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1. 发明授权

US5110851A Method for producing free-flowing, water-soluble polymer gels 失效
标题翻译：用于生产自由流动的水溶性聚合物凝胶的方法
公开(公告)号：US5110851A
公开(公告)日：1992-05-05
申请号：US461897
申请日：1990-01-08
申请人： Wood E. Hunter , Gary P. Craun
发明人： Wood E. Hunter , Gary P. Craun
IPC分类号： C08J3/12
CPC分类号： C08J3/124 , C08J2300/14 , Y10S524/916
摘要： The instant invention is directed to a method for preparing free-flowing, water-soluble polymer gels comprising:(a) reducing the size of water-soluble polymer gels by a size-reduction means, so as to produce polymer gel particles which are less than 1/2 inch in their longest dimension; and(b) adding to the size-reduced polymer gels of Step (a) 0.001 to 20 percent, by weight, of an amphipathic compound, thereby reducing the adhesion of said gel particles to themselves and other substances.The instant invention is also directed to a free-flowing, water-soluble polymer gel admixture comprising:(a) size-reduced, water-soluble polymer gel particles, wherein said gel particles are less than 1/2 inch in their longest dimension; and(b) an amphipathic compound.
摘要翻译：本发明涉及一种制备自由流动的水溶性聚合物凝胶的方法，其包括：（a）通过减小尺寸的方法减小水溶性聚合物凝胶的尺寸，以便产生较少的聚合物凝胶颗粒超过1/2英寸的最长尺寸; 和（b）向步骤（a）的尺寸减小的聚合物凝胶中加入0.001至20重量％的两亲性化合物，从而降低所述凝胶颗粒对其自身和其它物质的粘附性。本发明还涉及一种自由流动的水溶性聚合物凝胶混合物，其包含：（a）尺寸减小的水溶性聚合物凝胶颗粒，其中所述凝胶颗粒的最长尺寸小于1/2英寸; 和（b）两亲性化合物。

2. 发明授权

US4654378A Process for the manufacture of high solids, free-flowing, granular poly(dimethyldiallyl ammonium chloride) 失效
标题翻译：制备高固体，自由流动的粒状聚（二甲基二烯丙基氯化铵）的方法
公开(公告)号：US4654378A
公开(公告)日：1987-03-31
申请号：US606048
申请日：1984-05-02
申请人： Wood E. Hunter , Gary P. Craun
发明人： Wood E. Hunter , Gary P. Craun
IPC分类号： C08F2/50 , C08F26/04
CPC分类号： C08F26/04 , Y10S522/903
摘要： The instant invention is directed to a process for the manufacture of poly(dimethyldiallyl ammonium chloride) comprising:(a) casting upon a continuous belt apparatus to form a film having a thickness of 1/4 inch to 1 inch an aqueous dimethyldiallyl ammonium chloride solution having a monomer concentration of at least 65 percent, by weight, monomer, said monomer solution also containing a photoreducible dye in a concentration of 1.times.10.sup.-7 to 1.times.10.sup.-4 moles per liter, a mild reducing agent in a concentration of 1.times.10.sup.-5 to 1.times.10.sup.-2 moles per liter and thermal initiator in a concentration of 1.times.10.sup.-5 to 1.times.10.sup.-2 moles per liter;(b) passing of the solution under a series of lights which emit visible light at an intensity of 0.1 to 10,000 foot candles and controlling the temperature of the monomer solution in the range of 5.degree. C. to 65.degree. C.;(c) allowing the polymerization to proceed until a polymer gel is formed;(d) reducing the size of the polymer gel of step (c) by a size reduction means, so as to produce polymer gel particles which are less than 1 inch in their longest dimension; and(e) further polymerizing the size-reduced polymer gel particles of step (d) to obtain higher conversion, thereby producing polydimethyldiallyl ammonium chloride gel particles which are at least 70 percent, by weight, active polymer, readily soluble and free-flowing.The instant invention is further directed to free-flowing, water-soluble granules of poly(dimethyldiallyl ammonium chloride), wherein said granules contain at least 70 percent, by weight, active polymer.
摘要翻译：本发明涉及一种制备聚（二甲基二烯丙基氯化铵）的方法，包括：（a）在连续带装置上浇铸以形成1/4英寸至1英寸厚度的二甲基二烯丙基氯化铵水溶液单体浓度为单体的至少65重量％，所述单体溶液还含有浓度为1×10 -7至1×10 -4摩尔/升的光还原性染料，浓度为1×10 -5至 1×10 -2摩尔/升和热引发剂，浓度为1×10-5至1×10-2摩尔/升; （b）将溶液通过发射强度为0.1至10,000英尺烛光的可见光的一系列灯，并将单体溶液的温度控制在5℃至65℃的范围内。（c）使聚合进行直至形成聚合物凝胶; （d）通过尺寸减小装置减小步骤（c）的聚合物凝胶的尺寸，以便产生其最长尺寸小于1英寸的聚合物凝胶颗粒; 和（e）进一步聚合步骤（d）的尺寸减小的聚合物凝胶颗粒以获得更高的转化率，从而产生至少70重量％的活性聚合物，容易溶解和自由流动的聚二甲基二烯丙基氯化铵凝胶颗粒。本发明进一步涉及聚（二甲基二烯丙基氯化铵）的自由流动的水溶性颗粒，其中所述颗粒含有至少70重量％的活性聚合物。

3. 发明授权

US4525509A Method for producing free-flowing, water-soluble polymer gels 失效
公开(公告)号：US4525509A
公开(公告)日：1985-06-25
申请号：US562303
申请日：1983-12-16
申请人： Wood E. Hunter , Gary P. Craun
发明人： Wood E. Hunter , Gary P. Craun
IPC分类号： C08J3/12 , C08K5/52 , C08L39/00
CPC分类号： C08J3/124 , C08J2300/14 , Y10S524/916 , Y10S524/922
摘要： The instant invention is directed to a method for preparing free-flowing, water-soluble polymer gels comprising:(a) reducing the size of water-soluble polymer gels by a size-reduction means, so as to produce polymer gel particles which are less than 1/2 inch in their longest dimension; and(b) adding to the size-reduced polymer gels of Step (a) 0.001 to 20 percent, by weight, of an amphipathic compound, thereby reducing the adhesion of said gel particles to themselves and other substances.The instant invention is also directed to a free-flowing, water-soluble polymer gel admixture comprising:(a) size-reduced, water-soluble polymer gel particles, wherein said gel particles are less than 1/2 inch in their longest dimension; and(b) an amphipathic compound.

4. 发明授权

US4415417A Photopolymerization using copper ions 失效
标题翻译：使用铜离子的光聚合
公开(公告)号：US4415417A
公开(公告)日：1983-11-15
申请号：US399578
申请日：1982-07-19
申请人： Lee W. Bush , Marie S. Chan , Gary P. Craun , William J. Erlanson , Wood E. Hunter , Wallace B. Ramsey
发明人： Lee W. Bush , Marie S. Chan , Gary P. Craun , William J. Erlanson , Wood E. Hunter , Wallace B. Ramsey
IPC分类号： C08F2/50
CPC分类号： C08F2/50
摘要： Photopolymerization of monomers by visible light using a photoreducible dye, a reducing agent and a controlled level of copper ions allows for high molecular weight polymer formation. The molecular weight is found to be proportional to the copper ion concentration. At 10 to 1,000 ppb copper ion concentration, the molecular weight of the polymer is optimum.
摘要翻译：使用可光还原染料，还原剂和受控量的铜离子可见光单体的光聚合允许形成高分子量聚合物。发现分子量与铜离子浓度成比例。在10至1,000ppb的铜离子浓度下，聚合物的分子量是最佳的。

5. 发明授权

US4666964A Method for producing free-flowing water-soluble polymer gels 失效
标题翻译：用于生产自由流动的水溶性聚合物凝胶的方法
公开(公告)号：US4666964A
公开(公告)日：1987-05-19
申请号：US722050
申请日：1985-04-11
申请人： Wood E. Hunter , Gary P. Craun
发明人： Wood E. Hunter , Gary P. Craun
IPC分类号： C08J3/12 , C08K5/19 , C08K5/16 , C08K5/32
CPC分类号： C08J3/124 , C08J2300/14 , Y10S524/912 , Y10S524/916
摘要： The instant invention is directed to a method for preparing free-flowing, water-soluble polymer gels comprising:(a) reducing the size of water-soluble polymer gels by a size-reduction means, so as to produce polymer gel particles which are less than 1/2 inch in their longest dimension; and(b) adding to the size-reduced polymer gels of Step (a) 0.001 to 20 percent, by weight, of an amphipathic compound, thereby reducing the adhesion of said gel particles to themselves and other substances.The instant invention is also directed to a free-flowing, water-soluble polymer gel admixture comprising:(a) size-reduced, water-soluble polymer gel particles, wherein said gel particles are less than 1/2 inch in their longest dimension; and(b) an amphipathic compound.
摘要翻译：本发明涉及一种制备自由流动的水溶性聚合物凝胶的方法，其包括：（a）通过减小尺寸的方法减小水溶性聚合物凝胶的尺寸，以便产生较少的聚合物凝胶颗粒超过1/2英寸的最长尺寸; 和（b）向步骤（a）的尺寸减小的聚合物凝胶中加入0.001至20重量％的两亲性化合物，从而降低所述凝胶颗粒对其自身和其它物质的粘附性。本发明还涉及一种自由流动的水溶性聚合物凝胶混合物，其包含：（a）尺寸减小的水溶性聚合物凝胶颗粒，其中所述凝胶颗粒的最长尺寸小于1/2英寸; 和（b）两亲性化合物。

6. 发明授权

US4904715A Method for producing free-flowing, water-soluble polymer gels 失效
标题翻译：用于生产自由流动的水溶性聚合物凝胶的方法
公开(公告)号：US4904715A
公开(公告)日：1990-02-27
申请号：US231113
申请日：1988-08-11
申请人： Wood E. Hunter , Gary P. Craun
发明人： Wood E. Hunter , Gary P. Craun
IPC分类号： C08J3/12
CPC分类号： C08J3/124 , C08J2300/14 , Y10S524/916
摘要： The instant invention is directed to a method for preparing free-flowing, water-soluble polymer gels comprising:(a) reducing the size of water-soluble polymer gels by a size-reduction means, so as to produce polymer gel particles which are less than 1/2 inch in their longest dimension; and(b) adding to the size-reduced polymer gels of Step (a) 0.001 to 20 percent, by weight, of an amphipathic compound, thereby reducing the adhesion of said gel particles to themselves and other substances.
摘要翻译：本发明涉及一种制备自由流动的水溶性聚合物凝胶的方法，其包括：（a）通过减小尺寸的方法减小水溶性聚合物凝胶的尺寸，以便产生较少的聚合物凝胶颗粒超过1/2英寸的最长尺寸; 和（b）向步骤（a）的尺寸减小的聚合物凝胶中加入0.001至20重量％的两亲性化合物，从而降低所述凝胶颗粒对其自身和其它物质的粘附性。

7. 发明授权

US5480921A Process for preparing novel high solids non-aqueous polymer compositions 失效
公开(公告)号：US5480921A
公开(公告)日：1996-01-02
申请号：US299689
申请日：1994-09-01
申请人： Wood E. Hunter , Kevin W. Frederick , Randy J. Loeffler
发明人： Wood E. Hunter , Kevin W. Frederick , Randy J. Loeffler
IPC分类号： C08J3/00 , C08F6/20 , C08J3/09 , C08K5/01 , C08J9/28 , C08L33/02 , C08L33/26
CPC分类号： C08F6/20 , C08J3/09
摘要： The use of falling-film evaporation and a concentration means such as centrifugal separation to dehydrate and concentrate a water-in-oil polymer emulsion or suspension is disclosed. In a preferred embodiment, a water-in-oil polymer composition containing less than about 25% active polymer solids is dehydrated in falling-film evaporator to produce an evaporator concentrate containing less than about 5.0% water. The evaporator concentrate then flows to a separation device such as a centrifuge, wherein oil is removed to produce a composition that is substantially a polymer and emulsifying surfactant-in-oil composition containing in excess of about 60 weight % polymer solids. The centrifuge raffinate may optionally be treated in a second separation means to capture additional polymer solids, with optional recycle of the oil-rich raffinate. The concentrated polymer composition is preferably stabilized with a steric stabilizer to produce a free flowing liquid product.

8. 发明授权

US4325794A Combined visible light and thermally activated continuous polymerization process 失效
标题翻译：组合可见光和热激活连续聚合过程
公开(公告)号：US4325794A
公开(公告)日：1982-04-20
申请号：US155268
申请日：1980-06-02
申请人： Wood E. Hunter , Kenneth A. Kun , Wallace B. Ramsey
发明人： Wood E. Hunter , Kenneth A. Kun , Wallace B. Ramsey
IPC分类号： B29C35/08 , B29C41/28 , C08F2/10 , C08F2/48
CPC分类号： B29C41/28 , C08F2/10 , C08F2/48 , B29C2035/0833 , B29K2033/00 , B29K2105/0073
摘要： Continuous process for the preparation of water-soluble polymers in which highly concentrated monomer solutions may be polymerized by a combination of a visible light and a thermally initiated process.
摘要翻译：用于制备水溶性聚合物的连续方法，其中高浓度的单体溶液可以通过可见光和热引发方法的组合聚合。

9. 发明授权

US5567277A Cellulosic, modified lignin and cationic polymer composition and process for making improved paper or paperboard 失效
标题翻译：纤维素，改性木质素和阳离子聚合物组合物和制备改进纸或纸板的方法
公开(公告)号：US5567277A
公开(公告)日：1996-10-22
申请号：US566469
申请日：1995-12-04
申请人： David L. Elliott , Wood E. Hunter , Ronald J. Falcione
发明人： David L. Elliott , Wood E. Hunter , Ronald J. Falcione
IPC分类号： D21H17/23 , D21H17/37 , D21H17/44 , D21H17/45 , D21H21/10
CPC分类号： D21H17/375 , D21H17/23 , D21H17/44 , D21H17/455
摘要： A composition comprising an aqueous cellulosic furnish, a high molecular weight cationic polymer, and an anionic polymer comprising a modified lignin wherein the ratio of the cationic polymer to the anionic polymer is from about 10:1 to 1:10 on an active basis is disclosed. A process employing this composition for making paper or paperboard having improved drainage, retention and formation properties is also provided.
摘要翻译：公开了一种组合物，其包含水性纤维素配料，高分子量阳离子聚合物和包含改性木质素的阴离子聚合物，其中阳离子聚合物与阴离子聚合物的比例为活性基础为约10:1至1:10 。还提供了一种采用该组合物制备具有改进的排水，保留和形成性能的纸或纸板的方法。

10. 发明授权

US5318707A Method of clarifying phosphoric acid 失效
标题翻译：澄清磷酸的方法
公开(公告)号：US5318707A
公开(公告)日：1994-06-07
申请号：US936462
申请日：1992-08-28
申请人： Paul A. Rey , Wood E. Hunter
发明人： Paul A. Rey , Wood E. Hunter
IPC分类号： B01D21/01 , C01B25/235
CPC分类号： C01B25/235 , B01D21/01
摘要： A method for clarifying phosphoric acid by flocculation or coagulation of solids wherein an effective amount of a carboxylic-type polymer having a portion of sulfonic functionality is used as the clarification aid. Preferred polymers are high molecular weight acrylic acid/acrylamido methylpropyl sulfonic acid-type polymers.
摘要翻译：用于通过絮凝或固体凝固来澄清磷酸的方法，其中使用有效量的具有一部分磺酸官能团的羧酸类聚合物作为澄清助剂。优选的聚合物是高分子量丙烯酸/丙烯酰胺基甲基丙基磺酸型聚合物。

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