请号：US13976621
申请日：2011-12-23
申请人： Joseph August Bartel , Yongfen Chen , Noah Lermer , Timothy Carter , Scott Sweeney , Chad Teters , Wenxi Huang
发明人： Joseph August Bartel , Yongfen Chen , Noah Lermer , Timothy Carter , Scott Sweeney , Chad Teters , Wenxi Huang
IPC分类号： G01N33/533 , H01L51/00
CPC分类号： H01L29/0665 , B82Y20/00 , B82Y30/00 , B82Y40/00 , C30B7/00 , C30B29/40 , C30B29/48 , C30B29/60 , G01N33/533 , G01N33/588 , H01L21/02628 , H01L31/035209 , H01L33/04 , H01L51/0007
摘要： Semiconductor nanocrystals prepared using a mixture of organic ligands (e.g., oxoacids), as well as compositions, kits, and methods of using such semiconductor nanocrystals are disclosed.
摘要翻译：公开了使用有机配体（例如含氧酸）的混合物制备的半导体纳米晶体，以及组合物，试剂盒和使用这种半导体纳米晶体的方法。

7. 发明申请

US20100112716A1 SYNTHESIS OF NANOASSEMBLIES CONTAINING LUMINESCENT QUANTUM DOTS AND MAGNETIC NANOPARTICLES 失效
标题翻译：含有发光量子点和磁性纳米粒子的纳米粒子的合成
公开(公告)号：US20100112716A1
公开(公告)日：2010-05-06
申请号：US11088242
申请日：2005-03-23
申请人： Zeev Rosenzweig , Yongfen Chen , Desheng Wang
发明人： Zeev Rosenzweig , Yongfen Chen , Desheng Wang
IPC分类号： G01N21/76 , G01N33/68 , G01N33/574
CPC分类号： G01N21/6489 , B82Y15/00 , B82Y30/00 , G01N21/6428 , G01N33/533 , G01N33/57415 , G01N33/588 , Y10S977/773 , Y10S977/783 , Y10S977/824 , Y10S977/83 , Y10S977/834 , Y10S977/838 , Y10T428/2982 , Y10T428/2991 , Y10T428/2998
摘要： Negatively charged luminescent CdSe—ZnS quantum dots (QDs) were successfully incorporated into novel luminescent glyconanospheres averaging around 190 nm in diameter through electrostatic interactions with carboxymethyldextran (CM-dextran) and polylysine. The glyconanospheres preferably contain as well carboxyl-modified iron oxide nanocrystals. In addition to electrostatic attraction between the negatively charged dextran, the negatively charged CdSe—ZnS QDs (and negatively charged iron oxide nanocrystals, if present), and the positively charged polylysine, covalent amide bonds were introduced to cross link the QDs (and negatively charged iron oxide nanocrystals, if present) with the polysaccharide matrix to further stabilize the glyconanospheres. The dextran residues on the surface of the nanospheres show high affinity toward the glucose binding protein-Concanavalin A (Con A). As a result, these luminescent CdSe—ZnS QD incorporated glyconanospheres are a useful tool for studying carbohydrate-protein interactions that are critical steps in bacterial and viral infection.
摘要翻译：通过与羧甲基葡聚糖（CM-葡聚糖）和聚赖氨酸的静电相互作用，将带负电的发光CdSe-ZnS量子点（QDs）成功地并入平均约190nm直径的新型发光糖球中。优选地，葡萄球藻中含有羧基改性的氧化铁纳米晶体。除了带负电荷的葡聚糖之间的静电吸引，带负电荷的CdSe-ZnS量子点（和带负电荷的氧化铁纳米晶体，如果存在）和带正电荷的聚赖氨酸，引入共价酰胺键以交联QD（和带负电荷的氧化铁纳米晶体（如果存在）与多糖基质一起进一步稳定糖藻球。纳米球表面的葡聚糖残基对葡萄糖结合蛋白 - 伴刀豆球蛋白A（Con A）表现出高亲和力。结果，这些发光的CdSe-ZnS QD掺入的糖藻球是研究碳水化合物 - 蛋白质相互作用的有用工具，这是细菌和病毒感染的关键步骤。

8. 发明授权

US10224398B2 Preparation of nanocrystals with mixtures of organic ligands 有权
公开(公告)号：US10224398B2
公开(公告)日：2019-03-05
申请号：US13976621
申请日：2011-12-23
申请人： Joseph Bartel , Yongfen Chen , Noah Lermer , Timothy Carter , Scott Sweeney , Chad Teters , Wenxi Huang
发明人： Joseph Bartel , Yongfen Chen , Noah Lermer , Timothy Carter , Scott Sweeney , Chad Teters , Wenxi Huang
IPC分类号： H01L29/06 , G01N33/58 , B82Y30/00 , C30B7/00 , C30B29/40 , C30B29/48 , C30B29/60 , G01N33/533 , H01L51/00 , H01L21/02 , H01L31/0352 , H01L33/04 , B82Y40/00 , B82Y20/00
摘要： Semiconductor nanocrystals prepared using a mixture of organic ligands (e.g., oxoacids), as well as compositions, kits, and methods of using such semiconductor nanocrystals are disclosed.

9. 发明申请

US20140001436A1 NANOCRYSTALS WITH HIGH EXTINCTION COEFFICIENTS AND METHODS OF MAKING AND USING SUCH NANOCRYSTALS 有权
标题翻译：具有高放电系数的纳米晶体及其制备和使用这种纳米晶体的方法
公开(公告)号：US20140001436A1
公开(公告)日：2014-01-02
申请号：US13997598
申请日：2011-12-23
申请人： Eric Welch , Joseph Bartel , Eric Tulsky , Joseph Treadway , Yongfen Chen
发明人： Eric Welch , Joseph Bartel , Eric Tulsky , Joseph Treadway , Yongfen Chen
IPC分类号： H01L29/06 , H01L21/02
CPC分类号： H01L29/0665 , B82Y20/00 , B82Y30/00 , B82Y40/00 , C30B7/00 , C30B29/40 , C30B29/48 , C30B29/60 , G01N33/533 , G01N33/588 , H01L21/02628 , H01L31/035209 , H01L33/04 , H01L51/0007
摘要： A population of bright and stable nanocrystals is provided. The nanocrystals include a semiconductor core and a thick semiconductor shell and can exhibit high extinction coefficients, high quantum yields, and limited or no detectable blinking.
摘要翻译：提供了一群明亮稳定的纳米晶体。纳米晶体包括半导体芯和厚半导体外壳，并且可以表现出高消光系数，高量子产率以及有限或无可检测的闪烁。

10. 发明授权

US07935419B1 Thick-shell nanocrystal quantum dots 有权
标题翻译：厚壳纳米晶体量子点
公开(公告)号：US07935419B1
公开(公告)日：2011-05-03
申请号：US12322813
申请日：2009-02-06
申请人： Jennifer A. Hollingsworth , Yongfen Chen , Victor I. Klimov , Han Htoon , Javier Vela
发明人： Jennifer A. Hollingsworth , Yongfen Chen , Victor I. Klimov , Han Htoon , Javier Vela
IPC分类号： B32B5/16
CPC分类号： C01B19/007 , B82Y10/00 , B82Y30/00 , C01P2002/84 , C01P2002/90 , C01P2004/64 , C01P2004/80 , C01P2006/40 , H01L29/127 , Y10T428/12028 , Y10T428/12049 , Y10T428/12181 , Y10T428/2982 , Y10T428/2991 , Y10T428/2993 , Y10T428/2995 , Y10T428/2996 , Y10T428/2998
摘要： Colloidal nanocrystal quantum dots comprising an inner core having an average diameter of at least 1.5 nm and an outer shell, where said outer shell comprises multiple monolayers, wherein at least 30% of the quantum dots have an on-time fraction of 0.80 or greater under continuous excitation conditions for a period of time of at least 10 minutes.
摘要翻译：包含平均直径为至少1.5nm的内芯和外壳的胶体纳米晶体量子点，其中所述外壳包含多个单层，其中至少30％的量子点的导通时间分数为0.80或更大，连续激发条件至少10分钟的时间。

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